Wednesday Morning

Optical and X-ray Spectros- copy—Past, Present, and Future. ... Umea. Elimination of Background Cor- rection Errors. J. M. Harnly, J. A.. Holcombe, ...
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News Trace Element Analysis of Geo­ logical Materials by Direct Inser­ tion of Graphite Cups into an ICP. A. Lorber, Z. Goldbart Determination of Wear Metals in Oil by Electrothermal Vaporiza­ tion-Plasma Emission Spectrom­ etry. T. J. Hook, J. A. Caruso, SUNY at Buffalo Vaporized Sample Introduction to the ICP for the Analysis of Semi­ conductor Materials. S. J. Evans, D. R. Demers, Baird Corp. Application of Glow DischargeOptical Emission Spectroscopy to Routine Foundry Alloys. R. R. Com­ tois, Vhg Labs Inc.; P. P. Bradley, Arrowhead Metals Ltd. Electrochemical Preconcentration for Simultaneous Multiele­ ment Determination by ICP-AES with Electrothermal Vaporization. H. K. Matusiewicz, F. L. Fricke, U.S. Food and Drug Administration Enrichment of Trace Elements for Inductively Coupled Plasma Spectrometry with a Polyurea Polyamino Aeetic-Polyiminodiacetic Acid (PPA) Chelating Resin. Cs. Horvath, R. M. Barnes, U of Massa­ chusetts Determination of Copper in White Cast Iron by Direct Current Plasma Atomic Emission Spectrom­ etry. Ν. Μ. Potter, General Motors Research Laboratories Determination of Oxygen, Hy­ drogen, and Carbon in Nitrogen Gas by Helium Microwave Plasma Emission Spectrometry. S. Hanamura, W.-J. Wang, J. D. Winefordner, U of Florida Simultaneous Background Cor­ rection for Graphite Furnace-Inductively Coupled Plasma. C. C. Wohlers, D. R. Hull, R. G. Schleicher, Allied Analytical Systems Atomic Emission Spectroscopy and the Pharmaceutical Industry. R. M. Kinsey, Beckman Instruments, Inc. Determination of Ρ and Β in Steel Alloys by ICP-AES Utilizing Air Path Wavelengths. J. P. McCar­ thy, Ε. Β. Nunn, Monsanto Research Corp. Study of Analyte Emission Sig­ nals in Flame Spectrometry by Aerosol Modulation. C. B. Boss, M. Pearce, North Carolina State U Analysis of Trace Impurities in Gold Bullion by Plasma Emission Spectrometry. C. J. Flora, S. R. Maggs, J. R. Eldridge, Inco Ltd. Program in BASIC for Quantita­ tive Optical Atomic Emission Spec­ trograph^. J. B. Zink, U.S. Bureau of Mines

Elemental Analysis of Organic Microsamples Using Microwave Plasma Induced Atomic Emission. D. B. Hooker, J. Dezwaan, Upjohn Co.

Wednesday Morning Anachem Award Symposium

Arranged by D. Buchanan Award Address. F. W. McLafferty, Cornell U Utility of MS/MS for the Study of Radical Isomerizations. C. N. McEwen, Du Pont Digital Controlled Mass Spec­ trometry, the Past and Future. J. Michnowicz, Hewlett Packard Sci­ entific Title Not Available. R. B. Cody, Nicolet Instrument Co. Liquids, Ions, and Langmuir. W. V. Ligon, General Electric Co. Atomic Absorption Spectroscopy

Présider: S. R. Koirtyohann Summary of Renewing Events in Optical Spectroscopy. S. R. Koirtyohann, U of Missouri Businessman's View of the Development of Analytical Atomic Spectroscopy. R. E. Reiss, ESA Laboratories Optical and X-ray Spectroscopy—Past, Present, and Future. F. Brech Impact of Selected Discoveries in Analytical Atomic Spectroscopy. W. Slavin, Perkin-Elmer Furnace Atomization Information by Real-Time Atmospheric Pressure Sampling Mass Spectrometry. D. L. Styris, Pacific Northwest Laboratories Theoretical and Experimental Study of Carbide Formation in Graphite Furnace AAS. A. Cedergren, E. Lundberg, W. Freeh, U of Umeâ Elimination of Background Correction Errors. J. M. Harnly, J. A. Holcombe, USDA, NCL

Comparison of Analytical Figures of Merit of Conventional Pneumatic Ultrasonic and Direct Injection Nebulization for Sample Introduction into ICPs. Κ. Ε. Law­ rence, V. A. Fassel, Ames LaboratoryIowa State U; G. W. Rice, College of William and Mary Characterization and Applica­ tions of a Recycling Nebulizer Sys­ tem for Inductively Coupled Plas­ ma Spectrometry. C. Zicai, R. M. Barnes, U of Massachusetts Recent Developments in Sample Introduction for Ultratrace Analy­ sis by ICP-AES. J. E. Goulter, D. B. Tasker, M. W. Tikkanen, M. W. Routh, Applied Research Laboratories Preconcentration Methods for FIA Atomic Spectrometry. G. Chris­ tian, U of Washington Interfacing Liquid Chromatog­ raphy with Inductively Coupled Plasma-AES: Fundamental Consid­ erations. R. F. Browner, A. J. Faske, Georgia Institute of Technology Monodisperse Aerosol Genera­ tion Interface for Combining Liq­ uid Chromatography with ICP Spectrometry (MAGIC-LC/ICP). A. J. Faske, R. F. Browner, Georgia Institute of Technology Simultaneous, Multielement Analysis of HPLC Effluents Using the Direct Injection Nebulizer with Subsequent ICP-AES Detection. Κ. Ε. Lafreniere, V. A. Fassel, Iowa

State U Analytical Applications of NMR

Arranged by H. C. Dorn Magic-Angle Spinning in the Analysis of Surfaces. G. E. Maciel, Colorado State U Flow NMR Applications in Chemical Analysis. C. L. Wilkins, U of California Two-Dimensional NMR of Glycopeptide Antibiotics. S. L. Heald, L. Mueller, P. W. Jeffs, Smith Kline & French Laboratories One- and Two-Dimensional 1 3 CNMR Studies of Polymers. M. W. Crowther, G. C. Levy, Syracuse U Chemometrics

Advances in Plasma Spectrometry— Sample Introduction

Arranged by A. Montaser and D. W. Golightly In Search of the "Perfect" Aerosol for ICP Emission Spectroscopy. J. R. Miller, R. F. Browner, Georgia Institute of Technology

910 A · ANALYTICAL CHEMISTRY, VOL. 57, NO. 8, JULY 1985

Arranged by D. Honigs Sequential Simplex Optimization in Chemistry. S. Deming, U of Hous­ ton Kalman Filter in Dynamic Sys­ tems. S. D. Brown, Washington State U; S. C. Rutan, Virginia Common­ wealth U

News Analysis of the Effects of Errors in Measuring Absorbance and Time on the Calculated Value of a Pseudo-First-Order Rate Constant. E. D. Johnson, J. P . Weber, L. Meites, George Mason U Theory of the Distribution of Error Eigenvalues Resulting from Factor Analysis with Applications to Chemical Data. E. R. Malinowski, Stevens Institute of Technology Modified Factor Analysis Spectral Resolution Algorithm. S. L. Neal, I. M. Warner, Emory U Use of Factor Analysis and HPLC to Study Chemical Equilibrium—Reactions between Amino Acids and Alkaline. M. D'Amboise, D. Noel, U of Montreal

Applications of Spectroscopic Analysis of Polypropylene Orientation Using Internal Reflection Spectroscopy. F. M. Mirabella, Northern Petrochemical Co. Dynamic Infrared Linear Dichroism of Biopolymèrs and Amorphous Polymers. I. Noda, A. E. Dowrey, C. Marcott, Procter & Gamble Co. Segmental Orientation Studies of Isotopically Labeled Triblock Copolymers Using Polarization Modulated Infrared Dichroism. J. T. Koberstein, B. Lawrey, R. K. Prudhomme, Princeton U Quantitative Infrared Spectroscopic Analysis of Thin Organic Films on Nonmetallic Surfaces. M. D. Porter, D. L. Allara, Bell Communication Research Fourier Transform-IR Studies of Chain Scission in Polymers. B. Fanconi, National Bureau of Standards

Vibrational Spectroscopy for the Analysis of Polymers and Thin Films

Arranged by F. M. Mirabella Internal and External Reflection Spectra of Biological Thin Films. R. J. Jakobsen, R. A. Dluhy, Battelle—Columbus Labs Molecular Interpretation of Macroscopic Properties in Heterophase Polymers. S. L. Hsu, L. D. Coyne, U of Massachusetts

Liquid Chromatography— Pharmaceutical and Clinical Applications

Decanoate in Haldol Decanoate-Injectable Solutions. C. Y. Ko, McNeil Pharmaceutical Enantiomeric Resolution of 2Tetradecylglycidic Acid Esters and Other Fatty Acid Esters on HPLC Chiral Stationary Phases. L. E. Weaner, D. C. Hoerr, McNeil Pharmaceutical Determination of Vitamin Ε in Liquid Nutritional Products by Nonaqueous Reversed-Phase HPLC. T. M. Jones, Mead Johnson & Co. Identification of Cephalosporin Degradation Procedures by HPLC/ MS. D. Humphrey, J. James, A. O'Campo, J. Baldini, M. Siegel, American Cyanamid Separation of Halogenated Nico­ tine Acids by HPLC with Electro­ chemical Detector. A. U. Shaikh, F. L. Setliff, U of Arkansas Trace Analysis in Physiological Fluids Using Microbore HPLC and On-Line Preconcentration. M. J. Koenigbauer, R. C. Willoughby, S. P . Assenza, M. A. Curtis, Stuart Pharma­ ceuticals

Simultaneous Determination of Benzyl Alcohol and Haloperidol

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CIRCLE 32 ON READER SERVICE CARD ANALYTICAL CHEMISTRY, VOL. 57, NO. 8, JULY 1985 · 911 A

News Newly Observed Urinary Meta­ bolites of Thyroid Hormones: I. Solid-State Extraction Methods Used for Isolation and Character­ ization. II. Purification for Mass Spectral Analysis Achieved by Use of a Bonded Phenyl Phase after HPLC Separation on ReversedPhase Cig. J. T. Gordon, M. B. Dratman, VA Medical Center Determination of Cimetidine in Whole Blood and Plasma by Rapid Reversed-Phase High-Performance Liquid Chromatography. A. M. Rustum, N. E. Hoffman, T. Wehr, Marquette U Absorption: A New Technique in Treating Diseases of Plants, Ani­ mals, and Humans. R. C. Crippen, Crippen Laboratories, Inc.

Studies. L. P. Hart, B. W. Smith, N. Omenetto, ISPRA Laser-Excited Atomic Fluores­ cence in a Graphite Furnace. D. Goforth, J. D. Winefordner, U of Flor­ ida Laser-Excited Atomic Fluores­ cence in a Carbon Tube Furnace. M. D. Seltzer, J. P. Dougherty, R. G. Michel, U of Connecticut Zeeman Background Correction for Laser-Excited Atomic Fluores­ cence in a Carbon Furnace. J. P. Dougherty, M. D. Seltzer, R. G. Mi­ chel, U of Connecticut Plasma Spectroscopy—Sample Introduction

Near-Infrared Qualitative Anal­ ysis. H. Mark, Technicon Instruments Corp. Pattern Recognition Studies in Chemical Communication. Β. Κ. Lavine, P. C. Jurs, Pennsylvania State U Chemometrics and Process Ana­ lytical Chemistry. D. Honigs, U of Washington Diffuse Reflectance FT-IR Stud­ ies at Elevated Temperatures. K. Krishnan, S. Hill, Bio-Rad, Digilab Division Statistical Practices for Spectrophotometric Calibrations. P. J. Coo­ per, Pacific Scientific Co. Vibrational Spectroscopy for the Analysis of Polymers and Thin Films

Arranged by J. A. Caruso

Wednesday Afternoon Anachem Award Symposium Arranged by D. N. Buchanan Applications of Fast Atom Bombardment. L. Baczynskyj, Upjohn Co. Structure Analysis of Bioactive Molecules Using Soft Ionization and MS/MS Methods. S. A. Carr, Smith Kline & French Labs High-Pressure Collisional Activation Mass Spectrometry. B. Munson, U of Delaware Title Not Available. M. V. Buchanan, Oak Ridge National Laboratory Title Not Available. A. J. DeStefano, Norwich-Eaton Pharmaceutical Title Not Available. W. Benz, Hoffmann-La Roche Atomic Fluorescence Spectrometry Spectral Interferences, Matrix Effects, and Improved Detection Limits in ICP-Excited-ICP Atomic Fluorescence Spectrometry. R. J. Krupa, G. L. Long, J. D. Winefordner, U of Florida Laser-Excited Fluorescence of Diatomic Molecules of Copper and Lead in a Glow Discharge Sputter­ ing Source. B. Patel, J. D. Wine­ fordner, U of Florida Fluorescence and Ionization Studies in Flames and Plasma by Dual Wavelength Laser Excitation. B. W. Smith, L. P. Hart, N. Omenetto, ISPRA Laser-Excited Fluorescence of Argon in an Inductively Coupled Plasma as a Tool for Diagnostic

Alternatives to the Nebulizer in ICP Analysis. M. A. Sainz, J. S. Beaty, S. B. Smith, R. J. Bellmore, Al­ lied Analytical Systems Direct Introduction of Powder Samples in Inductively Coupled Plasma Emission Spectroscopy. K. N. Desilva, R. Guevremont, Na­ tional Research Council Slurry Injection dc Plasma Anal­ ysis of Coal. V. C. Anigbogu, G. N. Coleman, U of Alabama Organic Solvent Introduction into a Free-Running Cavity-Oscil­ lator Inductively Coupled Plasma. P. G. Brown, B. S. Burnes, J. A. Caru­ so, U of Cincinnati Aluminum Speciation by LC-ICP with a Fritted Nebulizer Interface. J. A. Koropchak, D. H. Winn, South­ ern Illinois U Flow-Injection Hydride Genera­ tion Analyses with the dc Plasma Jet. V. C. Anigbogu, G. N. Coleman, U of Alabama Multielement Determination by Plasma Emission Spectroscopy with Electrothermal Vaporization Sample Introduction. P. Pfannerstill, J. A. Caruso, U of Cincinnati Multielement Analysis of Waters and Wastes by Electrothermal Volatilization into an ICP Emission Spectrometer. D. A. Leighty, D. D. Nygaard, D. R. Hull, R. G. Schleicher, Allied Analytical Systems

Arranged by F. M. Mirabella Infrared Characterization of Conductive Metal Oxide Films on Glass. R. O. Carter, Ford Motor Co. Optical Constants of Selected Polymers. E. G. Brame, B. V. Lockshin, V. A. Yakovlev, G. N. Zhizhin, Institutes of Spectroscopy and Organo-Element Compounds of the U.S.S.R. Academy of Sciences Current Developments and Ap­ plications of FT-IR/ATR and PAS Dichroism or Polymer Surface Characterization. C. S. P. Sung, J. P. Hobbs, U of Connecticut Applications of Photoacoustic and Attenuated Total Reflection Spectroscopies to Polymer Sur­ faces. J. A. Graham, Hercules Inc. Characterization of Highly Drawn Polypropylene Films. F. M. Mirabella, Northern Petrochemical Co. Multiaxial Characterization of Oriented Polarized Infrared Spec­ troscopy. R. J. Samuels, Georgia In­ stitute of Technology FT-IR Studies of Molecular De­ formation Mechanisms. R. P. Wool, U of Illinois Raman Scattering in Submicron Polymer Films at Cryogenic Tem­ peratures Using Integrated Optical Techniques. J. F. Rabolt, IBM Re­ search Laboratory

Chemometrics

Separation of Blomolecules: State of the Art

Arranged by D. Honigs

Arranged by J. Dibussolo

Spectral Compound Identifica­ tion—Qualitative Chemometrics? M. F. Delaney, J. R. Hallowell, D. M. Mauro, F. V. Warren, S. F. Rhode, Boston U

Benchmarking Size-Exclusion Chromatography for Biopolymer Separations. F. E. Régnier, Purdue U; E. Pfannkock, W. R. Grace & Co.

912 A · ANALYTICAL CHEMISTRY, VOL. 57, NO. 8, JULY 1985