Photochemistry of phospholenes. 6. The photochemical polar addition

Photochemistry of phospholenes. 6. The photochemical polar addition of alcohols involving participation by trivalent phosphorus. Hideo Tomioka, Kazuo ...
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3070 J.Org. Chem., Vol.42,No.18,1977

Tomioka, Sugiura, Takata, Hirano, and Izawa

(95%)of 41b as a white powder: lH NMR (MezSO-de)6 7.5 (q,4 H, ArH), 6.0 (br s, 2 H, NH),2.3 (a, 6 H, ArCH3, HetH); crystallized from DMF-95% ethanol, does not melt