Protonation of Diene Complexes of Rhodium, Iridium, and Agostic

SOC., Dalton Tram. 1982, 1019. ...... Zaragoza, CSZC, 50009 Zaragoza, Spain. Received ... 5 Departamento de Quimica Inorginica, Universidad de Zaragoz...
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Organometallics 1992, 11, 127-138 (Grant CHE-8819760) and for the purchase of the Nicolet R3m diffractometer and computing system. K.P. is also grateful to the Deutsche Forschungsgemeinschaft for financial assistance. We also thank E. K. Barefield for helpful discussions. Registry No. 7,137365-76-5;8,137365-77-6;9,137393-39-6; 11,137365787;CF3C02H,76-051; Cp,ZrMe(0,CCF3),99494-55-0;

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tBuNC, 7188-38-7; Cp,Zr(Me)H, 67659-92-1. Available: Lists of complete bond

lengths and anisotropic thermal parameters,and H coordinatesfor 8 and lists of completebond length and angles and anisotropic and isotropic thermal Darameters for 9 (26 Danes): . tables o i structure fa