Pittcon
PITTCON
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eleasing the Power of Imagination" is the theme of the 47th Pittsburgh Conference and Exposition on Analytical Chemistry and Applied Spectroscopy, which will convene March 3-8,1996, at McCormick Place Convention Center in Chicago. The Technical Program will feature a plenary lecture, 41 invited symposia, and more than 1800 contributed papers and posters. Highlights will include the Waters Symposium, devoted this year to ionselective electrodes; nine award presentations; workshops on the use of chemical sensors in environmental analysis and traceability; and institutes that will focus on advances in pharmaceutical and biopharmaceutical science, food analysis, environmental analysis, and quality. The Sunday program has been expanded and will include two workshops, three user-manufacturer information exchange sessions, poster sessions, and an evening plenary session that will be open to die public and to conferees. Leon Lederman, the Pritzker Professor of Science at Illinois Institute of Technology and Director Emeritus of Fermilab, will deliver an address entitled "Does Science Have a Future in America?" At the Exposition of Modern Laboratory Equipment—featuring the latest instruments, equipment, chemicals, and 86 A
publications—more than 1000 companies will occupy more than 3000 booths. Exhibit hours have been expanded this year to allow conferees more opportunities to visit the show. The exhibit will be open Monday, 10 a.m. to 7 p.m.; Tuesday and Wednesday, 9 a.m. to 5 p.m.. and Thursday, 9 a.m. .o 4 p.m. Continuing education remains a cornerstone of the Pittsburgh Conference. More than 86 courses are being offered by the Pittsburgh Conference and the American Chemical Society. A listing of the classes appears on pp. 89 A and 102 A For more information on the Pittcon courses, consult the preliminary program or contact the Pittcon office. For more information on the ACS courses, contact ACS Department of Continuing Education, 1155 16th St. N.W. Washington DC 20036 (202-872-4508; fax 202-872-6336; e-mail
[email protected]) An employment bureau will also be provided to conferees. Preregistration information for employers and candidates is included in the preliminary program. On-site registration for conferees and exhibitors will be located in the North and East Halls of McCormick Place. Hours are Saturday, March 2, from 9 a.m. to 5 p.m. (exhibitors only); Sunday, March 3, from 10 a.m. to 7:30 p.m.; Monday, March 4, from 7:30 a.m. to 5 p.m.; and Tuesday,
Analytical Chemistry News & Features, February 1, 1996
March 5, through Thursday, March 7, from 8 a.m. to 5 p.m. Feee sre e$10 for conferees, $15 for students, and $35 for oneday admission. All registrants will be entitled to an abstract book and conference souvenir and may participate in any conference activity. The highlight of this year's activities program is the 3rd Fifty Trillion Angstrom Race, which will be held Sunday, March 3, inside the East Building of McCormick Place. Information about registration, tours, and other activities are available in the preliminary program. Special rates for airline flights and car rental discounts can be obtained through Travel Planners, 381 Park Ave. South, New York, NY 10016 (800-248-7488 or 212-5321660; fax 212-532-9426). For hotel information and reservattons, contact the Pittcon Housing Bureau (800-945-7488; fax 312567-8577). For more information about any aspect of the meeting, contact the Pittsburgh Conference, 300 Penn Center Blvd., Suite 332, Pittsburgh, PA 14235-5503 (800825-3221 or 412-825-3220; fax 412-8253224). The technical program listing begins on p. 90 A. The New Products section (p. 136 A) features instruments and other products that will be introduced at the conference.
Technical Sessions
Monday Morning Symposium: Chromatography Forum of Delaware Valley Dal Nogare Award— The Role of Theory in LC Monday Afternoon Symposium: James L. Waters 7th Annual Symposium Recognizing Pioneers in the Development of Analytical Instrumentation—Ion-Selective Electrodes Tuesday Morning Symposium: Pittsburgh Analytical Chemistry Award Symposium: Williams-Wright Industrial Spectroscopist Award Tuesday Afternoon Symposium: Pittsburgh Spectroscopy Award Symposium: Charles N. Reilley Award and the Young Investigator Award of the Society for Electroanalytical Chemistry Wednesday Morning Symposium: Keene P. Dimick Award
Wednesday Morning Institute: Pharmaceutical/ Biopharmaceutical Symposium: Pharmaceutical Analysis— Releasing the Power of MS Computer Applications in Pharmaceutical Analysis Application of CE as a Routine Analytical Tool in the Pharmaceutical Industry Symposium: In Vivo Analytical Chemistry Wednesday Afternoon Institute: Pharmaceutical/ Biopharmaceutical LC Applications in Biopharmaceuticals Symposium: Dynamic Vibrational Spectroscopy of Proteins and Other Biomolecules Bioanalytical VI: Separations and Detection Thursday Morning Institute: Pharmaceutical/ Biopharmaceutical Symposium: Chiral Separations in the Pharmaceutical Industry Extraction/Purification of Pharmaceuticals Bioanalytical VII: Peptides and Amino Acids Instrumental Applications to Toxicological and Clinical Analysis Thursday Afternoon Institute: Pharmaceutical/ Biopharmaceutical Bioanalytical Sensors for the Pharmaceutical Industry IR-Near-IR of Pharmaceuticals Symposium: The New Nucleic Acid Electrophoresis
Wednesday Afternoon Symposium: Bomem-Michelson Award Thursday Morning Near-IR Instrumentation and Methodology—Includes the Tomas Hirschfeld Award
Monday Morning Symposium: Electrodes as Materials: Where Analytical Chemistry and Materials Science Meet Electrochemistry: Specific Analytical Applications Monday Afternoon Bioanalytical I: Biomolecular Structure and Function Bioanalytical II: New Approaches to Optical and Electrochemical Sensors Tuesday Morning Bioanalytical III: Applications of Sensors and Electrodes Bioanalytical IV: Imaging, Single Cells, and Single Molecules of DNA Tuesday Afternoon Bioanalytical V: Novel Extraction Methods
Wednesday Morning Electrochemistry: Sensors Wednesday Afternoon Electrochemistry: Charge and Mass Transfer Thursday Morning Electrochemistry: Polymers, Surfaces, Films Thursday Afternoon Electrochemistry Coupled with Spectroscopic and Other Techniques
Monday Afternoon Advances in Instrumentation for Environmental Analysis Tuesday Morning Energy and Fuels: Source Rock and By-Product Analysis Tuesday Afternoon Institute: Environmental Pesticides—Detection and Analysis I Quality of Data for Environmental Assessments Wednesday Morning Institute: Environmental Field Analysis Metals Detection and Determination in Various Environmental Media IR-FT-IR Environmental Analyses and Monitoring Wednesday Afternoon Institute: Environmental Symposium: The Power of Imagination Through Immunochemistry Environmental Analysis Inorganic Analyses—Specialized Approach Pesticide, PCB, PAH—Detection and Analysis II Water Analysis Thursday Morning Institute: Environmental Workshop: Implications of New Technology and Methods with Emphasis on SW-846—Test Methods for Evaluating Solid Waste Mercury in the Environment Microwave Sample Processing for Environmental Analyses Solid-Phase Extraction and Microextraction Thursday Afternoon Institute: Environmental Symposium: Microwave-Enhanced Environmental Analysis Oils, Greases, and Fuels in Waters and Soils VOCs Friday Morning Institute: Environmental Symposium: Mixed Waste and Radionuclides GC/MS—Volatile, Semivolatile Organic Compounds, Extraction Method Inorganic Analyses Sample Preparation Techniques for Environmental Samples
Pittcon
Material Characterization V: Electrochemical Methods, X-ray Techniques, and Microscopy Thermal Analysis
Monday Morning Institute: Food Analysis Symposium: Bioanalysis of Chemicals and Pathogens in Foods Determination by AA, MS, IR, and Other Methods Thermal Analysis, Combustion Techniques, and GC Analysis of Foods Monday Afternoon Institute: Food Analysis and Quality Symposium: Traceability in Food Analysis Supercritical Fluid Extraction and Titration of Food Products Tuesday Morning Institute: Food Analysis Symposium: Nutritional Analysis Focusing on Trans Fatty Acids HPLC Analysis and Solvent Extraction of Foods
Wednesday Afternoon Workshop: Designing Your Laboratory Forensic and Toxicology Analysis Incorporating State-of-the-Art Instrumentation Sample Handling Techniques Sensors: General Thursday Morning Symposium: Analytical Rheology—Probing the Microstructure of Matter and Its Practical Applications Material Characterization VI: Other Techniques Process Analytical Chemistry I Thursday Afternoon Organics: Separation, Detection, and Validation Process Analytical Chemistry II Sample Preparation Specific Sensors and Techniques for Measurement of Specific Classes of Compounds
Monday Morning Symposium: How to Save Time With Chromatographic Analysis CE Coupled to Other Techniques Chromatographic Techniques and Software GC: Environmental Analysis Material Characterization I: Separation by Chromatography
Monday Morning Ion Trap MALDI
Monday Afternoon Analytical Instrumentation and Techniques New Instrumentation II Specialty Gas Analysis Tuesday Morning Computers in Chemistry: Chemometrics I
Monday Afternoon Symposium: Electrospray Ionization—MS of Large Molecules and the Characterization of Noncovalent Associations in Solution Material Characterization II: MS Tuesday Morning Symposium: Membrane Introduction MS: Environmental and Other Applications Tuesday Afternoon Electrospray MS Thursday Morning MS: General
Tuesday Afternoon Symposium: Pathological Science Wednesday Morning Symposium: Forensic Science Chemical Functionalities in Gasolines and Related Fuels Computers in Chemistry: Chemometrics II
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Tuesday Afternoon Institute: Quality Symposium: ISO 14001—The Environmental Management System Standard Getting a Handle on Reality
Friday Morning Macro and Micro Detection and Extraction Process Analytical Chemistry: General
Tuesday Afternoon Institute: Food Analysis Electronic Nose Solid-Phase Extraction and Ion-Detecting Techniques
Monday Morning Chemical Weapons Convention: Analytical Requirements Computers in Chemistry—LIMS Effective Analysis and Management in the Laboratory New Instrumentation I
Tuesday Morning Institute: Quality Symposium: Global Traceability and the Quality of Chemical Measurements Alive in Industry
Analytical Chemistry News & Features, February 1, 1996
Monday Afternoon CE: EKC GC: Applications HPLC: Fundamental Studies Tuesday Morning Countercurrent Chromatography SFC GC: Detectors HPLC: Instrument Developments Tuesday Afternoon GC-Atomic Emission Detection HPLC: Column Development Wednesday Morning Supercritical Fluid Extraction Wednesday Afternoon Symposium: Getting More From Your Sample: New Approaches to Sample Extraction and Selective Enrichment GC: Columns HPLC: Method Development Thursday Afternoon CE: Instrumentation and Techniques GC: Inlets and Columns Ion Chromatography HPLC: Mobile-Phase Chemistry
Friday Morning CE: Applications High-Speed GC and GC Automation
Monday Morning Symposium: Process Imaging Data-Processing Techniques in FT-IR Spectroscopy Near-IR I: Methodology Monday Afternoon Symposium: Single-Molecule Detection Comes of Age Symposium: Spectroscopic Probes of Supercritical Fluid Science and Technology FT-IR Microscopy: Applications and Data Management ICP Data Validation, Management, and Reporting Electrothermal Atomization AAS Near-IR II: Methodology
ACS Short Courses For more information, contact the hepartment of Continuing Education, ACS, 1155 16th St., N.W., Washington, DC 20036 (202-872-4508; fax 202-872-6336) Feb. 2 9 - M a r c h 2 Electronics for Laboratory Instrumentation March 1 - 3 Analytical Methods for Proteins Applied Optical Microscopy for unemists Experimental Design for Productivity ******
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Tuesday Morning Characterizing Solid Samples with Atomic Spectroscopy FT-IR: Applications and Data Processing Material Characterization III: IR Spectroscopy Near-IR, Process, and On-line Methodology Tuesday Afternoon Symposium: Nature and Applications of EPR Spectroscopy Fluorescence Analysis FT-IR Techniques and Structure Studies Fundamental Studies of Inductively Coupled Plasmas Development of Innovative Atomic Spectroscopic Instrumentation Material Characterization IV: IR-Raman Spectroscopy and Other Optical Techniques Wednesday Morning Symposium: Present and Future Impact of Array Detectors on Spectroscopy Applications of Atomic Spectroscopy Raman Spectroscopy: Techniques and In Situ Studies Surfaces: Spectroscopic Analyses of Surface Films
Wednesday Afternoon Symposium: Axial Viewing of ICP Emission—New Capabilities or New Problems? Elemental MS/ICPMS Thursday Morning Symposium: Approaching the Ideal in Atomic Spectrometry Symposium: Raman Spectroscopy in the Real World—Routine Analysis and Process Monitoring Symposium: Raman Spectroscopy in the Real World: Routine Analysis and Process Monitoring Elemental Speciation by Atomic Spectroscopy and Solutions to Atomic Spectroscopy Sample Introduction Problems Optical Sensors Spectrophotometric Analysis Thursday Afternoon Symposium: Applications of Near-Field Scanning Optical Microscopy Innovative Approaches to Sample Nebulization and Introduction New Designs for IR Instrumentation Raman Techniques and Imaging Surface Studies by Advanced Microscopic Techniques Friday Morning Symposium: War of the Nebulizers Optical Instrumentation Developments
Capillary GC: Techniques and Problem Solving Chemometrics: Principles and t i r e d e a agement o C mica Analysis Laboratories Environmental Data Validation Good Laboratory Practices and ISO 9000* Quality Standards for Chemical Laboratories I ahnratnrv Informal'
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Practical HPLC Method Development Practical LC/MS, SFC/MS, and CE/MS Practical Near-IR Analysis Quality Assurance/Quality Control in the Analytical Testing Laboratory Size Exclusion Chromatography and e ated Methods Solid-pnase Extraction in v * h e s n y
Spectroscopic Characterization of Polymers Statistical Analysis of Laboratory Data Supercritical Fluid Extraction/ Chromatnnranhv Technical WHtina york«!hor» Tecrmal Analv
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News & Features, February
1, 1996
(095) Use of the lodine/Triiodide Redox Couple as an Improved Standard Solution for Oxidation-Reduction Potential Measurements—Steven J. West (096) Flow Injection Analysis of Aqueous Samples for Magnesium with a Magnesium Ion-Selective Electrode as Detector— N.A. Chaniotakis, J.K. Tsagatakis, Steven J. West (097) Analytical Applications of Paired Carbon-Fiber Electrodes—John E. Baur, David O. Wipf (098) Digital Processing of Sinusoidal Voltammetry for Biological Molecules at Carbon-Fiber Electrodes—Wilbur B. Nowall, Werner G. Kuhr (099) Experimental Design for Optimal Fabrication of Glass Capillary Microelectrodes—Mahmoud Kamel, James L. Anderson, William Kisaalita (100) Artificial Neural Network Processing of Stripping Voltammetry for the Identification and Quantification of Heavy Metals—Michael S. Freund (101) Characterization of Recycling Electrochemical Detectors for Capillary Separations—Sunday A. Brooks, Robert T. Kennedy (102) Amplified Potentiometric Determination of pK'0, p/C, and pK2 of Hydrogen Sulfide with Ag 2 S ISE—Y.S. Su, K.L. Cheng (103) Direct Determination of Molybdenum in Seawater by Adsorption Cathodic Stripping Square-Wave Voltammetry— Yuh-Chang Sun, Chi-Ren Lan, MoHsiung Yang (104) Electrochemical Analysis of Sulfur—K. Saraswathi, K. Vijayalakshmi
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(729) Immobilization of Sulphite Oxidase into a Conducting Polymer Used for Biosensing—J.N. Barisci, G.G. Wallace, S. Adeloju (730) Miniaturized Amperometric Lactate Biosensor Based on a Flexible ThinSubstrate Using Immobilized Lactate Oxidase—Sayed A.M. Marzouk, Vasile V. Cosofret, Saad S.M. Hassan, Richard P. Buck (731) Development of an Alcohol Biosensor Based on Various Coupled Oxidase-Peroxidase Systems—Elisabeth Csoregi, A.R. Vijayakumar, L. Gorton (732) Studies on the Use of a Human Serum Albumin Biosensor Based on Conducting Polymer Electrodes—J.N. Barisci, D. Hughes, G.G. Wallace
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Chemistry
News & Features, February
1, 1996
127 A
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(1198) Determination of Amines in Biological Samples Using Microbore Chromatography with Tris (2,2'-Bipyridyl) Ruthenium(ll) Electrogenerated Chemiluminescence Detection—David R. Skotty, Timothy A. Nieman, Peter T. Kissinger (1199) Effect of pH upon UV Spectral Behavior of Ionic Compounds—Bruce E. Wilson, Jeanne B. Li (1200) Retention Behavior of Heteropoly Anions on Reversed - Phase Micellar LC— Yan-Ping Wang, Zhi-Ling Ma, Chun-Xu Wang
10:25 (1315) Development of an Automated Multidimensional GC/FT-IR/MS System for the Analysis of Complex Mixtures— Tania A. Sasaki, Kevin A. Krock, Nicholas L. Pivonka, Charles L. Wilkins 10:45 (1316) A Silicon Micromachined Gas Chromatograph Used for Fast and Accurate Analysis of Trace Impurities in Specialty, Medical, and Welding Gases— Lisa A. Nakaji 11:05 (1317) Validation of an Automatic Integration Algorithm for GC—Charles F. Steele, Ronald A. Gatten
N e a r - I R I: M e t h o d o l o g y Room E350, East Bldg. Singh Manocha, Presiding 8:30 8:50
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CE: Applications Room E265, East Bldg. Thomas E. Wheat, Presiding 8:30
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(1300) Anion Analysis Using Capillary Ion Analysis: The Chemistry and Performance of Chromate-Based Electrolytes— Jim Krol, Jeffrey R. Mazzeo, Mark Benvenuti, Joseph P. Romano, Gary Fallick, Edward R. Graver (1301) Trace-Ion Analysis of High-Purity Sample Matrices as Found in the Semiconductor and Power Industries Using Capillary Ion Electrophoresis and Conductivity Detection—William R. Jones, John Soglia, Carsten Haber (1302) Direct Measurement of Soluble Gases and Volatile Organic Species by CE—Satyajit Kar, Purnendu K. Dasgupta (1303) The Use of a Reliable CE Column Coating for DNA Fragment Separations—Mingxian Huang, Mark Bigelow (1304) Postcolumn Affinity Detection of Biotinylated Molecules in CZE—Ravi Reddy, Jing Wei, Cheng S. Lee (1305) Determination of Inorganic Ions at Trace Levels in Pharmaceutical Matrices by Capillary Ion Analysis—Michael E. Swartz, Jim Krol (1306) Separation and Indirect UV Detection of Phosphorylated Sugars Using CE—James P. Schaeper, Shahab A. Shamsi, Neil D. Danielson (1307) Determination of Small, Molecular Weight Ions in Various Industrial Samples Using Capillary Ion Electrophoresis and Conductivity Detection—John Soglia, William R. Jones (1308) Separation of Enantiomers Using the Macrocyclic Antibiotics in a Countercurrent Process by Suppression of Electroosmosis—Timothy J. Ward, Charles Dann III, Andy P. Brown (1309) Simultaneous Separation of Ammonium and Alkali, Alkaline Earth Transition, and Rare-Earth Metal Ions in Organic Media by CE—Y.S. Fung, K.M. Lau
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Monday Morning Symposium: Process Imaging (Arranged by Patrick J. Treado and E. Neil Lewis)
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Room N230b, North Bldg. E. Neil Lewis, Presiding
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Introductory Remarks. E. Neil Lewis (041) IR Spectroscopic Imaging with an InSb Focal Plane Array Detector—Curtis Marcott, Robert C. Reeder 9:10 (042) Development of IR Imaging Arrays and Their Use in Scientific Instrumentation—John F. Arens, E. Neil Lewis, Michael C. Peck 9:45 (043) Process Chemical Imaging: Methodologies and Applications— Patrick J. Treado, Hannah R. Morris 10:35 (044) A Method of Analyzing Sets of Congruent Magnetic Resonance Images by Multivariate Visual Exploration—Hans Grahn, Jan Saaf, Frank Delaglio, Paul Geladi 11:10 (045) Principle Component Analysis: Scatter Diagrams and Color Overlays for Analyzing Multivariate Image Data— David S. Bright
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Room E450a, East Bldg. Gary M. Hieftje, Shuming Nie, Presiding
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Room E258, East Bldg. Joseph J. Harland, Presiding
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Symposium: Single-Molecule D e t e c t i o n C o m e s of A g e (Arranged by Gary M. Hieftje and Shuming Nie)
Room E265, East Bldg. Christine McCreary, Presiding
High-Speed GC and GC Automation
(1310) Multidimensional Selectivity Tuning for High-Speed GC—Heather Smith, Richard D. Sacks (1311) Measuring Fuel Contamination Using High-Speed GC and CPT—Mark A. Klemp, Michael L. Akard, Anita J. Gorsuch (1312) Portable, High-Speed Micro GC Applied to the Reclamation of Contami nated Refrigerant Supplies—Mark W. Bruns, Feng Li (1313) Strategies for the High-Speed GC Analysis of Oxygen-Containing Compounds— Mark L. Nowak, Richard D. Sacks (1314) Use of EPC for Multidimensional Chromatography in the Analysis of Com plex Gas Mixtures—Ruder Schill
Monday Afternoon
D a t a - P r o c e s s i n g T e c h n i q u e s in FT-IR Spectroscopy
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(085) Calculated GC/FT-IR Calibration Curves for the Analysis of Reformulated Gasolines—John W. Diehl, Frank P. DiSanzo (086) Using Windows DDE to Customize FT-IR Software Behavior—Bruce Mcintosh, Mitch Mallough (087) Multichannel Data Acquisition Using a DSP-Controlled Step-Scanning IR Spectrometer—Dirk D. Laukien, Thomas J. Tague, Jr. (088) Validating the Ordinate Performance of FT-IR Spectrometers—R.A. Spragg, C M . Deeley (089) Automatic System Diagnostics of a Process FT-IR Instrument Using PCA Analysis of an On-Board Reference Function—David Marrow, Bruce Mclntosh, GenA Dp Dios
Chemistry News & Features, February
1, 1996
(145) Near-IR Technologies—Arnold J. Eilert, Donald Muller (146) Scattering Coefficients and Internal Standards in Extended Near-IR Diffuse Reflectance Spectroscopy—Nathan Chaffin, Peter R. Griffiths (147) Estimation of Rheological Properties of Molten EVA Using Near-IR Spectroscopy—Srinivas Vedula, Marion G. Hansen (148) Identification of Nicarbazin by Near-IR Reflectance Spectroscopy— Keith B. Bradfield, Robert A. Forbes (149) Chemical Identification of Incoming Raw Materials Before It's a Problem: At the Receiving Area—Paul J. Brimmer, Denise E. Root (150) Model System for Noninvasive Near-IR Spectra of Human Tissue— Jason Burmeister, Mark A. Arnold (151) The Study of Water as a Shift Reagent for the Determination of Polysaccharides Using Near-IR Spectrometic Analysis—Pamela R. Keating, Stacy A. MacDonald, Gary M. Hieftje (152) Fast, Precise, and Accurate Determination of Hydroxyl Value in Polyols Using FT-Near-IR Spectroscopy— Christine Simard, Martine Leblanc, Henry Buijs (153) Two-Dimensional Near-IR Correlation Spectroscopy of Amino Acids and Polypeptides—Nelson L. Sefara, Hugh H. Richardson (154) Near-IR Determination of Xylene Extractables and C 2 Content in Polypropylene Pellets—Paul Dallin, Alfred Klapper
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Introductory Remarks. Gary M. Hieftje (179) Following the Reactions of Single Molecules: Implications on Molecular Conformations and Microenvironments— Edward S. Yeung (180) Counting Molecules in Microdroplets—Michael Ramsey (181) Single-Molecule Imaging and Spectroscopy—Shuming Nie (182) Observation of Single Chemical Reactions in Solution—R.M. Wightman (183) Electrochemical Single-Molecule Detection—Allen J. Bard, Fu-Ren Fan
Symposium: Spectroscopic Probes of S u p e r c r i t i c a l F l u i d S c i e n c e a n d Technology (Arranged by Frank V. Bright) Room N228, North Bldg. Frank V. Bright, Presiding 1:30 1:35
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Introductory Remarks. Frank V. Bright (184) Preferential Solvation of PRODAN in Modified Supercritical Carbon Dioxide Mixtures—Charles A. Eckert, Barry L. West, Frank V. Bright (185) Vibrational Spectroscopy in Supercritical Fluids—Steven M. Howdle, D.G. Robertson, M.C. Clarke, M. Poliakoff
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(186) Structure-Function Relationships for Solvent Density Augmentation via Solute Rotational Relaxation in Supercritical Fluid Solutions—John F. Kauffman, Robert Anderton (187) Spectroscopy in Compressed Carbon Dioxide and Water—Keith P. Johnston, Carson Meredith, Tao Xing, Todd Ryan, William Wofford, Marye Anne Fox, Earnest Gloyna (188) Probing Dynamical Processes in Supercritical Fluids—Frank V. Bright, Jeanette K. Rice, Richard A. Dunbar, Mark P. Heitz, Emily D. Niemeyer
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FT-IR Microscopy: Applications and Data Management Room N229, North Bldg. James A. de Haseth, Presiding 1:30 1:50 2:10
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(243) Biomedical Applications of IR and Raman Microspectroscopy—V.F. Kalasinsky, Syed Ali, J.A. Centeno, F.B. Johnson, J.L. Luke (244) FT-IR Microspectroscopy Analysis of Brain Pathology—D.L. Wetzel, S.M. LeVine (245) Localization of Drugs in Hair by Synchrotron-Powered FT-IR Microspectroscopy—D.L. Wetzel, Kathryn S. Kalasinsky, G.P. Williams, John A. Reffner (246) A Mapping Study of Integrated Circuit Chip Using an IR Microscope— Koichi Nishikida (247) Use of Spectral and Image Processing to Improve Upon Challenging Mapping Analyses in IR Microspectroscopy— Pamela A. Martoglio, John A. Reffner
ICP Data Validation, Management, and Reporting
(238) Reaction Monitoring Using In Situ FT-IR—James T. Cronin (239) Analysis of Polymer Plastics by FT-IR Microscopy—Stephen D. Kent (240) Microbeam ATR of Localized Single-Fiber Finish with a SynchrotronPowered FT-IR Microspectrometer—D.L Wetzel, L. Cho, N. Morris (241) Molecular Orientation of a Single Fiber Using FT-IR Microspectroscopy—L Cho, D.L. Wetzel (242) Partial Least Squares: Correlation of Physical Properties to IR Spectra of Polyurethane Foams—Sanmitra A. Bhat, James A. de Haseth
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Electrothermal Atomization AAS Room E265, East Bldg. John Novak, Presiding 3:25
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Room E265, East Bldg. John Novak, Presiding 1:30
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(268) A New Technology in Automated ICP Validation—Scott Heideman, Maxine A. Pitard, Sung S. Chang, Duane Standish (269) Organizing AA and ICP Data for Regulatory Compliance, Reporting, and Archiving—William B. Barnett, Peter Seferovic (270) Automatic Long-Term Quality Control and Diagnosis of ICP-OES with Dedicated Software—O. Samuel, Jobin Yvon, E. Poussel, J.M. Mermet
(271) Using a "State-of-the-Art" Computing Environment to Maximize Productivity in Atomic Emission Spectroscopy— Gerald Shkolnik, Christine FlajnikRivera, Philip Wilson, Stewart Smith (272) Optimization of Calibration Accuracy in Emission Spectrometry—P. Chapon, Jobin Yvon, Leonid Litvin, D. Tournarie
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(273) Direct and Near-Real-Time Determination of Metals in Air by Impaction Graphite Furnace Atomic Absorption Spectrometry—Suneetha Indurthy, Mark V. Smith, Yong-ll Lee, Joseph Sneddon (274) Extended Calibration Curves in Zeeman AAS: How Far Can We Go?— Alexander I. Yuzefovsky, Robert F. Lonardo, John T. McCaffrey, Robert G. Michel (275) Evaluation of Pulsed Hollow Cathode Lamp Background Correction for a Portable Electrothermal Atomic Absorption Spectrometer—K.M. Aldous, E. Mills, W. Slavin, H. Qiao, P.J. Parsons (276) Determining the Optimum Approach to Processing Transient Signals in Graphite Furnace AAS—Doug Shrader, Chris Webb, Joachim Mika, Eric Vanclay (277) Method Development Considerations for Multielement Graphite Furnace AAS—G. Carnrick, Gerhard Schlemmer, F. Portala, M. Feuerstein
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Analytical Chemistry News & Features, February 1, 1996 129 A
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Near-IR II: Methodology Room N227a, North Bldg. Gregory J. Meisner, Presiding 1:30
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(296) Closing in on Polypropylene/ Polyethylene Production with Near-IR Spectroscopy—Jeffrey W. Hall, Paul J. Brimmer (297) Mid- Versus Near-IR Spectroscopy for Composition Determination of Diversely Treated Feedstuffs—James B. Reeves, III (298) Transferring Calibrations Among Polarization Interferometer FT-Near-IR Instruments Using NIST-Traceable Standards—Horst Grunewald, Donald Muller (299) Near-IR Analysis of Dry Mixes for Product Development and Quality Control—Kathryn A. Budding Lee, Al DeMoya, Mario Esposito, Jim Eden (300) Multiplicative Scattering Effects in Near-IR Spectroscopy: A Comparison of Mathematical Treatments—Rich L. Cox, Frank A. DeThomas (301) Chemical Imaging in the Mid- and Near-IR by Hadamard Transform FT-IR Spectrometry—Michael K. Bellamy, A. Norman Mortensen, Timothy L. Marshall, Robert M. Hammaker, William G. Fateley (302) Near-IR Fluorescence Imaging Detection of Ligand Binding on a Planar Evanescent Wave Sensor—John W. Silzel, Robert J. Obremski, Lisa E. Silzel, Dennis A. Palmer (303) Determination of Water in Organic Solvents by a Spectrophotometric Method with a Near-IR Dye—Mingshu Li, G.E. Pacey (304) Mid- and Near-IR Emission Spectra from Heated Gases—Chris W. Brown, John Seelenbinder, Amit Mangal, Nagendra Modadugu (305) Enhanced Collection Optics for Highly Scattering Samples on a Near-IR Acousto-optic TFS—D.L. Wetzel, J.A. Sweat
11:05 (388) Automatic Polarity Switching DCARC: A Tool to Augment Multielement Analysis of Solids—Charles Hodges, A. Kamenschikov, Gerhard Meyer 11:25 (389) Direct Solids Analysis of Geological and Related Materials: A Comparison of Spark Ablation and Slurry Nebulization ICP-AES—I.B. Brenner, A. Zander, A. Henderson 11:45 (390) Analysis of Metals and Alloys by Atomic (Absorption or Emission) Spectrometry in Combination with the Spark Sample Preparation Technique—A.I. Pchelkin, E.V. Shipova, I.P. Kharlamov FT-IR: Applications and Data Processing Room E351, East Bldg. Christine McCreary, Presiding 8:30 8:50
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Tuesday Morning Characterizing Solid Samples w i t h Atomic Spectroscopy
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Room N230b, North Bldg. F.M. Evens, Presiding (381) Enhanced Detector System for Depth Profile Analysis by GD-RF—Full Dynamic Range On-the-Fly—P. Hunault, Jobin Yvon, T. Nelis, A. Le Marchand, R. Kenneth Marcus, William G. Fateley 8:50 (382) Analysis of Simulated Nuclear Waste by Glow Discharge Atomic Emission Spectrometry—Xiaohan Pan, Tina R. Harville, R. Kenneth Marcus 9:10 (383) Depth Profile and Bulk Analyses Using a Dual-Source, Glow Discharge Atomic Emission Spectrometer—Douglas L. Harper, John T. Riley, Janet Adair, Dave Jedrejcic 9:30 (384) Depth-Resolved Analysis of Solid Materials Utilizing a Radio Frequency Glow Discharge Atomic Emission Source—Mark A. Parker, Matthew L. Hartenstein, R. Kenneth Marcus 9:50 (385) Evaluation of Different Calibration Strategies for ETV-ICPMS—Rodney W. Fonseca, Nancy J. Miller-Ihli 10:25 (386) The Role of Moisture in ETVICPMS—Trinidad Munoz, Jr., Anthony J.J. Schleisman 10:45 (387) Determination of Boron in Steel by Laser Ablation and ICPMS—Jim J. Zhu, Abe Gutierrez
(421) Very Rapid-Scan FT-IR Spectrometry—Christopher Manning, Peter R. Griffiths, Bryan Bowie (422) Room-Temperature Diode-Based Difference Frequency Lasers for Mid-IR Spectroscopy—G.J. Dixon, R.D. Peterson (423) Advances in Two-Dimensional IR Spectroscopy—W.J. McCarthy, T. Nakano, K. Krishnan (424) Use of a Reflection/FT-IR for Quantification of Anti-rust Oil Weight on Steel Sheet—Young-Min Choi, Ho-Su Ahn (425) Data Integrity of FT-IR Spectra Improved by Triplet File Format—D.K. Walker, W.P. King, R.B. Lacount, D.G. Kern, T.J. Schroyer (426) Universal FT-IR Controller/Data Station—Christopher Manning (427) Time-Resolved FT-IR Spectroscopy with Nanosecond Time Resolution— W.J. McCarthy, K. Krishnan, R.P. Dasari, T. Nakano (428) Performance Features of an Extended-Range Beamsplitter for Mid- and Near-IR Spectroscopy—Bonnie Leimer, K. Kempfert (429) Digital Signal Processing in StepScan FT-IR Spectroscopy—David L. Drapcho, Raul Curbelo, Luther L. Barber, Richard A. Crocombe, Jay R. Powell (430) Applications of Digital Signal Processing in Step-Scan FT- IR Spectroscopy—Jay R. Powell, Raul Curbelo, Luther L. Barber, Richard A. Crocombe, David L. Drapcho
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(457) Applications of Solvent Elimination LC-IR to the Analysis of Adhesives and Polymers—P.T. McKittrick, S.J. Marin 11:05 (458) Compositional Analysis of Molten Polymers Using a FT-Near-IR Fiberoptic Process Analyzer—David Marrow 11:25 (459) Prediction of Reological Properties of Molten Thermoplastic Polymers Using a FT-Near-IR Fiber-Optic Process Analyzer—David Marrow 11:45 (460) In Situ IR Monitoring of Emulsion Polymerizations—Alan J. Rein, Steven M. Donahue, E.D. Sudol Near-IR, Process, and On-Line Methodology Room E265, East Bldg. E.W. Stark, Presiding 8:30
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M a t e r i a l C h a r a c t e r i z a t i o n I I I : IR Spectroscopy
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Room E352, East Bldg. C. Dobbs, Presiding 8:30
(451) IR Study of Supercritical Fluid Drying of Polymers—Sergei G. Kazarian, Michael F. Vincent, Charles A. Eckert, Frank V. Bright 8:50 (452) Study of the Formation and Curing of Flexible Polyurethane Foams by Factor Analysis—Xihui Liang, James A. de Haseth 9:10 (453) Analysis of Carbon Species in HighTemperature Superconducting Ceramics Using IR Spectroscopy—Paul D. Maroni, Victor A. Maroni, Konrad Wu 9:30 (454) Depth Profiling by Impulse/ Response Photoacoustic Step-Scan FT-IR Spectrometry—Boiana O Budevska 9:50 (455) Quantitative IR Analysis of Engine Oil Degradation Products Using a Disposable Polyethylene IR Card—R.M. Pieper, J.E. Aysta, T.J. DeVenney, M.C. Garry 10:25 (456) FT-IR Speciation Studies of a Zwitterionic Macrocycle and Two Transition Metal-Macrocycle Complexes—Thomas L. Hatfield, David T. Pierce
News & Features, February
1, 1996
(461) Real-Time Determination of Multiple Chemical End Points with Near-IR Spectroscopy—Peter J. Brush, Edward A. Orr (462) Calibration Transfer from a Scanning Near-IR Spectrometer to a FTNear-IR Spectrometer—Jie Lin, Su-Chin Lo, Chris W. Brown (463) In-Line Monitoring of Composition and Color in Polymer Extrusion—Stephen T. Balke, Ramin Reshadat, Felix Colidonio, Sina Sayed, Saed Sayed, William R. Cluett, Christopher J.B. Dobbin, Jeffrey W. Hall (464) An AOTF-Based Solution to Near-IR Monitoring and Control of Petrochemical and Other Organic Chemical Processes—Arnold J. Eilert, Steve Brezina, Ralph Ottensmeyer (465) Monitoring Gas-Phase Production Processes with Near-IR Spectroscopy— Peter J. Brush, Paul J. Brimmer (466) On-Line Analysis of Environmentally Important Parameters in the Refining Industry Using Near-IR—Larry McDermott (467) Design and Implementation of an FT-Near-IR System for Rapid Quality Control—S.S. Cantor, K. Krishnan, C. Jansen (468) QC Methods Using IR Spectroscopy: Choosing Between Mid- and NearIR—Dean E. Roberts (469) Development and Installation of and Experiences with an Integrated On-Line Process Refinery Near-IR Analyzer System—Larry McDermott, Bruce E. DeSimas, III, John Irlam, Karen Colclazier, Jay Jackson (470) Instrumental Requirements for Transferring Calibrations in the Near- and Mid-IR—R.A. Spragg, R.A. Hoult, J. Sellors
Tuesday Afternoon Symposium: Nature and A p p l i c a t i o n s of E P R S p e c t r o s c o p y (Arranged by Herbett L. Retcofsky and Kurt S. Rothenberger) Room N230b, North Bldg. Herbert L. Retcofsky, Kurt S. Rothenberger, Presiding 1:30 1:35 2:10
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Introductory Remarks. Herbert L. Retcofsky (537) Modern EPR Instrumentttion— James S. Hyde (538) Applications of Bioanalytical EPR— Robert B. Clarkson, R.L. Belford, A.I. Smirnov (539) EPR in the Petroleum Industry— Bernard G. Silbernagel (540) Use of EPR in QA for the RadiationProcessing Industry—Marc F. Derosiers
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(541) EPR Imaging: Principles and Applications—Sandra S. Eaton, G.R. Eaton, M. Sueki, G.A. Rinard, R.W. Quine
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Fluorescence Analysis
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Room N229, North Bldg. C.L. Holifield, Presiding
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(565) Development of Real-Time Optical Biopsy Instrumentation for Cancer Diagnosis Using Fluorescence Spectroscopy—A. Katz, S. Ganesan, R.R. Alfano, H.E. Savage, S.P. Schantz (566) Characterization of the Chemiluminescence Reaction Involving Aromatic and Aliphatic Amines with Tris(bipyridyl) Ruthenium (III) by GC/MS—Michael E. Bolden, James R. Marsh, Neil D. Danielson (567) A New Analyzer for the Determination of Total Trace Sulfur Using Oxidative/Reductive Pyrolysis and Chemiluminescence Detection—Einhard Schmidt, Xinwei Yan, John Crnko (568) Determination of Hydrocarbons in Seawater via UV-lnduced Total Fluorescence and Multivariate Statistical Analysis—A.R. Muroski, Karl S. Booksh, Michael L. Myrick (569) Steady-State and Time-Resolved Fluorescence Studies of Organic Solutes in Supercritical Water—Emily D. Niemeyer, Frank V. Bright (570) Lifetime-Resolved FluorescenceDetected Circular Dichroism: The Next Generation—Sheryl A. Tucker, Melissa J. Joseph, Linda B. McGown (571) Comparative Performance of Fluorescent Species for Assay Instrumentation—Edward J.A. Pope, Art Hentschel (572) Rapid Analysis of Nitric Oxide by Chemiluminescence—Ric S. Hutte, Brian K. Clay (573) Dynamic Applications of the Maximum Entropy Method: Investigations of Time-Resolved Fluorescence Processes—Peter J. Tandler, Linda B. McGown (574) Solid-Surface Luminescence Optosensing in Continuous-Flow Systems— L.E. Zel'tser, M. Bastic
FT-IR Techniques and Structure Studies
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(581) Application of Polarization Modulation FT-IR to Studies of Atmospheric Corrosion—Richard S. Jackson, Gail R. Ball, Peter W. Faguy, Joseph Payer (582) Remote Detection of Environmental Pesticide Spray FT-IR Spectroscopy— Jack C. Demirgian (583) Step-Scan and 2-D Correlation FT-IR Spectroscopy of Liquid Crystals and Polymers Under the Influence of Electric and Mechanical Fields—H.W. Siesler, S. Okretic, U. Hoffmann (584) Interactions of Conjugated and Unconjugated Bile Salts with Model Membrane Assemblies: An IR Spectroscopic Study—Kimberly A. Parthum, Kristine M. Phillips, Sterling A. Tomellini
F u n d a m e n t a l S t u d i e s of I n d u c t i v e l y Coupled Plasmas
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(575) Chemistry of Surface-Enhanced IR Absorption Spectrometry on Metal Films and the Use of SEIRA in Hyphenated Techniques—Gregory T. Merklin, Yuxin Zhu, Peter R. Griffiths (576) SEIRA of Organic Molecules on Thin Metal Films: Apparent Violations of Selection Rules and the Role of Chemisorption in Surface Enhancement— Gregory T. Merklin, Peter R. Griffiths (577) Characterization of Antibodies by Surface-Enhanced FT-IR External Reflectance Spectroscopy—Yue Li, Chris W. Brown (578) Solid Propellant Combustion Diagnostics Using Multichannel IR Absorption Spectroscopy—Steven H. Modiano, John A. Vanderhoff (579) Application of an IR Linear Array Spectrometer to Solution Photolysis of MO (CO)6—S. Alawi, A. Napper, A. Serra, Hugh H. Richardson (580) Acid-Base Behavior in Organized Molecular Coatings: An IR Spectroscopic and Contact-Angle Titration Study— Stephen E. Creager, Scott Savett, Christine Steiger, James Clarke
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(585) Effect of a Secondary Discharge on Optical Emission from a Mach Disk Extracted from an ICP—Ma'an Amad, R.S. Houk (586) Computer Simulation of the Vaporization of Mixed Solute Particles in an ICP—Julie A. Horner, Gary M. Hieftje (587) Fundamental Investigation of the Origins of Matrix Effects in the ICP by Observation of Individual Atom and Ion Clouds—Jeffery A. Kinzer, Lizla B. Daniels, John W. Olesik
(588) A Possible Linear Relationship in ICP Matrix Effects—Scott Lehn, Gary M. Hieftje (589) Fundamental Studies of Interelement Matrix Effects in the ICP—Norman N. Sesi, Mao Huang, Scott Lehn, Kathryn E. Shanks, Gary M. Hieftje
D e v e l o p m e n t of I n n o v a t i v e A t o m i c Spectroscopic Instrumentation Room N228, North Bldg. Eileen McClendon, Presiding 3:25
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Room N228, North Bldg. Eileen McClendon, Presiding 4:05 4:25 4:45
(590) Electrothermal Vaporization with Laser-Enhanced Ionization Detection in a Flame: An Evaluation of the Detection Efficiency for Magnesium—Wendy L. Clevenger, Ken Riter, Leah Mordoh, Ben W. Smith, James D. Winefordner (591) Tunable Solid-State Laser Applications in the Excited Atomic Fluorescence Spectrometry—Jack X. Zhou, Xiandeng Hou, Karl X. Yang, Robert G. Michel (592) Rotation Instead of Absorption?— Richard Billmers, William Scharpf (593) Dynamic Range Enhancements on Charge - Injection - Device - Based Atomic Emission Systems—Michael Pilon (594) Advances Made in Plasma Optical Emission MS—A.A. Van Der Hoeff, K. Hu, S. Luan
Everything you need to know about PARTICLE SIZE and ZETA POTENTIAL. Particle Characterization Instrumentation Flexible, comprehensive systems that work in easy-to-use menu-driven environments for fast, accurate results in minutes. AcoustoSizer • Measures particle size & zeta potential in slurries up to 75% solids •Size range 0.08-10 microns diameter •Simultaneous measurement of pH, conductivity, and temp. •Automated titration
Room E265, East Bldg. Richard W. Bormett, Presiding 1:30
2:30
ESA-8000 • Measures zeta potential in concentrated suspensions • Includes automated titration for rapid iso-electric point (IEP) determination • Simultaneous measurement of pH, conductivity, and temp. • Optional flow-throuqh electrokinetic sensor
CHDF-1100 • Measures high resolution sub-micron particle size distributions • Size range 0.015-1.1 microns diameter • Fractionation-based measurement identifies complex, multimodal size distributions directly
VI Ol I
Pittcon Booth #4759
MATEC APPLIED SCIENCES
A SUBSIDIARY OF|9M I R
'5 South Stteet, Hopkinton, MA 01748 USA Tel. (508) 435-9039 • Fax: (508) 435-2165 CIRCLE 12 ON READER SERVICE CARD Analytical
Chemistry
News & Features, February
1, 1996
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Pittcon
Material Characterization IV: IR-Raman Spectroscopy and Other Optical Techniques Room E258, East Bldg. Terry McKaveney, Presiding 1:30
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(615) Analysis of Both Whole and Ground Grain with a Dedicated Interference Filter-Based Near-IR Spectrometer—Horst Grunewald, Arnold J. Eilert (616) Distribution and Chemical State of Water in Glassy Materials by Confocal Raman Imaging—Nancy L. Bradley, Michael D. Morris (617) Incorporation of Near-IR FTRaman as a Quality Assurance Tool in the Specialty Chemical Industry—Chris Petty, Jackie Behnke (618) FT-Raman Spectroscopy of Proteins and Amino Acids—P.S. Bhandare, M. Cohenford, K. Krishnan, R.J. Jakobsen (619) Probing Composition Versus Depth in Samples Using Photoacoustic Spectroscopy—Roger W. Jones, Joan Power, John F. McClelland (620) FT-IR Photoacoustic Spectroscopy in the Industrial Laboratory—Stanley J. Bajic, Randy W. Snyder, John F. McClelland (621) Case Study Demonstrating Submicron Size and Zeta Potential Analysis of Biomolecules—Peter J. Logiudice (622) Understanding the Fluorescence Dynamics of Metal-Phosphonate Monolayers and Multilayers—J.C. Home, Y. Liu, G.J. Blanchard (623) Vibrational Spectroscopy of Normal and Partially Deuterated Minerals— Esther E. Coleyshaw, William P. Griffith (624) Material Characterization Using a Miniature Dual-Beam Spectrometer with a Fiber-Optic Probe—J.T. Brownrigg
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Raman Spectroscopy: Techniques and In Situ Studies
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Room N227b, North Bldg. M. Bonner Denton, Presiding 8:30 8:35
Introductory Remarks. M. Bonner Denton (694) New Technologies in Array Detectors—James R. Janesick 9:10 (695) Spectroscopic Imaging of Biomolecules: A Challenge for Array Detectors—Edward S. Yeung 9:45 (696) Impact of Array Detectors in Fluorescence and Phosphorescence Microscopy—Thomas M. Jovin 10:35 (697) Array Detectors and Fiber Optics: A New Tool for Spectroscopists—Gary R. Sims 11:10 (698) Atomic and Molecular Spectroscopy with Array Detectors—M. Bonner Denton
Room N230b, North Bldg. N. Curtis Radcliff, Presiding 8:30
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Analytical
Chemistry
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(699) ICP-AES for Process Monitoring: An Instrument Choice Worth Considering—Gerhard Meyer, Robert Foster, C. Carroll, T. Toothaker (700) Determination of Toxic Elements in Toys Using Microsampling Hydride Generation AAS—Doug Shrader, Eric Vanclay
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A p p l i c a t i o n s of A t o m i c Spectroscopy
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Room N230a, North Bldg. Christine McCreary, Presiding
Wednesday Morning Symposium: Present and Future I m p a c t of A r r a y D e t e c t o r s o n Spectroscopy (Arranged by M. Bonner Denton)
(701) Analysis of Impurities in Chemicals and Materials for Semiconductor with ICPMS—Kazuo Yamanaka, Michiko Matsuda, Yoko Kishi, Katsuhiko Kawabata (702) ICPMS Method for the Determination of Trace Elements of Nutritional Interest—Nancy J. Miller-lhli, Rodney W. Fonseca (703) Rapid Elemental Determination (Including Traces) of Environmental Samples with ICP-AES—C. Deraed, Jobin Yvon, O. Samuel (704) Determination of Mercury at the ppt Level—Doug Shrader, Brian Frary (705) Determination of Chromium, Lead, and Mercury in Cigarette Smoke by Impaction Graphite Furnace AAS—Mark V. Smith, Suneetha Indurthy, Yong-ll Lee, Joseph Sneddon (706) Steel Analysis by Spark Emission Utilizing a High-Resolution CID-Based Echelle Spectrometer—Richard Belmore, Michael Pilon, Peter Mitchell, Rocky Gulla (707) Strategies for Analysis of Organic Solvents in the Axial ICP—R.L. Stux, Robert Foster, Frank Bulman (708) Overcoming Solvent Overloading in the ICP by Emulsification: Determination of Pb in Gasoline and Other Volatile Solvents—J. Shkolnik, A. Zander, S. Kim, I.B. Brenner
(749) In Situ Fiber-Optic Fluorescence Spectroscopy of Organic Chemistry in a Supercritical Water Reactor—Wendy C. Bell, Michael L. Myrick (750) Monitoring of Emulsion Polymerization Using Fiber-Optic Raman Spectroscopy—Abdullah Al-Khanbashi, Marion G. Hansen, Eric A. Wachter (751) Control Laboratory "Through the Package" Testing of Pharmaceuticals with Raman Spectroscopy—-Alexander Macdonald (752) Fiber-Optic-Based Multipass Raman Cell for Trace Gas Detection— Samuel F. Brown, S.M. Angel (753) Intracapillary Raman Spectroscopy with Isotachophoretic Analyte Preconcentration—Patrick A. Walker, III, Michael D. Morris (754) Development of a Remote Raman Microprobe Using a Coherent Fiber-Optic Bundle — H.T. Skinner, Thomas F. Cooney, S.K. Sharma, S.M. Angel (755) Confocal and Near-Field Raman Spectroscopy: Vibrational Information in Nanometer Domains—Steven R. Emory, Shuming Nie (756) Confocal and Super-Focal FiberOptic Raman Microprobing of Temperature and Pressure—Kimberley Schrum, Dor Ben-Amotz (757) Time- and Frequency-Domain Measurements in FT-Raman Spectroscopy—Chris Petty, Rick Hanpanowicz, Mike Daun (758) Self-Consistent Decomposition of Polarized Raman and FT-IR Spectra of Model Peptides—Reinhard SchweitzerStenner, Guido Sieler, Gerasimos Karvounis
Surfaces: Spectroscopic Analyses of S u r f a c e F i l m s Room N226, North Bldg. R.T. Oliver, Presiding
News & Features, February
1, 1996
(759) Surface Analysis by SNMS: Femtosecond Laser Post-Ionization of Sputtered and Laser-Desorbed Atoms—G. Nicolussi, M.J. Pellin, K.R. Lykke, J.L. Trevor, D.E. Mencer (760) Structure of a Novel Binary Carbon Sulfide Containing Langmuir—Blodgett Film—Yang Zhang, M.A. Firestone, T.B. Rauchfuss, Paul W. Bohn (761) Formaldehyde Adsorption on Polycrystalline Silver: A Radiotracer, Electrochemical, and X-ray Photoelectron Spectroscopy Approach—Aliston E. Thomas, Artur Kolics, Andrzej Wieckowski, Marnix ten Kortenaar, G. Frens, Z.I. Kolar (762) Characterization of Supported Mo Catalysts by TOF-SIMS—Wllliam R. Wilkinson, Marwan Houalla, Andrew Proctor, Arkady I. Gusev, David M. Hercules (763) Application of Mid-IR Spectroscopy to the Identification of Materials and to the Determination of Surface Coatings— Tye E. Barber, G.L. Powell, J.T. Neu (764) Spectroscopic Characterization of Polymerized Self-Assembled Monolayers—Roger B. Jestel, Christine E. Evans (765) ECL Imaging of Defects in SelfAssembled Monolayers of Alkyl Thiols— Miles D. Koppang, Robert P. Carson (766) Second-Harmonic Generation and AC Impedance Study of Biased CopperAlkanethiolate Monolayer Interfaccs—• Yang Zhang, Paul W. Bohn (767) Surface Reactivity of Radicals During Plasma Deposition of Silicon Dioxide and Amorphous Silicon—Ellen R. Fisher, P.R. McCurdy, K.H.A. Bogart, G.R. Barker
Wednesday Afternoon S y m p o s i u m : A x i a l V i e w i n g of I C P E m i s s i o n — N e w C a p a b i l i t i e s or N e w Problems? (Arranged by John W. Olesik) Room N227b, North Bldg. John W. Olesik, Presiding 1:30 1:35 2:10 2:45
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Introductory Remarks. John W. Olesik (843) Axial Viewing of ICP Emission: History, Capabilities, and Potential Problems—Jean-Michel Mermet (844) Can Axial Viewing of ICP Emission Replace GFAA?—Juan Ivaldi, G. Carnrick, Zoe A. Grosser (845) Axial Viewing of ICP Emission Using PMT and Imaging Detector-Based Spectrometers: The Role of Optics— Robert Foster (846) Solid Sample Introduction and Axial Viewing of ICP Emission—Gary Horlick (847) Matrix Effects and Background in Axial Viewing of ICP Emission—John W. Olesik
Elemental MS/ICPMS Room N230b, North Bldg. Gregory J. Meisner, Presiding 1:30
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(883) Design and Characterization of a Simultaneous-Detection Plasma-Source Mass Spectrograph—Thomas W. Burgoyne, Gary M. Hieftje, Ronald A. Hites (884) Radio Frequency Glow Discharge Ion-Trap MS Using Filtered Noise Fields: Elemental Analysis and Ion-Molecule Chemistry—Ritchie C. Eanes, Steven J. Christopher, R. Kenneth Marcus (885) Automated Analysis of Biological Samples by ICPMS—-P.T. Sigsworth, J. Godfrey, D. Koller, Peter Brown
AmeJican CheMical Sociity Prvsents 2:30
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(886) Geolaser Probe: A Versatile Laser Ablation System for the Direct Analysis of Geological Materials by ICP-AES and MS—Jim J. Zhu, I.B. Brenner (887) A New Isotope Dilution Technique, "Speciated Isotope Dilution MS," Is Described Using Monte Carlo Simulation— Dengwei Huo, H.M. Kingston, Dan Taylor, Bret Larget (888) Electrospray and Ion Spray MS for Elemental Speciation — Kurt Thaxton, John W. Olesik, Susan V. Olesik (889) Installed Spray Chamber as a GasLiquid Separator for the Determination of Hydride Elements by Hg-ICPMS—Ling S. Zhang, Sherry M. Combs (890) Evaluation of an Atomic Time-ofFlight Mass Spectrometer for the Analysis of Microsamples and Transient Signals—S.J. Ray, Patrick P. Mahoney, Gary M. Hieftje (891) Quality Control of Pure Silver by Laser Ablation ICPMS—Valentina Kogan (892) Investigation of Ion-Formation Processes in the Laser and Glow Discharge Ion Sources of Mass Spectrometers—G.I. Ramendik, K.G. Oksenoid
Thursday Morning Symposium: Approaching the Ideal in Atomic Spectrometry (Arranged by Gary M. Hieftje) Room N227b, North Bldg. Gary M. Hieftje, Presiding 8:30 8:35
Introductory Remarks. Gary M. Hieftje (996) Flexibility in Sample Form and Intelligence in Data Utilization—M. Bonner Denton 9:10 (997) Robustness and Precision in ICPAES—Jean-Michel Mermet 9:45 (998) Simplicity and Capability in Sources and Detectors—Gary Horlick 10:35 (999) Toward Standardless Analysis and the Ultimate Detection Limit—James D. Winefordner 11:10 (1000) High-Precision Interference-Free Atomic MS—Gary M. Hieftje
Gas Chromatography: Theory And
Practice ivionday-1 iiiii scuty i ut,sody-r i rti
