UNITED STATES TESTING COMPANY, INC

Chemical Co. and at present with. Baird-Atomic ... Several other applications of emission spectroscopy were ... testing, research, product design, and...
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NEWS A.) also offer possibilities for nonmetallic element studies. A third area of improvement relates to developing instruments and methods for increasing conoentrational sensi­ tivity of spectrochemical analysis. Typical examples include the carrierdistillation method, utilization of vapor pressure differential of metallic ele­ ments when melted in vacuum furnaces, collection of sample fractions on elec­ trodes, ion exchange, chromatographic, electrochemical, and zone refining methods. A fourth area of improvement would increase accuracy of analysis by means other than improving sample quality. A fifth area involves computations. With more than two elements present in a sample, interelement effects occur, and as wider and wider concentration ranges are covered, the need for com­ puters becomes greater. Another pioneer in the field of di­ rect-reading spectrometry, J. L. Saunderson, who worked originally with Dow Chemical Co. and at present with Baird-Atomic, discussed recent devel­ opments in direct-reading spectrom­ eters. Such improvements as rapid change­ over for different types of analyses, and simple and speedy adjustments have led to improved performance, reli­ ability, and ease of operation. In­ creased flexibility has expanded the scope of work possible. A new approach to signal-measuring techniques, reported by Frederick Brech, Jarrell-Ash Co., involves con­ version of the signal from photomultiplier transducers into pulses, the inte­ grated number of which is a direct measure of the signal strength. Inte­ gration is achieved through use of a pulse-actuated motor responding to pulses at any rate up to 400 cycles per second. Precision and stability are at­ tained through this means, he said. Work done in the automatic record­ ing and computation of spectrochemical data at the National Bureau of Stand­ ards was outlined by B. F. Scribner. The spectrometer output is fed to a digital electronic storage and read into an IBM card. Intensity measurements on 18 elements are recorded in 10 sec­ onds after the exposure is completed. Advantages of high-speed electronic read-out systems are reduced transcrip­ tion errors and increased speed. NBS has applied this system to studies of homogeneity of alloys. Several other applications of emission spectroscopy were outlined at the sym­ posium. A pioneering application re­ lates to a study on the concentration of metals in human tissues. As many as 14 different tissues are analyzed for 13

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