Sedimentation and Hydraulic Classification - ACS Publications

AND ENGINEERING. CHEMISTRY. Vol. 40, No. 1 estimating net power requirements of mixers. The data for the nomograph were obtained from their own...
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INDUSTRIAL AND ENGINEERING CHEMISTRY

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estimating net power requirements of mixers. The d a t a for t h e nomograph were obtained from their own and from those previously noted in the literature. Two articles by Mack and Uhl (8, 4 ) have appeared pertaining t o performance of agitators. The fist deals with agitator power requirements for gas-liquid contacting equipment, and the second discusses mass and hea,t transfer in agitator systems. Both articles are intended t o show how impellers can be selected and operated for a given process application based on existing data in the literature, or from d a t a from plant or pilot plant operation. There are a few new data in these articles, but t h e articles are of value primarily in calling attention t o existing information already in t h e literature which may have been overlooked by newcomers t o the field. I n the fist article Mack and Uhl present again data on gasliquid contacting b y mixers and extend t h e d a t a for oxygen, carbon dioxide, chlorine, and hydrogen. They also give d a t a for the power characteristics of wire impellers. T h e wire impellers are simply described as having been made with piano wire, and t h e configuration and size are not mentioned. An analysis of power function os. Reynolds number is made along the conventional lines established by White and others, and it is emphasized t h a t power absorbed by impellers operating in baffled tanks may be as many as five times greater than power consumption in unbaffled tanks. Several hypothetical illustrations are given t o show how t o scale u p from pilot plant data t o large size in order to illustrate the method of handling the power relations discussed in the article. These examples are exercises in the use of the dimensionless equations correlating impeller performance and are of use for this reason. Illustrative examples on gas-liquid contacting concerning t h e absorption of carbon dioxide in a slurry of metallic hydroside are also given. This is an extension of previous work of t h e author with others. Several other hypothetical examples pxtaining t o gas-liquid contacting are also worked out.

Vol. 40, No. 1

The second article dealing with mass and heat transfer makes use of dimensionless correlations of Hixon and Baum and of t h e heat transfer d a t a of Chilton, Drew, and Jebens. Several examples for hypothetical cases are worked out t o illustrate the use of these data. A table for film coefficients of heat transfer for a large number of liquids is given. These coefficients are either those reported by Chilton, Drew, and Jebens or have been cornputed by the authors based on the dimensionless correlation of Chilton, Drew, and Jebens. There are no new experimental data t o warrant the assumptions and conclusions refcrred t o in t h e article. Several assumptions and inferences are made regarding heat transfer with relation t o power input t h a t are open t o serious question, and it is not likely t h a t the data of Chilton, Drew, and Jebens can be extended with any degree of accuracy beyond the condition specifically stated in their work. Mack and Uhl make extensions of the data to baffled conditions which were not covered by those reporting the data, and the assumption upon which the calculations are made cannot as yet be substantiated from experimental evidence. Review. A review article covering information on mixing during the preceding year was presented by Rushton ( 7 ) . This, . ~ N DENGINEERIKG together with previous reviews in INDUSTRIAL CHEMISTRY, includes a bibliography which will bring up t o date all information in t h e technical literature pertaining to mixing. LITERATURE

CITED

(I) Bridger, G. L., Wilson, R. A., and Burt, R. B., IXD. ENG.CHEDI., 39, 1265 (1947). (2) Chaddock, R. E., Chem. Eng., 53, 151 (Nov. 1946). (3) Mack, D. E., and Uhl, V. W., Ibid., 54, No. 9, 119 (1947). (4) Ibid., 54, No. 10, 115 (1947). ( 5 ) Martin, J. J., Trans. Am. Inst. Chem. Engrs., 42, 777-81 (1946). (6) Olney, R. B., and Carlson, G. J., Chem. Eng. Progress, 43,No. 9,

467 (1947). (7) Rushton, J. H., IND.ENG.CHEY.,39, 30, 43 (1947).

RECEIVED November 10, 1947.

SEDIMENTATION AND HYDRAULIC CLASSIFICATION mg

ANTHONY ANABLE, THE

DORR

C O M P A N Y , NEW YORK 22, N. Y.

E D I M E N T A T I O N and hydraulic classification are very old unit operations, the theory of which is well understood. Therefore, new developments of a basic character seldom occur in the short space of time of a year or two. On the other hand, improvement in the design of mechanical equipment is a continuous process which leads steadily towards increased efficiency and a general over-all bettering of operation. Sedimentation. The Trebler clarifier, which was mentioned in this journal's annual review of January 1946, has been rechristened the Dorr Duo-Clarifier (Figure l ) , and a dcscription of this unit i n its prcsent form may be of interest. It is basically a modification of the standard Dorr clarifier and consists of such a unit divided diametrically into two compartments by a vertical dividing wall extending from above the liquid level down to the sludge level. One compartment is used for primary scttling and the other for secondary settling. Tlic fccd well and the overflow collection trough are bisected by the dividing wall with separate feed and overflow lines. Recirculation take-offs are also separated and function independently.

Figure 2 shows this unit used in connection with a Dorrco DuoFilter for treating a biological waste a t a milk plant. Flow goes fist to the primary filter and then, in sequence, to the primary clarifier, secondary filter, and final clarifier. Because of lower installation costs of a Duo-Clarifier compared with two standard clarifiers of equal combined area, plus lower maintenance costs and simpler operation, the unit is proving attractive for small communitics, institutions, and trade waste-treatment plants. From two milk waste-treatment plants the following data are available. Results based on daytime composites over a 16-day Deriod. Flow, Gal./Min. 31 21 Flow Gal / i U i n .

31 21

Recirculation Ratio B.O.D., P.P.M. Second5% RePrimary ary Raw Final iiioved 533 20 95.8 1.26 2 23 3.52 4.52 648 33 95. Suspended Solids. P.P.M. % ReRaw Final moved 330 31 90.3 363 30 90.1

Total Solidi, P.P.II1 % ReRaw Final moved 1182 712 40. 1211 461 61.5

INDUSTRIAL AND ENGINEERING CHEMISTRY

January 1948

Figure 1.

Primary and Secondaty Sedimentation in a Single Clarifier

An intercompart,ment sludge scd, designhted llarnis sliidge s e d , lias bcen introduced for gene with Dorr 1m.v thickeners of the washing type. seal, one for each compartment of a multitray ing thickener, permits sludge to pms readily f n mnpurtmont to t,he iioxt for countercurrent wi brit completcly picvents tire p ~ ~ a of g asolution. forrncrly sometimes occurred. The result is a at or close to final density, .s greater displa( oEi:ienc.y, and a high degree of washing per c wnsh water. During the last year, lnrgc center-drive diuge 1,liickencrs of t,he center-column typo iiielodcd a new ailtonistie raising feature, as in the diagrammatic drawing of Figure 5. davicc is now included on ibicktiners manufa iiy this company in sizes from 100 feet in di, upxwd. The internal main spur gear is SUF on 1m11 bcarings at tho peripliery, and on mounted four sloping drive brackets which and drive rollers attached to the top of tho tobe, Jhring normal opcral.ion the weight mechanism is inore than suffieicnt to overem lifting effect of the sloping drive braoketa. ever, when tho torque increases 1.0 predete loading, the rollers st,& moving up the i bracket, raising the completc mechnnism. Ar

An iinprmwi I h r r i.laiilier (1:igure 3). type 5-7, provides additional s!n:ngtii i l i i t i rugged~!ss for sizes rmging from 30 t,a 100 i c r t in ditnneter. A eylindrimri central c i h m n uf stcvl eiiininates the conical-based conemtc pier mod in sinalliir units. Trussed-frame rake arms, providing wider support for rake blades, give greatcr strirctural rigidity and oliminnte tie rods and single bracing. 1,ongrr rake blades throughout t,he entire Ieng!.h of rakc arms result. in ferrer blades bcing required and Icssen tho c h a m ai sludgc bridang between blades. A skcl cage frame, supporting the arms, simplifies erection. The motor drive unit is stronger and simplor in consbroct.ion then pieviuus models and iu providcd with a doublc ovcrload protection. An improved Dorr hydroseparator (Figure 4 ) . t,ypr If, has bcen dcrelopcd for liaridling large volumcs of c,owse, grarrular solids such BS phosplinte rock. Units mngc in size from 50 to 100 feet in d i a m e k , capable of handling 100 to 1000 tons of solids per hour. 'f'ho distinctive feature is a n automatic hydraulic lifting device which raises the rakes rapidly 3 fcet in the event of a scrious ovdwad and tlicn l o m r s them slowly inio normnl pa& tion when tho overload has been mduced. The bdnncod spur gear drive is of the heavy-duty type.

-WALKWAY

rHANDkAlL

.a EFFLUEP

I

..-..N OUTLET PORTS CENTER COLUMN /RAKE ARM ~

52

INDUSTRIAL AND ENGINEERING CHEMISTRY

DRIVE TUBE RAKE ARMS

Figure 4,

Dorr Type

H Hydroseparator

Vol. 40, No. 1 been introduced for sevcral years. Existing designs have been modified and improved in minor respects, but these are not regarded a s being of sufficient importance t o warrant discussion of this article. It may, however, be said that The Dorr Company is in the final stages of developing a new classifier model that will probably be announccd publicly a year or so henrc. This development, based 011 the utilizat,ion of new and novel mechanical principles for achieving the desired rake motion. aims at a general over-all betterment in classificat,ion practice.

Diameter, 50-1 00 feet; extra-heavy construction; equipped with an automatic, hydraulic lilting device to deal with sudden overloads. BIBLIOGRAPHY

A survey of the literature for the last tivo years shows only a few references t o sedimentation and classification warranting mention in this review by reason of novelty, size, or other characteristic.