Preparation of Nonane and Decane α,ι-Dicarboxylic Acids1. William P. Hall, and E. Emmet Reid. J. Am. Chem. Soc. , 1943, 65 (8), pp 1468â1468. DOI:...
scribed by Bagard.2 It consists of the preparation of the acid chloride from the aliphatic acidand phosphorus trichloride and the subsequent addi- tion of 1.25 ...
[Contribution prom the Chemical Research Division op Schering Corporation] a-Bromination ... (1) Presented in abstract before the Division of OrganicChemistry.
The Oxidative Bisdecarboxylation of α,β-Dicarboxylic Acids1. W. von E. Doering, Milton Farber, and Adnan Sayigh. J. Am. Chem. Soc. , 1952, 74 (17), pp 4370â ...
M ethereal diazomethane. After 3 hr at room temperature excess diazomethane was distilled out on the steam bath and the solvent removed. The resulting ...
E. Doering, Milton Farber and. Adnan Sayigii. Vol. 74. Fig. 2.âInfrared absorption spectra of methylethylmale- imide and methylethylmaleimide ozonide. Fig. 3.
E. Doering, Milton Farber and. Adnan Sayigii. Vol. 74. Fig. 2.âInfrared absorption spectra of methylethylmale- imide and methylethylmaleimide ozonide. Fig. 3.
Synthesis of cis- and/or trans-Dispiro[3.1.3.1]decane-2,8-dicarboxylic Acid1. Clay M. Sharts, Alfred H. McLeod. J. Org. Chem. , 1965, 30 (10), pp 3308â3312.
methylsilane (TMS) with relative intensities in the ratio 1:2:1 (4:8:4). These unsplit peaks are assigned, respectively, as being due to four equivalent carboxyl.
WILLARD M. HOE" AND ROBERT BRUCE MOPFETT. Vol. 67. (XII) in 50 cc. of ether was cooled in an ice-bath and a solution of 6.0 g. of soclium azide. in 24 cc.
then removed in vacuo, the resulting oil was dissolved in a small amount of ether, and the ether solution placed in a refrigerator, where crystallization occurred.
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WXLLIAM P. HALLAND E. EMMET REID
pressure were taken in a Cottrell apparatus specially designed for a small quantitv of liquid, abour 2 r c . The v u . tical portion of this had a sealed on vatvuiil iacirrt si11 rnunding the Anschiitz themiornetxi. For taking a meit.ing point, a portion oi the liquid >ui ficient to cover the bulb of thc thermometer n-as put iii a test-tube. By alternately freezing and iiieitiiig the irieiting temperature was obtained. ‘Theri t lie same aniount of a substance of known nicltiug pr~iirii I I C ~ It!rai determined, was fimzeir and mr.1ter.l unci
