News Trace Element Analysis of Geo logical Materials by Direct Inser tion of Graphite Cups into an ICP. A. Lorber, Z. Goldbart Determination of Wear Metals in Oil by Electrothermal Vaporiza tion-Plasma Emission Spectrom etry. T. J. Hook, J. A. Caruso, SUNY at Buffalo Vaporized Sample Introduction to the ICP for the Analysis of Semi conductor Materials. S. J. Evans, D. R. Demers, Baird Corp. Application of Glow DischargeOptical Emission Spectroscopy to Routine Foundry Alloys. R. R. Com tois, Vhg Labs Inc.; P. P. Bradley, Arrowhead Metals Ltd. Electrochemical Preconcentration for Simultaneous Multiele ment Determination by ICP-AES with Electrothermal Vaporization. H. K. Matusiewicz, F. L. Fricke, U.S. Food and Drug Administration Enrichment of Trace Elements for Inductively Coupled Plasma Spectrometry with a Polyurea Polyamino Aeetic-Polyiminodiacetic Acid (PPA) Chelating Resin. Cs. Horvath, R. M. Barnes, U of Massa chusetts Determination of Copper in White Cast Iron by Direct Current Plasma Atomic Emission Spectrom etry. Ν. Μ. Potter, General Motors Research Laboratories Determination of Oxygen, Hy drogen, and Carbon in Nitrogen Gas by Helium Microwave Plasma Emission Spectrometry. S. Hanamura, W.-J. Wang, J. D. Winefordner, U of Florida Simultaneous Background Cor rection for Graphite Furnace-Inductively Coupled Plasma. C. C. Wohlers, D. R. Hull, R. G. Schleicher, Allied Analytical Systems Atomic Emission Spectroscopy and the Pharmaceutical Industry. R. M. Kinsey, Beckman Instruments, Inc. Determination of Ρ and Β in Steel Alloys by ICP-AES Utilizing Air Path Wavelengths. J. P. McCar thy, Ε. Β. Nunn, Monsanto Research Corp. Study of Analyte Emission Sig nals in Flame Spectrometry by Aerosol Modulation. C. B. Boss, M. Pearce, North Carolina State U Analysis of Trace Impurities in Gold Bullion by Plasma Emission Spectrometry. C. J. Flora, S. R. Maggs, J. R. Eldridge, Inco Ltd. Program in BASIC for Quantita tive Optical Atomic Emission Spec trograph^. J. B. Zink, U.S. Bureau of Mines
Elemental Analysis of Organic Microsamples Using Microwave Plasma Induced Atomic Emission. D. B. Hooker, J. Dezwaan, Upjohn Co.
Wednesday Morning Anachem Award Symposium
Arranged by D. Buchanan Award Address. F. W. McLafferty, Cornell U Utility of MS/MS for the Study of Radical Isomerizations. C. N. McEwen, Du Pont Digital Controlled Mass Spec trometry, the Past and Future. J. Michnowicz, Hewlett Packard Sci entific Title Not Available. R. B. Cody, Nicolet Instrument Co. Liquids, Ions, and Langmuir. W. V. Ligon, General Electric Co. Atomic Absorption Spectroscopy
Présider: S. R. Koirtyohann Summary of Renewing Events in Optical Spectroscopy. S. R. Koirtyohann, U of Missouri Businessman's View of the Development of Analytical Atomic Spectroscopy. R. E. Reiss, ESA Laboratories Optical and X-ray Spectroscopy—Past, Present, and Future. F. Brech Impact of Selected Discoveries in Analytical Atomic Spectroscopy. W. Slavin, Perkin-Elmer Furnace Atomization Information by Real-Time Atmospheric Pressure Sampling Mass Spectrometry. D. L. Styris, Pacific Northwest Laboratories Theoretical and Experimental Study of Carbide Formation in Graphite Furnace AAS. A. Cedergren, E. Lundberg, W. Freeh, U of Umeâ Elimination of Background Correction Errors. J. M. Harnly, J. A. Holcombe, USDA, NCL
Comparison of Analytical Figures of Merit of Conventional Pneumatic Ultrasonic and Direct Injection Nebulization for Sample Introduction into ICPs. Κ. Ε. Law rence, V. A. Fassel, Ames LaboratoryIowa State U; G. W. Rice, College of William and Mary Characterization and Applica tions of a Recycling Nebulizer Sys tem for Inductively Coupled Plas ma Spectrometry. C. Zicai, R. M. Barnes, U of Massachusetts Recent Developments in Sample Introduction for Ultratrace Analy sis by ICP-AES. J. E. Goulter, D. B. Tasker, M. W. Tikkanen, M. W. Routh, Applied Research Laboratories Preconcentration Methods for FIA Atomic Spectrometry. G. Chris tian, U of Washington Interfacing Liquid Chromatog raphy with Inductively Coupled Plasma-AES: Fundamental Consid erations. R. F. Browner, A. J. Faske, Georgia Institute of Technology Monodisperse Aerosol Genera tion Interface for Combining Liq uid Chromatography with ICP Spectrometry (MAGIC-LC/ICP). A. J. Faske, R. F. Browner, Georgia Institute of Technology Simultaneous, Multielement Analysis of HPLC Effluents Using the Direct Injection Nebulizer with Subsequent ICP-AES Detection. Κ. Ε. Lafreniere, V. A. Fassel, Iowa
State U Analytical Applications of NMR
Arranged by H. C. Dorn Magic-Angle Spinning in the Analysis of Surfaces. G. E. Maciel, Colorado State U Flow NMR Applications in Chemical Analysis. C. L. Wilkins, U of California Two-Dimensional NMR of Glycopeptide Antibiotics. S. L. Heald, L. Mueller, P. W. Jeffs, Smith Kline & French Laboratories One- and Two-Dimensional 1 3 CNMR Studies of Polymers. M. W. Crowther, G. C. Levy, Syracuse U Chemometrics
Advances in Plasma Spectrometry— Sample Introduction
Arranged by A. Montaser and D. W. Golightly In Search of the "Perfect" Aerosol for ICP Emission Spectroscopy. J. R. Miller, R. F. Browner, Georgia Institute of Technology
910 A · ANALYTICAL CHEMISTRY, VOL. 57, NO. 8, JULY 1985
Arranged by D. Honigs Sequential Simplex Optimization in Chemistry. S. Deming, U of Hous ton Kalman Filter in Dynamic Sys tems. S. D. Brown, Washington State U; S. C. Rutan, Virginia Common wealth U
News Analysis of the Effects of Errors in Measuring Absorbance and Time on the Calculated Value of a Pseudo-First-Order Rate Constant. E. D. Johnson, J. P . Weber, L. Meites, George Mason U Theory of the Distribution of Error Eigenvalues Resulting from Factor Analysis with Applications to Chemical Data. E. R. Malinowski, Stevens Institute of Technology Modified Factor Analysis Spectral Resolution Algorithm. S. L. Neal, I. M. Warner, Emory U Use of Factor Analysis and HPLC to Study Chemical Equilibrium—Reactions between Amino Acids and Alkaline. M. D'Amboise, D. Noel, U of Montreal
Applications of Spectroscopic Analysis of Polypropylene Orientation Using Internal Reflection Spectroscopy. F. M. Mirabella, Northern Petrochemical Co. Dynamic Infrared Linear Dichroism of Biopolymèrs and Amorphous Polymers. I. Noda, A. E. Dowrey, C. Marcott, Procter & Gamble Co. Segmental Orientation Studies of Isotopically Labeled Triblock Copolymers Using Polarization Modulated Infrared Dichroism. J. T. Koberstein, B. Lawrey, R. K. Prudhomme, Princeton U Quantitative Infrared Spectroscopic Analysis of Thin Organic Films on Nonmetallic Surfaces. M. D. Porter, D. L. Allara, Bell Communication Research Fourier Transform-IR Studies of Chain Scission in Polymers. B. Fanconi, National Bureau of Standards
Vibrational Spectroscopy for the Analysis of Polymers and Thin Films
Arranged by F. M. Mirabella Internal and External Reflection Spectra of Biological Thin Films. R. J. Jakobsen, R. A. Dluhy, Battelle—Columbus Labs Molecular Interpretation of Macroscopic Properties in Heterophase Polymers. S. L. Hsu, L. D. Coyne, U of Massachusetts
Liquid Chromatography— Pharmaceutical and Clinical Applications
Decanoate in Haldol Decanoate-Injectable Solutions. C. Y. Ko, McNeil Pharmaceutical Enantiomeric Resolution of 2Tetradecylglycidic Acid Esters and Other Fatty Acid Esters on HPLC Chiral Stationary Phases. L. E. Weaner, D. C. Hoerr, McNeil Pharmaceutical Determination of Vitamin Ε in Liquid Nutritional Products by Nonaqueous Reversed-Phase HPLC. T. M. Jones, Mead Johnson & Co. Identification of Cephalosporin Degradation Procedures by HPLC/ MS. D. Humphrey, J. James, A. O'Campo, J. Baldini, M. Siegel, American Cyanamid Separation of Halogenated Nico tine Acids by HPLC with Electro chemical Detector. A. U. Shaikh, F. L. Setliff, U of Arkansas Trace Analysis in Physiological Fluids Using Microbore HPLC and On-Line Preconcentration. M. J. Koenigbauer, R. C. Willoughby, S. P . Assenza, M. A. Curtis, Stuart Pharma ceuticals
Simultaneous Determination of Benzyl Alcohol and Haloperidol
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CIRCLE 32 ON READER SERVICE CARD ANALYTICAL CHEMISTRY, VOL. 57, NO. 8, JULY 1985 · 911 A
News Newly Observed Urinary Meta bolites of Thyroid Hormones: I. Solid-State Extraction Methods Used for Isolation and Character ization. II. Purification for Mass Spectral Analysis Achieved by Use of a Bonded Phenyl Phase after HPLC Separation on ReversedPhase Cig. J. T. Gordon, M. B. Dratman, VA Medical Center Determination of Cimetidine in Whole Blood and Plasma by Rapid Reversed-Phase High-Performance Liquid Chromatography. A. M. Rustum, N. E. Hoffman, T. Wehr, Marquette U Absorption: A New Technique in Treating Diseases of Plants, Ani mals, and Humans. R. C. Crippen, Crippen Laboratories, Inc.
Studies. L. P. Hart, B. W. Smith, N. Omenetto, ISPRA Laser-Excited Atomic Fluores cence in a Graphite Furnace. D. Goforth, J. D. Winefordner, U of Flor ida Laser-Excited Atomic Fluores cence in a Carbon Tube Furnace. M. D. Seltzer, J. P. Dougherty, R. G. Michel, U of Connecticut Zeeman Background Correction for Laser-Excited Atomic Fluores cence in a Carbon Furnace. J. P. Dougherty, M. D. Seltzer, R. G. Mi chel, U of Connecticut Plasma Spectroscopy—Sample Introduction
Near-Infrared Qualitative Anal ysis. H. Mark, Technicon Instruments Corp. Pattern Recognition Studies in Chemical Communication. Β. Κ. Lavine, P. C. Jurs, Pennsylvania State U Chemometrics and Process Ana lytical Chemistry. D. Honigs, U of Washington Diffuse Reflectance FT-IR Stud ies at Elevated Temperatures. K. Krishnan, S. Hill, Bio-Rad, Digilab Division Statistical Practices for Spectrophotometric Calibrations. P. J. Coo per, Pacific Scientific Co. Vibrational Spectroscopy for the Analysis of Polymers and Thin Films
Arranged by J. A. Caruso
Wednesday Afternoon Anachem Award Symposium Arranged by D. N. Buchanan Applications of Fast Atom Bombardment. L. Baczynskyj, Upjohn Co. Structure Analysis of Bioactive Molecules Using Soft Ionization and MS/MS Methods. S. A. Carr, Smith Kline & French Labs High-Pressure Collisional Activation Mass Spectrometry. B. Munson, U of Delaware Title Not Available. M. V. Buchanan, Oak Ridge National Laboratory Title Not Available. A. J. DeStefano, Norwich-Eaton Pharmaceutical Title Not Available. W. Benz, Hoffmann-La Roche Atomic Fluorescence Spectrometry Spectral Interferences, Matrix Effects, and Improved Detection Limits in ICP-Excited-ICP Atomic Fluorescence Spectrometry. R. J. Krupa, G. L. Long, J. D. Winefordner, U of Florida Laser-Excited Fluorescence of Diatomic Molecules of Copper and Lead in a Glow Discharge Sputter ing Source. B. Patel, J. D. Wine fordner, U of Florida Fluorescence and Ionization Studies in Flames and Plasma by Dual Wavelength Laser Excitation. B. W. Smith, L. P. Hart, N. Omenetto, ISPRA Laser-Excited Fluorescence of Argon in an Inductively Coupled Plasma as a Tool for Diagnostic
Alternatives to the Nebulizer in ICP Analysis. M. A. Sainz, J. S. Beaty, S. B. Smith, R. J. Bellmore, Al lied Analytical Systems Direct Introduction of Powder Samples in Inductively Coupled Plasma Emission Spectroscopy. K. N. Desilva, R. Guevremont, Na tional Research Council Slurry Injection dc Plasma Anal ysis of Coal. V. C. Anigbogu, G. N. Coleman, U of Alabama Organic Solvent Introduction into a Free-Running Cavity-Oscil lator Inductively Coupled Plasma. P. G. Brown, B. S. Burnes, J. A. Caru so, U of Cincinnati Aluminum Speciation by LC-ICP with a Fritted Nebulizer Interface. J. A. Koropchak, D. H. Winn, South ern Illinois U Flow-Injection Hydride Genera tion Analyses with the dc Plasma Jet. V. C. Anigbogu, G. N. Coleman, U of Alabama Multielement Determination by Plasma Emission Spectroscopy with Electrothermal Vaporization Sample Introduction. P. Pfannerstill, J. A. Caruso, U of Cincinnati Multielement Analysis of Waters and Wastes by Electrothermal Volatilization into an ICP Emission Spectrometer. D. A. Leighty, D. D. Nygaard, D. R. Hull, R. G. Schleicher, Allied Analytical Systems
Arranged by F. M. Mirabella Infrared Characterization of Conductive Metal Oxide Films on Glass. R. O. Carter, Ford Motor Co. Optical Constants of Selected Polymers. E. G. Brame, B. V. Lockshin, V. A. Yakovlev, G. N. Zhizhin, Institutes of Spectroscopy and Organo-Element Compounds of the U.S.S.R. Academy of Sciences Current Developments and Ap plications of FT-IR/ATR and PAS Dichroism or Polymer Surface Characterization. C. S. P. Sung, J. P. Hobbs, U of Connecticut Applications of Photoacoustic and Attenuated Total Reflection Spectroscopies to Polymer Sur faces. J. A. Graham, Hercules Inc. Characterization of Highly Drawn Polypropylene Films. F. M. Mirabella, Northern Petrochemical Co. Multiaxial Characterization of Oriented Polarized Infrared Spec troscopy. R. J. Samuels, Georgia In stitute of Technology FT-IR Studies of Molecular De formation Mechanisms. R. P. Wool, U of Illinois Raman Scattering in Submicron Polymer Films at Cryogenic Tem peratures Using Integrated Optical Techniques. J. F. Rabolt, IBM Re search Laboratory
Chemometrics
Separation of Blomolecules: State of the Art
Arranged by D. Honigs
Arranged by J. Dibussolo
Spectral Compound Identifica tion—Qualitative Chemometrics? M. F. Delaney, J. R. Hallowell, D. M. Mauro, F. V. Warren, S. F. Rhode, Boston U
Benchmarking Size-Exclusion Chromatography for Biopolymer Separations. F. E. Régnier, Purdue U; E. Pfannkock, W. R. Grace & Co.
912 A · ANALYTICAL CHEMISTRY, VOL. 57, NO. 8, JULY 1985