Meetings
ACS Northwest/Rocky Mountain meeting The ACS Northwest/Rocky Mountain Regional Meeting will be held at the University of Utah, Salt Lake City, on June 12-14. The meeting will be hosted by the ACS Salt Lake City Section. Leonard D. Spicer and Edward M. Eyring, both with the University of Utah, are general chairman and program chairman, respectively. In addition to the technical sessions, about 30 exhibits will be located in the Behavioral Science Building on the university campus. One of the highlights of the meeting will be a symposium honoring Henry Eyring in his 80th year. On-campus housing at the university may be arranged through the meeting committee (see preregistratian form on page 37). These rooms are limited so early registration is essential to ensure on-campus accommodations. Verification and check-in information will be mailed to registrants. Those desiring off-campus housing must make their own arrangements;
ANALYTICAL CHEMISTRY G. D. Christian,
Chairperson
THURSDAY MORNING Room Beh S. 101
General Analytical Chemistry I R. Hurtubise, Presiding 8:55—Introductory Remarks. R. Hurtubise 9:00—1. Thin-Layer Chromatography Using a Multichannel Detector for Two-Dimensional Fluorescence Analysis. M. L. Gianelli, J. B. Callis, N. H. Andersen, G. D. Christian 9:15—2. Investigation to Increase Sensitivity and Selectivity of a Silicon Ionization Detector. M. A. Osman, H. H. Hill 9:35—3. Measurement of Neutral Products from Electron Capture Detector. D. L. Berglund, E. P. Grimsrud 9:55—4. Use of Oxygen in Nitrogen Carrier Gas for Altering the ECD Responses to Polynuclear Aromatic Hydrocarbons. D. A. Milier, E. P. Grimsrud 10:15—Intermission 10:30—5. Gas Chromatographic Determination of Organotin Pesticides and Herbicides with Selective Flame Ionization Detection. D. Hansen, T. Gilfoil, H. H. Hill 10:50—6. Environmental Analyses by Gas Chromatography Using Fused Silica Capillary Columns. R. M. Barkley, R. S. Hutte, J. S. Stanley, M. A. Caolo, S. D. Harvey, R. E. Sievers 11:10—7. Permabond—a New Generation in High-Efficiency Chemically Bonded Columns for GC L. F. Jaramillo, E. S. Atwood, J. N. Driscoll, K. J. Conroy 11:30—8. Binuclear Complexes of Lanthanide(lll) and Silver(l) and Their Function as Shift Reagents for Aromatic and Olefinic Compounds. T. J. Wenzel, R. E. Sievers 11:50—9. Liquid Chromatographic Analysis of Biogenic Amines as "Dansyl" Derivatives R. A. Kagel, J. D. Willett, S. O. Farwell THURSDAY
AFTERNOON
Room Beh S. 101
General Analytical Chemistry II R. M. Barkley, Presiding 1:15—Introductory Remarks. R. M. Barkley 1:20—10. Resolution of Fluorescent Mixtures Using an Emission Wavelength/Decay Time Data Matrix. F. J. Knorr, J. M. Harris
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1:40—11. Time Correlation Methods for Fluorescence Lifetime Measurements. M. J. Pelletier, J. M. Harris 2:00—12. Room-Temperature Phosphorescence of Nitrogen Heterocycles and Phenols. C. Ford, R. Hurtubise, R. Dalterio 2:20—13. Fourier Transform Photoacoustic Spectroscopy. M. M. Farrow, L. B. Lloyd, R. K. Burnham, E. M. Eyring 2:40—Intermission 2:55—14. Design and Construction of a Mass Spectrometer for Identification of Collected Ions from Analytical Flames. W. H. Chambers III, H. H. Hill Jr. 3:15—15. Experience and Unsolved Problems in Pursuit of the Ultimate Spectrochemical Analytical Method. R. Woodriff, S. Lawson, G. DeWalt 3:35—16. Reduction of Interferences in a Commercial Electrothermal Atomizer for Atomic Absorption Using Two-Pronged Electrode Heating. S. R. Lawson, J. Nichols, R. Woodriff 3:50—17. Determination of Calcium in Cement by Internal-Standard Atomic Absorption Spectroscopy. H. L. Kahn, J. Sotera, A. Ratonetti 4:10—18. Recent Advances in Specific Ion Electrodes. E. S. Atwood, J. N. Driscoll, J. E. Fowler, K. J. Conroy 4:30—19. Analysis of "Difficult" Samples by ICP Spectroscopy. R. Schleicher, H. L. Kahn, A. Ratonetti 4:50—20. Behavior of Metal Ions in Solutions Containing Strong Ligands and a Chelating Ion Exchange Resin. R. J. Stolzberg 5:10—21. Precision and Interference Studies in Long-Tube-Furnace AAS Using Peak Height, Area, and Width. J. A. Nichols, R. Woodriff, F. G. DeWalt, R. L. Sanks
SATURDAY MORNING Room Beh S. 101
General Analytical Chemistry III E. P. Grimsrud, Presiding 8:55—Introductory Remarks 9:00—22. Determination of Alkaline Earth and Divalent Transition Metal Cations by Ion Chromatography with Sulfate-Suppressed Barium or lodate-Suppressed Lead Eluents. J. D. Lamb, F. R. Nordmeyer, G. Patch 9:20—23. Cell Length Dependence of Trace-Level Measurements by Thermal Lens Calorimetry. C. Dorsey, J . M. Harris 9:40—24. Flow Cell Thermal Lens Calorimetry. N. J. Dovichi, J. M. Harris 10:00—Intermission 10:15—25. Carbon Analysis of Cast Tungsten Carbide by X-Ray Diffraction. K. A. Bodily, D. C. Staplin
a list of nearby motels and hotels will be furnished upon request. Social events during the meeting include a mixer on Thursday evening. On Friday evening, June 13, a barbecue will be held from 6 to 10PM at the Snowbird ski resort—approximately 20 miles into Little Cottonwood Canyon. The price is $17.50 per person including transportation (see coupon for reservations). Meals will be available at Ballif Hall and the Union Building; both are convenient to the meeting activities. A preregistration form is included with the meeting program (see page 37) and early registration is highly recommended. On-site registration will be held in the foyer of the Behavioral Science Building beginning 8AM each day of the meeting. Non-ACS family members of attendees will be registered free. Admission to meetings, exhibits, and socials will be by badge only.
10:35—26. Electron Capture Cell Design for Gas-Phase Coulometry. S. W. Warden, E. P. Grimsrud 10:55—27. Negative Surface Ionization as an Analytical Tool for the Detection of Atmospheric Chlorine. E. A. McCullough, W. M. Moore 11:15—28. Characterization of Trace Contaminants in Oil Shale Retort Waters. M. J. Kland, H. L. Eaton, A. S. Newton 11:35—29. Surface-Bonded Thiaether Chelating Agents. B. J. Nusser, T. E. Jones 11:55—30. Potential Errors Associated with the Use of Optogalvanic Techniques for Wavelength Tuning of Tunable Dye Lasers. G. J. Beenen, E. H. Piepmeier
APPLIED CHEMISTRY R. E. Wood, Chairman THURSDAY MORNING Room Beh S. 108 9:00—Introductory Remarks 9:05—1. Environmental Impact of Underground Coal Gasification, Adsorption Characteristics of Aquifer Contaminants on Coal and Mineral Matter. E. A. Walter, T. M. Niemczyk, G. A. Merrell, J. P. Erspamer, H. Na, M. S. Silver 9:25—2. Selectivity of Catalysts Toward Coal-Derived Products. M. G. Thomas, D. G. Sample, J. L. Floyd 9:45—3. Solubility of Coal in Solvents at Room Temperature and Atmospheric Pressure. R. R. Beishline, K. Rogers, O. L. Stone 10:05—4. Catalytic Hydrogenation of Sulfur and Nitrogen in Model Compounds and Shale Oil. H. J. Moore, A. L. Tyler 10:25—Intermission 10:40—5. Rapid Chromatographic Procedure for Characterizing Hydrocarbons in Petroleum Naphtha. A. E. George, G. T. Smiley, H. Sawatsky 11:00—6. Photochemical Reactions of Polycyclic Aromatic Hydrocarbons with S0 2 Gas. D. R. Kalkwarf 11:20—7. Effect of Temperature and Impurities on the Strength of Synthetic Diamonds. D. C. Staplin 11:40—8. Recovery of Lithium from Clay by Selective Chlorination. C. F. Davidson, J. T. May 12:00—9. Structure of Detonation Waves. G. H. Duffey
BIOCHEMICAL N. H. Andersen, Chairman THURSDAY MORNING Room Beh S. 109
R.J. Brown, Presiding 9:00—1. Physical Studies of 16S rRNA in Reconstitution Buffer. J. A. Dodd, M. F. Tarn, W. E. Hill, J. D. Scott 9:20—2. Physical Studies of Reconstitution Intermediates of 30S Ribosomal Subunit from Escherichia coli. M. F. Tarn, W. E. Hill, J. D. Scott 9:40—3. Probable and Improbable Ribosomal Structures. W. E. Hill, J. D. Scott 10:00—4. Characterization of a Reverse Transcription Complex from Avian Myeloblastosis Virus. J. M. Ong, K. F. Watson, J. D. Scott 10:20—5. Retrovirus RNA-Directed DNA Synthesis by Purified Reverse Transcriptase. K. F. Watson, J. C. Olsen, J. D. Scott 10:40—6. Function of the Modified Nucleosides t6A and mt6A in Transfer RNA. Metal Binding Studies. R. P. Reddy, M. P. Schweizer, W. D. Hammill Jr. 11:00—7. New Microbial Iron Chelate Containing Malonic Acid. T. Emery 11:20—8. Activity of Ceruloplasmin in Cattle Blood. H. Righib, C. Blincoe 11:40—9. Selenium Interaction with Heavy Metals: a Model Study of a Biological System. K. L. Nuttall, F. S. Allen THURSDAY
AFTERNOON
Room Beh S. 109
N. H. Andersen, Presiding 2:00—10. Synthesis and Reactivity of E-7Methyl-2,6-Octadien-1-yl Pyrophosphate. V. M. Dixit, C. D. Poulter 2:20—11. Prenyltransferase. Studies on lonization-Return of the Allylic Substrate with 1 8 0 Geranyl Pyrophosphate. C. D. Poulter, G. M. Gurria, E. A. Mash 2:40—12. Competitive Enzyme Affinity Assays Based on Agarose Tethered 15-3HProstaglandin F 2 «. N. H. Andersen, J. Watkins Jr., S. S. Tynan 3:00—13. Enzyme Immunoassay for Penicillin in Biological Fluids. R. J. Brown. 3:20—14. Use of Prostaglandin Albumin Conjugates as Probes of Platelet Receptors. S. S. Tynan, N. H. Andersen 3:40—15. Use of Prostaglandin Antisera as Agonist Traps in Pharmacology and in Physiological Investigations. N. H. Andersen, C. H. Wilson, S. S. Tynan
4:00—16. Photoaffinity Labeling Studies with Carnitine Acetyltransferase and an Analog of Long-Chain Acyl-Coa. F. M. Achenjang, R. E. Barden 4:20—17. Synthesis and Biological Activity of D,L-Thiolcarnitine and S-Acetyl-D,LThiolcamitine. E. F. Duhr, J. M. Mauro, R. E. Barden 4:40—18. Order-Disorder Phase Transition of Phospholipid Bilayers. B. S. Hudson
CHEMICAL EDUCATION W. C. Gottschall, Chairman
THURSDAY MORNING
Chemistry Course. W. A. Wimberley, M. Frisch, R. T. Keys 10:00—22. Hydrocarbon Structure Program. M. C. Rose 10:20—23. A Year in Industry—the Report of an Academic Chemist on an NSF Science Faculty Professional Development Grant. J. M. Hayes 10:40—24. Chemistry Course for Work Experience Credit. R. A. Cormier 11:00—25. Lab Experiment That Teaches Observational Skills. G. C. Grey, R. O. Ragsdale 11:20—26. Traditional General Chemistry—More Effective Than the "Modern" Approach? D. A. Lokken 11:40—27. Some Questions About the Michelson-Morley Experiment and a Conceptual Model of Fields, Waves, and Quantization. C. Graden, R. Woodriff
Room Beh S. 110
Excited States and Photochemistry A Tutorial Series G. A. Crosby, Presiding 8:55—Introductory Remarks 9:00—1. Determination of Excited State Properties. G. A. Crosby 10:00—2. Inorganic Systems. W. F. Coleman 11:00—3. Organic Systems. T. H. Koch
THURSDAY AFTERNOON Room Beh S. 110
What Employers Look for in New Graduates W. C. Gottschall, Presiding 1:30—4. What the Mining and Mineral Industries Would Like to Find in New University Graduates. C O. Ingamells, W. G. Sherwood 2:00—5. The Ideal Petroleum Chemist. F. C Trusell 2:30—6. What a Chemistry R&D Organization Looks for in Hiring, or Chemistry Courses Are Important, But. . . F. J. Miner 3:00—7. What a Government Laboratory Looks for in Hiring a Chemist. R. L. McAvoy 3:30—8. An Academic Response. W. C. Gottschall
S. B. Wilson-Wright, Chairperson SATURDAY MORNING Room Beh S. 115 8:55—Introductory Remarks 9:00—1. American Chemical Society and the Chemical Technician. M. H. Campbell 9:20—2. Determination of Fluoride in Solids Using an Ion-Selective Electrode. A. E. French 9:40—3. Roll of the Gamma Energy Detector at Hanford, Wash. C. P. McLaughlin 10:00—4. In-Place Testing of Off-Gas Iodine Filters. S. W. Duce 10:20—Intermission 10:30—5. Hot Cell Facility and Equipment for Test of the Hanford Radionuclide Removal Process. A. P. Hamitt
INORGANIC CHEMISTRY J. M. Shreeve, Chairperson THURSDAY MORNING Room Beh S. 116
General Session
Room Beh S. 108
Non Mainstream Courses
CHEMICAL TECHNICIANS
Chemistry
R. P. Steiner, Presiding 2:00—9. Genochemistry. D. McLaughlin, E. P. Papadopoulos 2:30—10. Undergraduate Courses in Radiochemistry at Arizona State University. H. B. Whitehurst 3:00—11. Chemistry at Colorado School of Mines—Nonmainstream Curriculum. G. H. Kennedy 3:30—12. Forensic Chemistry. K. Berry 4:00—13. Computers in Chemistry. B. Litchman, E. P. Papadopoulos 4:30—14. Combined Courses for Chemistry Majors. D. H. Hunter
SATURDAY MORNING Room Beh S. 108
ACS, Chemical Careers, and Chemical Education at the High School Level J. H. Nelson, Presiding 9:00—15. Young Chemists in Transition. J. H. Nelson 9:30—16. ACS and Chemical Education. R. W. Parry 10:00—17. Education for a Chemical Career. S. A. Ware 10:30—18. Current Job Market for Chemists and Chemical Engineers. J. R. Nelson Room Beh S. 111
General Session W. C. Gottschall, Presiding 9:00—19. Computer-Assisted Instruction (CAI): Development of Beginning CAI Programs. K. W. Morse, C. Leman 9:20—20. Microcomputer Interfacing in Chemistry. A. K. Jameson, C. J. Jameson 9:40—21. Interactive Computer Program for Use with the Introductory Analytical
D. M. Roundhill, Presiding 8:35—Introductory Remarks. D. M. Roundhill 8:40—1. Crystal Structures of 4,7,13,16Pentaoxa-1-Thiacyclooctadecane and the Rubidium and Silver Complexes of That Ligand. N. K. Dalley, M. L. Campbell, S. B. Larson 9:00—2. Transition Metal Selenocarboxamido Complexes: the Crystal Structure of [Rh(Ph3P)(Se2CNMe2)(SeCNMe2)CI] • CHCl 3 . C. M. Nicks, C. F. Campana, W. K. Dean 9:20—3. Transition Metal Thiocarboxamido Complexes: the Crystal Structure of [Pd(Ph3P)(SC(0)NMe2)(S2CNMe2)]. M. M. Dobry, C. F. Campana, W. K. Dean 9:40—4. Crystal Structure of Disodium Tris(glycinato)nickelate(ll) Perchlorate Monohydrate. C. F. Campana, D. F. Sheppard, W. M. Litchman 10:00—5. Structure and bonding in a Phosphenium Ion-Metal Complex. CH3NCH2CH2N(Cbi3)PMo(775-C5H5)(CO)2. L. D. Hutchins, R. T. Paine, C. F. Campana 10:20—Intermission 10:35—6. Cyclen Pyrrolidylphosphorane and Dicyclen Phosphorane—the First Example of a Pentaaminophosphorane and a P(V)P(V) Bond. J. E. Richman 10:55—7. NMR Evidence for Unusual Bonding in Cyclen Phosphoranes. J. E. Richman 11:15—8. XPS Investigation of Ligand Effects on the Core Binding Energies of Transition Metals. R. D. Feltham, P. Brant 11:35—9. IETS Study of the Adsorption of Some Cyanide-Containing Iron Complexes on Aluminum Oxide. U. Mazur, K. W. Hipps 11:55—10. Structural Aspects of the MetalMetal Bonded Oligomers MFe(CO)4, RMFe(CO)4, R2MFe(C0)4, and Their Lewis-Base Adducts (M = Group MB, NIB, and IVB Metal, Respectively). R. D. Ernst, T. H. Cymbaluk, J. C. Vanderhooft Room Beh S. 115
General Session J. M. Shreeve, Presiding 8:35—Introductory Remarks. J. M. Shreeve
8:40—11. Selective Transport of Sr 2+ from Sr 2 + -M n + Mixtures Using a Liquid Membrane System. D. G. Garrick, J. D. Lamb, J. J. Christensen, R. M. Izatt 9:00—12. Reaction Between Sulfur Dioxide and Hexamethyldisilazane: Some Surprising Results. D. W. Bennett, L. D. Spicer 9:20—13. Reactions of Diborane with Some Phenylhydrazines. P. C. Keller 9:40—14. Cleavage of Pentaborane(9) by Trimethylphosphine. Formation of a New Hypho Triborane Compound. G. Kodama, M. Kameda 10:00—15. Factors Influencing the Release of Boron from Coal Ash Materials. A. S. Halligan, G. K. Pagenkopf 10:20—Intermission 10:35—16. Pentamethylcyclopentadienide Complexes of Metalloid Elements. P. R. Schonberg, R. T. Paine, C. F. Campana 10:55—17. Structure and Dynamics of Some Adducts of Germanium Tetrafluoride. R. 0. Ragsdale, S. D. Lessley 11:15—18. F-Ethylamine, F-Ethylimine, and Other Reaction Products of A/,A/-DichloroF-Ethylamine. R. C. Kumar, J. M. Shreeve 11:35_19. Molecular Orbital Model for the Alternation of S-F Bond Dissociation Energies in the Series SFX (x = 2-6). S. D. Roberts, W. F. Coleman 11:55—20. Laser-Induced Separation of Sulfur Isotopes in Thiophosphoryl Fluoride. L. B. Asprey, L. H. Jones
THURSDAY AFTERNOON Room Beh S. 116
Symposium Honoring Prof. Randall E. Hamm D. M. Grant,
Presiding
1:25—Introductory Remarks. D. M. Grant 1:30—21. Making of a Chromatographer. E. Johnson 1:50—22. Coal Liquefaction—Where to Go from Here. R. Kollrack 2:10—23. Tissue Acid-Base Homeostasis in Vivo. C. D. Withrow 2:30—24. How Accurate Are Clinical Chemistry Analyses in the U.S.? D. J. Boone 2:50—25. Kinetics and Mechanisms of the Reactions of Macrocyclic Tetrathiaether Ligands with Palladium(ll) Moieties. T. E. Jones 3:10—Intermission 3:30—26. Synthesis, Structure, and Reactivity of Manganese-Crown Ether Complexes. G. L. Blackmer, M. Hampton 3:50—27. Kinetics of Aquation of cisBis(oxalato)dicyanochromate(lll) and cisBis(oxalato)cyanoaquochromate(lll) in Acid Solution. K. R. Ashley 4:10—28. Chemistry of Manganese(ll) EDTA-Type Complexes. T. Shioyama, R. E. Hamm 4:30—29. Oxygen-17 NMR Studies on Iron(lll) and Manganese(lll) Water-Soluble Porphyrin Complexes. J. P. Hunt, H. W. Dodgen, S. A. Gower, I. J. Ostrich 4:50—30. Dipolar Carbon-13 Magnetic Resonance in Solids. K. Zilm, D. M. Grant
FRIDAY MORNING Room Beh S. 116
General Session G. K. Pagenkopf, Presiding 8:35—Introductory Remarks. G. K. Pagenkopf 8:40—31. Further Studies on Co(l) Complexes Formed by NaBH4 Reductions. S. Maciaszek, D. G. Holah, A. N. Hughes 9:00—32. Synthesis and Characterization of Pentadienyl Transition Metal Complexes. D. R. Wilson, A. A. DiLullo, R. D. Ernst 9:20—33. Catalysis by Multimetallics. Catalyzed Homogeneous Oxidation of Alcohols and Ketones with Molecular Oxygen in the Presence of Hexarhodium Dodecacarbonyl and Dirhenium Decacarbonyl. M. K. Dickson, N. S. Dixit, B. P. Sudha, D. M. Roundhill 9:40—34. Formation of Cr(VI) in the 254-Nm Photoloysis of Cr(lll) Complexes. W. F. Coleman, R. R. Ruminski 10:00—35. Chromium(lll) in Glucose Tolerance Factor (GTF)—a Survey of Attempts to Synthesize GTF. E. E. Zamora, T. L. Martinez, S. D. Casaus, W. F. Coleman 10:20—Intermission 10:35—36. Stereospecific Tritium and Deuterium Labeling of Chelated Amino Acids for Biological Studies. J. I. Legg, M. S. Urdea, W. B. Keyes
10:55—37. Nitrogen Base Adducts of Cobalt and Nickel Bis-Semiquinone Complexes. R. M. Buchanan, C. G. Pierpont 11:15—38. Mechanistic Studies on Methylthioether Palladium(ll) Complexes. D. M. Roundhill, S. G. N. Roundhill, U. Bagchi, W. B. Beaulieu 11:35—39. Valence Tautomerism of Copper Quinone Complexes. C. G. Pierpont, C. Goldberg, R. M. Buchanan 11:55—40. Reduction of the Mixed Bimetallic System: |Fe(CO)4SnR2] in Lewis Bases. B. A. Sosinsky, R. Shong, J. Shelly
FRIDAY AFTERNOON Room Beh S. 112
General Session K. W. Morse, Presiding 1:25—Introductory Remarks. K. W. Morse 1:30—41. New Molybdenum Complexes: Redox Models for Molybdenum Enzymes. J. T. Spence, M. Minelli 1:50—42. Characterization of the Reactions of S8 with Cyclopentadienyl Molybdenum Complexes. M. R. DuBois, M. C. VanDerveer, R. C. Haltiwanger, D. L. DuBois 2 : 10—43. Preparation and Reactions of Mo 3+ . K. Gilmore, G. K. Pagenkopf, E. H. Abbott 2:30—44. Energy Transfer in Cr(lll)-Cr(VI) Mixed Valence State Salts. W. F. Coleman, S. D. Roberts 2:50—45. Charge-Transfer Fluorescence of Eu + 3 in Bromo Elpasolite Crystal. A. K. Banerjee, R. W. Schwartz 3:10—Intermission 3:30—46. Synthesis and Characterization of Various Lanthanide and Actinide Allyl and Modified Allyl Compounds. T. H. Cymbaluk, R. D. Ernst 3:50—47. Synthesis and Coordination Properties of Dihexyl-N,N-diethylcarbamylmethylenephosphonate. S. Bowen, R. T. Paine 4:10—48. Copper Complexes of Phosphine as Sensitizers in the Valence Isomerization of Norbornadiene to Quadricyclane. D. Fife, W. M. Moore, K. W. Morse, R. Blau 4:30—49. Analysis of Solvay Clusters with AH Versus AS Diagrams. E. L. King 4:50—50. Microemulsions as Media for Modifying Inorganic Reactions. S. L. Holt
NUCLEAR CHEMISTRY D. C. Hoffman, Chairman THURSDAY MORNING Room BehS. 105
General Session D. C. Hoffman, Presiding 9:00—Introductory Remarks 9:10—1. Groundwater Composition and Element Concentration as Factors Affecting the Sorption Behavior of Geologic Media. S. J. DeVilliers, B. R. Erdal, K. Wolfsberg 9:35—2. Physicochemical States of Plutonium in Natural Waters. A. E. Nevissi 10:00—3. Determination of the Plutonium and Americium in Environmental Samples. L. A. Weinrich, C. W. Filby 10:25—Intermission 10:40—4. Microautoradiographic Studies of Radionuclide Sorption in Geologic Media. J. L. Thompson, W. R. Daniels, B. R. Erdal, S. Maestas, E. N. Vine, K. Wolfsberg 11:05—5. Particle Size Classification Characteristics of Selected Radionuclides in Fuel Reprocessing and Waste Solidification Facility Off-Gases. F. N. McDonald, S. J. Femande, B. G. Motes 11:30—6. Measurement of 129 l by Low-Energy Photon Detection. J. W. Tkachyk, B. G. Motes 11:55—7. Adsorption and Desorption Equilibria of 85Sr, 106 Ru, 137Cs, 237 Pu, and 241 Am in Laboratory Sediment-Water Systems. A. L. Sanchez, T. H. Sibley, W. R. Schell
THURSDAY AFTERNOON Room Beh S. 105
General Session R.J. Gehrke, Presiding 2:00--8. Characterization of the Gaseous Iodine-129 Species in the Process Off-Gas System at the Idaho Chemical Processing Plant. D. C. Hetzer, S. J. Fernandez, B. G. Motes
April 28, 1980 C&EN
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2:25—9. Automated System for Selective Fission Product Separations. D. H. Meikrantz, R. J. Gehrke, L. D. Mclsaac, J. D. Baker, R. C. Greenwood 2:50—10. Gamma-Ray Emission Probability Measurements of Fission Product Isotopes. R. J. Gehrke, R. G. Helmer, J. D. Baker, C. W. Reich 3:15—Intermission 3:30—11. Capture of Negative Muons in Some Simple Covalent Molecules—Can It Provide Chemical Structure Information? J. D. Knight, C. J. Orth, M. E. Schillaci, R. A. Naumann, F. J. Hartmann, J. J. Reidy, H. Schneuwly 3:55—12. Muonic Lyman X-Ray Intensities in Pure Elements. M. E. Schillaci, J. D. Knight, L. F. Mausner, C. J. Orth, R. A. Naumann, G. Schmidt 4:20—13. Studies of Short-Lived Spontaneously Fissioning Nuclides. D. C. Hoffman, D. Lee, A. Ghiorso, M. Nurmia, K. Aleklett 4:45—14. Effects of Salinity and Organic Ligands on Adsorption of Radionuclides in Sediment-Water Systems from the Hudson River Estuary. J. R. Clayton Jr., T. H. Sibley, A. L. Sanchez, W. R. Schell
ORGANIC CHEMISTRY P. W. Jennings, Chairperson THURSDAY MORNING
Section A
Room Beh S. Auditorium
Synthesis and Natural Products G. M. Rubottom, Presiding 9:00—Plenary Lecture. Acyclic Stereocontrol in Natural Product Synthesis. P. A. Bartlett 10:00—Intermission 10:20—1. Synthetic Studies of Perhydrohistrionicotoxin. G. E. Keck, J. B. Yates 10:40—2. Synthesis and Interesting Features of Bis-Trifuoromethyl Synthons and Their Use in Prostaglandin Analogs Synthesis. N. H. Andersen, S. Y. Gabhe, L. J. Theodore 11:00—3. Model Studies on the Use of Sulfoxide Chemistry for Prostaglandin Construction. N. H. Andersen, S. Y. Gabhe, L. J. Theodore 11:20—4. Studies on the Total Synthesis of Lycoricidine. G. E. Keck, U. Sonnewald 11:40—5. Synthesis and Chemistry of 1(butadiynyl)-vinyl Trifluoromethanesulfonates. M. Ladika, P. J. Stang Room Beh S. 114
Section B
General Session J. Michl, Presiding 10:00—Coffee 10:20—6. Gas-Phase Dehalogenation of o:,co-Diiodoalkanes. D. Otteson, J. Michl 10:40—7. Small-Ring Propellanes by GasPhase Dehalogenation. D. Otteson, J. Michl 11:00—8.7r-Electron Effects of Substituents from Magnetic Circular Dichroism of Substituted Benzenes. G. Weeks, K. A. Klingensmith, J. Waluk, J. Michl, W. Adcock, R. West 11:20—9. Evidence for Transannular Interaction and Hyperconjugation in Bridged Annulenes from Magnetic Circular Dichromism. J. Michl, K. A. Klingensmith, H. J. Dewey, E. Vogel, V. Boekelheide 11:40—10. Photosolvolysis and Related Reactions of a 1-Arylethyl Acetate. D. A. Jaeger, G. H. Angelos
THURSDAY AFTERNOON Section A Room Beh S. 115
Synthesis W. W. Epstein, Presiding 1:30—11. Preparation and Characterization of 2-Substituted 6-Methylthiobicyclo[2.2.1] heptanes. R. S. Glass, J. R. Duchek, U. D. Gopala Prabhu, W. N. Setzer, G. S. Wilson 1:50—12. Preparation and Conformational Analysis of Thymidine 3',5'-Cyclic Nucleotide Derivatives. A. E. Sopchik, G. S. Bajwa, W. G. Bentrude 2:10—13. Synthesis of Depsipeptides Containing Lanthionine as Models of the Quinomycin Antibiotics. G. Kini, R. K. Olsen
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C&EN April 28, 1980
2:30—14. Studies Toward the Synthesis of Streptolutine. W. J. Hennen, R. K. Olsen 2:50—Intermission 3:10—15. Synthesis of 14 C- or 13 C- Containing Furan Compounds for the Purpose of Metabolism Studies. W. H. Campbell, P. W. Jennings 3:30—16. Determination of Chlorzoxazone and Acetaminophen in Pharmaceutical Formulations by GLC. J. D. Goss, J. J. Shah 3:50—17. Synthesis of an Inhibitor of Squalene Synthetase. C. D. Poulter, M. D. Thompson, R. G. Gaughan 4:10—18. Nucleotide Synthesis in Formamide. A. M. Schoffstall, R. J. Barto 4:30—19. Ring-Expansion Routes to Hormone Analogs. R. W. Thies, J. Pierce, S. Yue Room Beh S. 114
Section B
Active Phosphine Oxides. M. Moriyama, W. G. Bentrude 1:50—39. Nature of the Phlobaphenes from Douglas Fir Bark. M. L. Laver, R. W. Hemingway, P. M. Loveland 2:10—Intermission 2:30—40. Metal Binding Site in Fulvic Acid. R. A. Ekeland, P. W. Jennings 2:50—41. Structural Parameters Affecting Phase-Transfer Catalysis by Crown Ethers and a Comparison of the Effectiveness of Crown Ethers to That of Other PhaseTransfer Catalysts. P. E. Stott, J. S. Bradshaw, W. W. Parish 3:10—42. Thermal Rearrangements of Fluorinated Benzenes. J. R. Highsmith, L. T. Scott
Room Beh S. 114 Heterocycles
Section B
General Session
K. D. McMichael,
E. L. Allred,
1:30—43. Annulation of Nitrogen-Containing Rings via Intramolecular Ene Reactions. G. E. Keck, R. R. Webb 1:50—44. Synthesis of Oxygen and Nitrogen Analogs of Cannabinoids. V. K. Mahesh, R. Sharma, M. Maheshwari 2:10—Intermission 2:30—45. Reaction of Selectively Deuterium-Labeled Azetidinium Salts with Butyllithium. M. T. Wills, I. E. Wills, L. Von Dollen, B. L. Butler, J. Porter, A. G. Anderson Jr. 2:50—46. Tris(Amino) Boranes—the Effect of Angle Strain on Hybridization. J. E. Richman, N. C. Yang, L. L. Andersen 3:10—47. Studies in Antifertility Agents: Synthesis of Basic Ethers of 2(1',2'-Diphenylvinyl)-3-phenylbenzo- and Naphtho 2,1-b Furans. V. K. Mahesh, M. Maheshwari, R. Sharma 3:30—48. Palladium Catalyzed Alkylations—New Synthetic Methods. E. Keinan, B. M. Frost
Presiding
1:30—20. Steric and Electronic Factors in the Mechanism of Anchimeric Assistance for the Tetracyclo[6.4.1. 1 - 8 .1 3 - 6 .0 2 ' 7 ] Undec9-En-11-Y1 System. E. J. Allred, G. D. Lyon, G. G. Stroebel, R. J. Coots 1:50—21. Relative Rates of Heteroarylmethyl Radical Formation. H. Soppe-Mbang, G. J. Gleicher 2:10—22. Free Radical Halogenations. V. Reaction of Chlorosulfonyl Isocyanate with Alkanes. M. W. Mosher 2:30—Intermission 2:50—23. Rates of Racemization and Activation Parameters of Free Acidic Amino Acids and Free Hydroxy Amino Acids. G. G. Smith, D. Wonnacott 3:10—24. Evidence for Intramolecular Amino Group Assistance in Dipeptide-Bound Amino Acid Racemizations. G. G. Smith, R. C. Evans 3:30—25. Rate of Racemization and Activation Parameters of Amino Acids in Collagen. G. G. Smith, B. Silva de Sol 3:50—26. Stereochemistry of Intramolecular Electrophilic Condensation Reaction. C. D. Poulter and C.-H. R. King 4:10—27. Solvolysis of Small-Ring Trialkyl Diazenium Salts. E. L. Allred, J. E. Oberlander, C. G. Sanders
Presiding
PHYSICAL CHEMISTRY E. R. Bernstein, Chairperson THURSDAY MORNING
FRIDAY MORNING
Section A
Room AAC 127
General Session P. W. Jennings,
Presiding
9:00—Plenary Lecture. Mechanisms of Some Fundamental Organometallic Reactions and Their Implications in Transition-MetalCatalyzed Organic Syntheses. J. K. Stille 10:00—Intermission 10:20—28. Transition-Metal-Catalyzed Cleavage of Small Carbocycles. R. B. Taylor, P. W. Jennings 10:40—29. LTA Oxidation of Bicyclic Cyclopropanols. G. M. Rubottom, C. W. Kim 11:00—30. LTA Oxidation of Aldehyde Enol Silyl Ethers. G. M. Rubottom, R. Marrero, D. K. Heckendorn 11:20—31. Dimerization of 2-Trimethylsiloxy-1,3-butadiene. M. D. Waddington, P. W. Jennings 11:40—32. Alkylthiylations of Pentacovalent PH Compounds. W. Heide, W. G. Bentrude Room Beh S. 114
Section B
Heterocycles D. A. Nelson, Presiding 10:00—Coffee 10:20—33. Synthesis of Some 1,3-Disubstituted-2-Pyridones and Their Use as Fluorescent Labels. J. H. Bush, D. A. Nelson 10:40—34. Application of 13C NMR Spectroscopy to the Synthesis of Ammonium2,4,5-Trinitroimidazole. B. W. Harris 11:00—35. Heteroaromatic Cope Rearrangement of 1-Heteroaryl-2-Vinyl Cyclopropanes. G. Maas, C. Hummel 11:20—36. Conformations of 2-Oxo- and 2-Thio-1,3,2-Oxazaphosphorinanes. S. Chandrasekaran, W. G. Bentrude 11:40—37. Thermolytic Generation of Azetidines. K. A. Nelson, G. S. Bajwa, W. G. Bentrude FRIDAY AFTERNOON
Room Beh S. 106
Theory B. M. Ladanyi, Presiding
Section A
Room Beh S. 115
General Session J. S. Bradshaw, Presiding 1:30—38. New Preparations of Optically
9:00—1. Fermi Resonance of Raman Modes: a Theoretical Investigation of Concentration Effects in Molecular Liquids. J. L. McHale, C. H. Wang 9:20—2. Fundamental Roles Played by Symmetry Considerations in Quantum Mechanics. G. H. Duffey 9:40—3. Relativistic Effective Potentials for the Study of Molecules Containing Heavy Elements. P. A. Christiansen 10:00—4. Barrier Parameter for Doped M-l-M Diodes and Their Relation to Surface Chemistry. K. W. Hipps, U. Mazur 10:20—Intermission 10:30—5. General Method for Deriving Conformation-Dependent NMR Coupling Constant Expressions. D. Caldwell 10:50—6. Explicit Model for the Coupling Constant of the Hydrogen Molecule. P. Redington, D. Caldwell 11:10—7. Computer Analysis of the BricePhoenix Differential Refractometer. E. W. Anacker, A. E. Westwell, D. C. Anacker. 11:30—8. Applications of Polynomial Root Interpolation to Potential Surfaces: H3 and H 2 0. J. Downing, J. Michl 11:50—9. Computation of Chemical Equilibria in Complex Systems. H. J. Byker, R. E. R. Craig, I. Eliezer, R. A. Howald Room Beh S. 107
Nonlinear Optics C. H. Wang, Presiding 9:00—10. Coherent and Incoherent Multiphoton Spectroscopy. B. S. Hudson 9:45—11. Multiphoton Spectroscopy. E. R. Bernstein, K. Swift, J. D. Webb 10:30—Intermission 10:45—12. UV Multiphoton Photochemistry of CF2CI2. F. B. Wampler, J. J. Tiee, W. W. Rice 11:05—13. Two-Photon Spectroscopy of UF6 in the Near Ultraviolet. P. Kennedy, E. R. Bernstein 11:25—14. Electronic Raman Scattering— Transition Metal Hexafluorides. D. L. Michalopoulos, E. R. Bernstein 11:45—15. Two-Photon Spectroscopy of Osmium Tetroxide. K. M. Swift, E. R. Bernstein I
THURSDAY AFTERNOON Room Beh S. 106
Laser Photochemistry B. Wampler, Presiding 1:30—16. Laser-Induced Temporal and Wavelength Resolved Spectroscopy of the 2 2 ~ - 2 I I and 2 A - 2 I I Systems of CH and CD Isolated in Rare Gas Matrices. R. Bhatnagar, J. L. Wilkerson, G. R. Smith, W. A. Guillory 1:50—17. Photochemical Studies of Catalytic Hydrogenation Using Wilkinson's Catalyst. J. Peterson, D. W. Bennett, L. D. Spicer 2:10—18. Infrared Laser Photolysis: a New Tool for the Study of Prebiotic Chemistry. D. D. Davis, G. R. Smith, W. A. Guillory 2:30—19. Photochemical Generation and Spectroscopy of a Diazaquinodimethane Derivative. R. D. Miller, H. J. Dewey, J. Michl 2:50—Intermission 3:00—20. Adiabatic Photochemistry of 1,4Dewarnaphthalene in N 2 Matrix. S. L. Wallace, J. Michl 3:20—21. C0 2 Laser-Induced Decomposition of 2-Methyl Oxetan. R. Bhatnagar, P. E. Dyer, G. A. Oldershaw, W. A. Guillory 3:40—22. Determination of Initial RotationalQuantum-State Distributions of Diatomic Chemical Reaction Products Using the Laser "Pump-and-Probe" Technique. W. H. Breckenridge, D. Oba 4:00—23. Molecular Beam Photoionization of OCS Monomers and Dimers. E. A. Walters, N. C. Blais 4:20—24. State-to-State RXN Dynamics of CH(v = 0,1) Radical with 0 2 . R. C. White, M. L. Lesiecki, W. A. Guillory Room Beh S. 107
Phase Transitions, Nucleation, Condensed Phase Dynamics E. R. Bernstein, Presiding 1:30—25. How Do 2-D Crystals Melt? J. P. McTague 2:15—26. Laser Light Scattering Investigation of the Effect of Relaxation and RotationTranslation Coupling in Molecular Solids and Polymer Solutions Which Undergo Phase Transition. C. H. Wang. 3:00—27. Recent Advance in Understanding the Molecular Details of Nucleation Phenomena. A. W. Castleman Jr. 3:45—Intermission 4:00—28. Light-Scattering Studies of the Structural Phase Transition in sym-Triazine. C. L. Pan, E. R. Bernstein 4:20—29. Light Scattering from Flexible Molecules. B. M. Ladanyi, T. Keyes 4:40—30. Rayleigh-Brillouin Scattering and Structural Relaxation of Polystyrene-Cyclohexane Solutions. W. R. Lempert, C. H. Wang 5:00—31. Structural Phase Transitions in (RNH3)2MCI4 Salts: an NMR Study of Crystalline Models of Lipid Bilayers. H. W. Dodgen, R. D. Willett, G. F. Needham
SATURDAY MORNING Room Beh S. 106
Spectroscopy, General Session J. D. Webb, Presiding 9:00—32. Inhomogeneous Broadening of the ODMR and T r S 0 Optical Transitions of 1Methylnaphthalene in 3-Methylpentane. R. L. Williamson, T. J. Aartsma, A. L. Kwiram 9:20—33. Triplet State Spectroscopy of Matrix-Isolated Acridine and Phenazine. M. B. Mitchell, G. R. Smith, W. A. Guillory 9:40—34. Absorption Spectroscopy of Cryogenic Solutions. J. Lee, E. R. Bernstein 10:00—35. Magnetic Circular Dichroism of Matrix Isolated Aromatic Hydrocarbons. K. A. Klingensmith, J. Michl 10:20—Intermission 10:30—36. Magnetic Circular Dichroism of Cyclic 7r-Electron Systems. The Spectrum of S3N3-. J. Waluk, J. Michl 10:50—37. Alignment of Aromatic Molecules Embedded in Stretched Polyethylene. P. B. Pedersen, E. W. Thulstrup, J. Michl 11:10—38. Resonance Raman Spectrum of Lycopene. L. C. Hoskins 11:30—39. Polarized Emission of Partially Aligned Molecules in Uniaxial Samples. M. Gisin, J. Michl 11:50—40. Fifth Raman Band (and Others) of Solvated Perchlorate. A. G. Miller, J. W. Macklin
12:10—41. Mixing of Inter- and Intramolecular Motions in the Vibrations of the Crystals of a Large Flexible Molecule. B. S. Hudson, N. E. Schlotter
3:30—6. Criterion for Quantum Stochasticity in Intramolecular Dynamics. R. A. Marcus 4:30—7. Laser-Induced Dissociation of Molecules. Y. T. Lee
ACS Northwest/Rocky Mountain Regional Meeting
Room BehS. 107
General Session E. McCullough, Presiding 9:00—42. Mechanism of the N2 Self-Exchange Reaction. A. L. Rockwood, E. A. McCullough Jr. 9:20—43. Mechanism of the CO Self-Exchange Reaction. A. L. Rockwood, E. A. McCullough, Jr. 9:40—44. Temperature Dependence of Chemical Shielding in Pyramidal AX3-Type Molecules. A. K. Jameson, C J. Jameson 10:00—45. Experimental and Theoretical Studies of the Strongly Positive Temperature Dependence of the Quenching of Mg(3P) by H2. W. H. Breckenridge, W. L. Nikolai, N. Adams 10:20—Intermission 10:30—46. Critical Analysis of the Moderated Recoil Technique for Measuring Thermal Rate Constants. J. Chang, L. D. Spicer 10:50—47. Interaction of Oxygen and Cesium with LaB6(100). S. A. Chambers, P. R. Davis 11:10—48. Solution Thermodynamics of 7-Butyrolactone and Ethyl Acetate in Isooctane. J. H. Rytting, Y. T. Hwang, T. Higuchi 11:30—49. Thermodynamics of the CaO-Si02 System. I. Eliezer, N. Eliezer, R. A. Howaid, P. Viswanadham 11:50—50. Polarization Ratio Spectroscopy: a Description of the Technique and Its Utility in the Assignment of the Charge-Transfer Excited States of d 6 Ruthenium Chelates with Bi- and Tridentate Ligands. S. F. Agnew, G. A. Crosby 12:10—51. Group Theoretical Assignment of the Electronic Transitions in Ruthenium(ll) Bis Chelates. M. L. Stone, G. A. Crosby
F. V. Hanson,
Chairperson
FRIDAY MORNING
8:50—Introductory Remarks. F. V. Hanson 9:00—1. Petroleum Resources in the Overthrust Belt. L. Hale 9:30—2. Coal Resources of the Intermountain West. H. Doelling 10:00—Intermission 10:15—3. Coal Combustion Technology. D. W. Pershing 10:45—4. Coal Gasification Technology. W. H. Wiser 11:15—5. Coal Liquefaction Technology. L. L. Anderson 11:45—6. Fischer-Tropsch and Related Synthesis Gas Conversion Technology. G. R. Hill 1:30—7. Bituminous Sands Resources of the Intermountain West. J. Campbell 2:00—8. In-Situ Bitumen Recovery Technology. K. P. Thomas 2:30—9. Production of Bitumen and Synthetic Crude' from Bituminous Sands: AboveGround Technology. A. G. Oblad 3:00—10. Bitumen and Bituminous Sand Derived Liquid Conversion Technology. J. W. Bunger
MATERIALS SCIENCE IN SPACE Chairperson
General Session J. H. Futrell, Presiding
FRIDAY MORNING
9:00—52. Tandem-Ion Cyclotron Resonance Study of the Reaction of N 2 + with S0 2 . J. H. Futrell, R. Orth, H. Nishimura 9:20—53. Surface Structure Determinations by Angle-Resolved X-Ray Photoemission from Adsorbate Core Levels. C. S. Fadley, S. Kono, J. T. Lloyd, K. A. Thompson 9:40—54. Temperature-Dependent AngleResolved X-Ray Photoemission Study of the Valence Bands of Single-Crystal Tungsten: Observation of Direct Transitions and Phonon Effects. Z. Hussain, C. S. Fadley, S. Kono 10:00—55. Spontaneous Raman Signal Profile Analysis of the A-, Mode of the H g l 4 = Species in Solution. F. G. Baglin 10:20—Intermission 10:30—56. Secondary Ion Mass Spectrometry of Species Trapped in Argon Matrices. H. T. Jonkman, D. H. Powell, J. Michl 10:50—57. Secondary Ionization of Solid NO, 0 2 , and C0 2 . H. T. Jonkman, R. G. Orth, J. Michl 11:10—58. Crystal and Molecular Structure of 3-Methylbenzoic Acid. R. J. Neustadt, F. W. Cagle Jr., A. D. Eastman
Room Beh S. 115
S Y M P O S I U M HONORING HENRY EYRING IN HIS 80TH YEAR S. H. Lin, Chairperson
FRIDAY NOON
MORNING
ANU AFTER-
Room AAC Auditorium 8:55—Introductory Remarks 9:00—1. Some Models in Chemistry. H. Eyring 10:00—2. Bond Exchange Among Hydrogen Atoms and Molecules. D. R. Herschbach 11:00—3. Reaction Path Hamiltonian for Polyatomic Molecules: Application to Tunneling Corrections for Rate Constants and to Intramolecular Energy Transfer. W. H. Miller 1:30—4. Photoelectrochemical Kinetics of Hydrogen Evolution. J. O'M. Bockris 2:30—5. Computer Graphics Studies of Laser-Induced Photodissociation. W. E. Lamb Jr.
ON-CAMPUS HOUSING RESERVATION Name___
Room Beh S. 110
M. Good,
Room Beh S. 110
University of Utah, Salt Lake City June -12-14, 1980
ENERGY RESOURCES IN T H E W E S T E R N U.S.
8:55—Introductory Remarks 9:00—1. Scope of Philosophy of the Materials Processing in Space Program. J. Carruthers 9:15—2. Review of Some Previous Materials Science Experiments in Space. R. Naumann 9:45—3. Vapor Deposition Crystal Growth in Space. F. Rosenberger 10:15—4. Science of the Float Zone Experiments. L. E. Scriven, A. Fowle 10:45—5. Monolayers at Liquid-Gas Interface as Related to Float Zone Experiments. J. A. Mann 11:15—6. Fusion Shell Research. R. Brown 11:45—7. Fluids Experiments Systems. B. Askins
OCCUPATIONAL SAFETY AND HEALTH J. H. Nelson,
Chairperson
FRIDAY MORNING Room Beh S. Auditorium 8:55—Introductory Remarks 9:00—1. Impact of Occupational and Environmental Health Regulations on Future Responsibilities of the Chemical Industry. G. D. Clayton 9:55—2. Nitrosamines and Occupational Safety. D. H. Fine, D. P. Rounbehler 10:30—Intermission 10:40—3. Methods of Predicting Occupational Health Effects of By-Products from Shale Oil Production. M. J. Kland 11:15—4. Technical Aspects of Diffusional Monitoring of Organic Vapors in the Workplace Environment. K. L. Scheel, F. W. Snowden 1:30—5. High-Resolution Gas Chromatography of Polynuclear Aromatic Hydrocarbons. M. L. Lee 2:15—6. Analytical Chemistry and OSHA. F. A. Madsen 3:15—7. Sulfur in Aerosols: Implications of Chemical Characterization. D. J. Eatough
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April 28, 1980 C&EN 37
