Spectrometric Determination of Rhenium and Its Separation from

24, 1997 (1952). (2) Corbridge, D. E. C., and Lowe, E. J., J. Chem. Soc., 1954, 493. 73) Ibid., p. 4555. (4) Crowther, J., Anal. Chem., 26,1383 (1954)...
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V O L U M E 2 7 , NO. 9, S E P T E M B E R 1 9 5 5 Geiger counter x-ray techniques ( 7 ) applied to the anslysis of commercial triphosphate are quicker and more sensitive than photographic methods ( I O ) , but the infrared method appears to be a t least as rapid and as accurate. ACKNOWLEDGWEYT

The authors thank J. T . Dixon for assistance in recording some of the spectra. LITERATURE CITED

(1) Bell, R. X.. Wreath, A. R., and Curless, 15'. T., - 4 ~ 4 CHEY., ~ . 24, 1997 (1952). (2) Corbridge, D. E. C., and Lowe, E. J., J . Chem. Soc., 1954, 493. (3) Ibid., p. 4555.

1387 (4) Crowther, J., ANAL.CHEX.,26, 1383 (1954). (51 Ford. 31. A.. and Wilkinson. C. R.. J . Sci. Instr., 31, 338 (1954).