Synthesis of Nortriptyline and Related Compounds

of piperidine at 90-100° for 15 hr. and recrystallization of the product from ethyl acetate; *?„0 276 m#t(e 10,200); analysis calculated for 0.25 H...
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u Prcpared by hydrogenation of 500 rng. of \-I \vi 0 nig. of SI ~ ~ : ~ l l : ~ ~ l i i ~ ~ i iii i - :Llisiiliite o ~ ~ - ~ ~ethiinol ~ ~ ~ l i :it ~ i 1 r ~atrn. for 4.2; 111.. :IIII~ recrystallization of the product frc~nibenzene; nip ( 6 21,!100). 2x2 ( l O , i O O ) , :G!)( I:;,OOOj, insharp contrast to niothyl 5-:~niin1i280 nip ( E 5400), 3 1 indole-3-propionate (see ref. l a ) , which had Af:;'" 400). h Prepared b y 1)ocIbner (see I