Synthesis and neuroleptic activity of isomeric thieno [1, 4

Aug 1, 1975 - J. Med. Chem. , 1975, 18 (8), pp 857–861. DOI: 10.1021/jm00242a023. Publication Date: August 1975. ACS Legacy Archive. Note: In lieu o...
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Journal of Medicinal Chemistry, 1975, Vol. 18, No. 8 857

Notes solid was filtered, washed with EtOAc-Me2CO (9:1), and dried to give 64.4 g (38%)of 9: mp 151-156.5'. Recrystallization from methyl isobutyl ketone gave 55.7 g (33%) of essentially pure 9, mp 159.5-161'; rods from i-PrOH, mp 160-