ACS Fall National Meeting | Analytical Chemistry

News

ACS Fall National Meeting Kansas City, Mo., Sept. 1 2 - 1 7 , 1982 All technical sessions The 184th National sponsored by the Analytical Meeting of the American Division will be held in the Chemical Society will be Convention Center. The held in Kansas City, Mo., jointly sponsored symposia Sept. 12-17, 1982. At the on the chemistry of plutomeeting, the Division of nium, the applications of Analytical Chemistry will stable isotopes, and new sponsor or jointly sponsor physical methods in meditechnical sessions and cal chemical research will symposia at which over 250 take place in the Hyatt Retechnical presentations are gency. The symposium on scheduled. In addition to archaeological chemistry the extensive technical will meet in the Holiday program, the meeting will Inn—Center City. All other feature a National Emjointly sponsored symposia ployment Clearing House, will be held in the Conven24 ACS short courses, and tion Center. meetings of the ACS council The Analytical Chemisand board of directors. A try Division dinner is number of social events are scheduled for Tuesday, also planned, including an Sept. 14, at the Hyatt ReACS mixer, an Analytical Kansas City's J. C. Nichols Memorial Fountain gency. An ACS mixer is also Division dinner, a reception through Thursday, Sept. 16, from 8:00 planned for that Tuesday. A number sponsored by the ACS Corporate A.M. to 4:00 P.M. of local tours of Kansas City and plant Associates with remarks by ACS The following Analytical Division trips to Marion Laboratories, TWA, President Robert Parry, and tours and symposia are scheduled: molecular Midwest Research Institute, Mobay plant trips in Kansas City. interactions in chemical separations— Chemical Corporation, and the EPA An exposition of chemicals, solutes, solvents, and surfaces; organic Laboratories and Criminalistics instruments, services, and technical analysis; inorganic analysis; liquid Laboratories are also scheduled. For literature will be housed in North Hall chromatography; food analysis— more details and ticket information of Bartle Hall in the Kansas City contaminants; remote sensing of for social activities, see the June 28 Convention Center. For the first time, physical chemical parameters over and Aug. 2 issues of C & EN. the exposition will be open on Sunday optical fibers; validation of data at the The ACS Education Division will from 3:00 P.M. to 8:00 P.M. In addition, trace level; gas chromatography and offer a series of short courses at the the exposition will run on Monday, mass spectrometry; electrochemistry; Kansas City meeting. See the July Sept. 13, from 12:00 P.M. to 5:00 P.M. and general topics. issue of ANALYTICAL CHEMISTRY for and on Tuesday and Wednesday, courses of particular interest to Sept. 14 and 15, from 9:00 A.M. to 5:00 Symposia on the following topics analytical chemists. Further P.M. A series of workshops will be held are jointly sponsored by the Division information may be obtained from the in conjunction with the chemical of Analytical Chemistry and other Education Division, American exposition. Workshop titles, sponsors, ACS divisions: the chemistry of Chemical Society, 1155 16th St., N.W., and registration forms appear in the plutonium—a profile of development Washington, D.C. 20036, 202-872-4508. Aug. 2 issue of Chemical & and future directions; applications of Preregistration forms and Engineering News. stable isotopes; analytical chemistry of additional details about the meeting Registration facilities at the nuclear safeguards; archaeological are available in the June 28 and Aug. 2 meeting will be located on the lobby chemistry; chlorinated dioxins and issues of C & EN. The latter issue level of the Convention Center and in dibenzofurans in the total contains the complete final program the Century foyer of the Crown Center environment; identification and for the meeting. The program that Hotel. Registration will be held on analysis of organic pollutants in air; follows includes all sessions sponsored Sunday, Sept. 12, 3:00 P.M. to 8:00 image devices in spectroscopy; and or jointly sponsored by the ACS P.M.; Monday, Sept. 13, 7:00 A.M. to new physical methods in medical Division of Analytical Chemistry. 4:00 P.M.; and Tuesday, Sept. 14 chemical research. ANALYTICAL CHEMISTRY, VOL. 54, NO. 9, AUGUST 1982 · 1029 A

News DIVISION OF ANALYTICAL CHEMISTRY H. L. Pardue, Chairman R. F. Hirsch, Secretary

Monday Morning

11:00 Selection of Analytical Methods for Characterization of Com mercial Chemicals. R. D. Brown, E. A. Murrill, K. M. Stelting, E. J. Woodhouse, C. W. Jameson 11:20 Determination of Shale Oil Stability by Thermal Analysis. M. K. Young, M. J. Billig, D. C. Young, R. G. Ruberto 11:40 Rapid Compleximetric Pro cedure for Citric Acid by Titration with CuSO 4 . A. L. Wade

SECTION A

Symposium on Molecular Interactions in Chemical Separations: Solutes, Solvents, and Surfaces C. H. Lochmüller, Presiding 9:00 Experimental Observations on, and Theoretical Interpretation of, Mixed Solvent Action in HPLC. J. H. Purnell, C. A. Wellington, S. Madden, M. McCann 9:30 Molecular Interactions in Liquids. R. P. W. Scott, C. Reese 10:00 Molecular Theory of Reversed-Phase HPLC. D. E. Martire, R. E. Boehm 10:45 Geometric Effects in Liquid Chromatography with Hydrocarbonaceous Stationary Phases. W. R. Melander, C. Horvath 11:15 Mobility of Bonded Alkyl Moieties. R. K. Gilpin

SECTION Β

Symposium on Organic Analysis Topics R. E. Smith, Presiding 9:00 Polyethylene Glycol Quanti tation by Laser Nephelometry. S. C. Cole, G. Christensen, W. P. Olson 9:20 Determination of Diallyl Phthalate and Pendant Allyl Content in a Polydiallyl Phthalate Prepolymer. G. W. Griffith, C. L. Long, R. E. Smith 9:40 Determination of Reactive Components in a Silicone Prepolymer Blend. S. V. Dubiel, G. W. Griffith, C. L. Long, R. E. Smith 10:00 Angular Distribution XPS Studies on P b ISE Membranes. V. Young 10:40 Investigations of H 3 PO 4 :BF 3 as a Catalyst for the Protection of Hydroxyl-Bearing Compounds with Isobutylene. J. C. Weygandt, M. Pallmer

SECTION C

Symposium on the Chemistry of Plutonium—A Profile of Development and Future Directions. Joint with Division of Nuclear Chemistry and Technology W. T. Carnall and G. R. Choppin, Pre siding 9:00 Introductory Remarks. 9:05 Forty Years of Plutonium Chemistry. G. T. Seaborg 9:40 Review of Aspects of Pu So lution Chemistry. G. R. Choppin 10:15 X-ray Photoemission Spec troscopy (XPS) Study of Neptunium and Plutonium Oxides in SilicateBased Glasses. D. J . Lam, B. W. Veal 11:05 Plutonium Hexafluoride Gas Photophysics and Photochemis try. J. V. Beitz, C. W. Williams, W. T. Carnall 11:40 Photochemistry of Aqueous Plutonium Solutions. J. T. Bell, L. M. Toth, H. A. Friedman

Monday Afternoon SECTION A

Symposium on Molecular Interactions in Chemical Separations: Solutes, Solvents, and Surfaces R. P. W. Scott, Presiding 1:45 Steric Orientation of Bonded Functional Groups at the Silica Sur face and Its Effect on Solute Reten tion in HPLC. K. Unger 2:15 Silylation Chemistry. D. E. Williams 2:45 Magic-Angle Spinning NMR Studies at Surfaces. G. E. Maciel, D. W. Sindorf, M. R. Seger, I.-S. Chuang, M. P. Shatlock 3:30 Solute and Solvent Interac tion with Chemically Modified Silicas. C. H. Lochmüller, D. R. Wilder, A. Colburn, D. B. Marshall 4:00 Chiral Recognition Mechanisms Responsible for Chromatographic Separation of Enantiomers upon Chiral Stationary Phases. W. H. Pirkle, J. M. Finn, B. C. Hamper, M. H. Hyun, J. L. Schreiner, J. R. Pribish, T. J. Sowin, C. J. Welch SECTION Β

Symposium on Inorganic Analysis Topics

H. D. Anderson, Presiding 1:30 Complexation of Arsenic(III) and Arsenic(V) Species with Calcium(II) and Magnesium(II) Ions in Aqueous Solution. A. U. Shaikh, D. E. Tallman SECTION D 1:50 Investigation of the Acidity Symposium on the Applications of and Calcium Complexes of 1,1-DiStable Isotopes. Joint with Divisions of fluoro-methane-1,1-diphosphonic Acid. T. Fonong, D. J. Pietrzyk, D. J. Nuclear Chemistry and Technology Burton and Physical Chemistry 2:10 Investigation of a Nitrogen15 NMR Method for the Determina tion of Binding in Zinc(II) Complexes. R. H. Herber, Presiding B. P. Brammel, R. F. Evilia 9:45 Introductory Remarks. 2:30 Carbon-13 NMR Investiga 9:50 National Uses and Needs for tion of Amino Carboxylate Binding. Separated Stable Isotopes in Physics, R. F. Evilia Chemistry, and Geoscience Research. 3:10 Analysis of Titanium in M. S. Zisman Tissues by ICP Spectroscopy. J. M. 10:25 ORNL Stable Isotope En Cannon, L. L. Wyatt, R. D. Brown, E. richment Program. E. Newman A. Murrill, C. W. Jameson, M. P. 11:00 Utilization of Stable Iso Dieter topes in Nuclear Chemistry and Nu 3:30 Comparison of Minor and clear Physics Research. G. J. Trace Elements in Human Milk, Mar Wozniak ket Milk, and Commercial Infant For 11:35 Use of Separated Isotopes in mulas. H. D. Anderson, J. S. Morris, Analytical Chemistry. I. L. Barnes C. J. Kanatzar, C. L. Callahan

1030 A · ANALYTICAL CHEMISTRY, VOL. 54, NO. 9, AUGUST 1982

News 3:50 Evaluation of the Total Con sumption Burner for Laser-Enhanced Ionization Spectrometry. J. E. Gard ner, R. B. Green 4:10 Ash Cycle in Carbon Rod Atomization. J. M. Shekiro, Jr., R. K. Skogerboe 4:30 Analysis of Zircons by Induc tively Coupled Plasma Emission. N. Korte, M. Hollenbach, S. Donivan SECTION C Symposium on the Chemistry of Plutonium—A Profile of Development and Future Directions. Joint with Division of Nuclear Chemistry and Technology

J. Kim and L. Leibowitz, Presiding 2:00 Introductory Remarks. 2:05 Organometallic and Coordi nation Compounds of Plutonium: Synthesis and Magnetic Properties. B. Kanellakopulos 2:35 Reaction of Plutonium Metal with Diiodoethane. D. G. Karraker 2:55 Synthesis and Characteriza tion of Di(/i-hydroxo)-tetraaquadiplutonium(IV) Sulfate, Pu2(OH) 2 (S0 4 )3· 4H2O, and Its Relation to Other Actinide Hydroxysulfates. D. W. Wester 3:30 Thermodynamics of Plutoni um Halides and Halogeno Complexes in the Solid State and in Aqueous Media. J. Fuger 4:00 Superconductivity and Mag netism in Metallic Plutonium Sys tems. J. L. Smith, R. G. Haire, J. O. Willis 4:30 Thermodynamics of Pluto nium-Noble Metal Compounds. D. E. Petersen SECTION D Symposium on the Applications of Stable Isotopes. Joint with Divisions of Nuclear Chemistry and Technology and Physical Chemistry

M. S. Zisman, Presiding 2:00 Application of Stable Iso topes in Solid-State Science. R. H. Herber 2:35 Applications of Macroscopic Quantities of Separated Isotopes to Chemical Problems. G, R. Choppin 3:10 Applications of Stable Iso topes in Geoscience and Geochronology. D. J. DePaolo 3:55 Biomedical Research Appli cations of Electromagnetically Sepa rated Stable Isotopes. R. M. Lambrecht

4:30 NRC Workshop on Stable Isotopes and Derived Radioisotopes. G. Friedlander

Tuesday Morning SECTION A Symposium on Trends In Liquid Chromatography

J. G. Dorsey, Presiding 9:00 Multifarious Effects of In jected Solvents in Liquid Chromatog raphy. D. J. Miner, K. Z. Farid, R. J. Bopp 9:20 Comparison of Stationary Phases for the Separation of Charged Analytes by Ion Interaction Chroma tography. R. L. Smith, Z. Iskandarani, D. J. Pietrzyk 9:40 Effect of Ionic Strength on Retention in Reversed-Phase PairedIon HPLC. B. A. Bidlingmeyer, F. V. Warren, Jr. 10:00 Efficiency Enhancement in Micellar Liquid Chromatography: The Role of Temperature and Organic Modifiers. J. G. Dorsey, M. T. DeEchegaray 10:40 Investigations of Some NotSo-Common Reversed-Phase Solvent Systems; R. L. Lewis, J. Chazaud, T. F.May 11:00 How Molecules Are Dis solved in the Reverse Phase of Chemi cally Bonded Cis Reversed-Phase Packings for HPLC. J. B. Callis, S. L. Hansen 11:20 Pore-Size Effects in HighPerformance Affinity Chromatogra phy. R. R. Walters 11:40 HPLC Purity Analysis of Benzidine Congener-Based Dyes^ L. W. Pittmann, M. A. Lillich, Κ. Μ. Walters, E. A. Murrill, C. W. Jameson SECTION Β

Symposium on Food Analysis— Contaminants

C. E. Meloan, Presiding 8:00 Natural and Synthetic Repel lents To Prevent Cockroach Contami nation. C. E. Meloan, R. Scriven 8:20 Mass Spectral Identification of Chemical Residues Found in the Total Diet Program. D. L. Heikes 8:40 Improved Wet Digestion Sys tem for Determining Pb, Cu, Hg, As, and Se in Foods. R. Marts 9:00 Improved Slurry Atomization

Techniques for Rapid Trace Metal Analysis. R. C. Fry, M. D. Wichman, N. Mohamed, R. Fietkau 9:20 Automated Gel Permeation System for the Rapid Separation of Industrial Chemicals, Organophosphate, and Chlorinated Pesticides from Fats. M. L. Hopper 9:40 Simple Procedure for the Re moval of Interferences in the Analysis of Organophosphate Pesticide Resi dues from Vegetables. J. J. Blaha, M. L. Hopper 10:20 Workable HPLC Method for the Determination of Multiple Carbamate Residues in Foods. R. G. Luchtefeld 10:40 Measuring Fungal Contami nation in Foods. L. M. Seitz 11:00 Rapid Qualitative Method for the Detection of Monofluoroacetic Acid (1080) in Liquid Baits. E. McGary 11:40 Near-Infrared Reflectance Analysis of Foods. D. L. Wetzel SECTION C

Symposium on Analytical Chemistry of Nuclear Safeguards. Joint with Division of Nuclear Chemistry and Technology

J. A. Carter, Presiding 9:00 Role of Analytical Chemistry Measurements in Safeguards of Nu clear Materials. P. J. Persiani 9:30 Recent Efforts in Evaluation of In-Plant Equipment Applied To Nuclear Material Inventory Verifica tion. R. H. Augustson, P. A. Russo, T. Fitzsimmons, E. Kuhn 10:00 Mass Spectrometry in Safe guards: Resin Bead Techniques and the Mobile Van Laboratory. D. H. Smith, R. L. Walker, J. A. Carter 10:50 Mass Spectrometry of Nanogram Quantities of Th and U from (Th, U ) 0 2 Fuels. L. W. Green, T. H. Longhurst 11:10 Measurement of Plutonium Isotopic Abundances by Gamma-Ray Spectrometry. R. Gunnink 11:40 Calorimetric Assay: An Ac curate Analytical Technique for Plu tonium Safeguards. C. L. Fellers SECTION D

Symposium on the Chemistry of Plutonium—A Profile of Development and Future Directions. Joint with Division of Nuclear Chemistry and Technology

ANALYTICAL CHEMISTRY, VOL. 54, NO. 9, AUGUST 1982 · 1031 A

News J. T. Bell and B. Kanellakopulos, Pre siding 9:00 Introductory Remarks. 9:05 Present Status and Future Direction of Plutonium Process Chemistry. E. L. Christensen, L. W. Gray, J. P. Navratil, W. W. Schulz 9:30 Recent Advances in Plutoni um Process Chemistry at Rocky Flats. C. E. Baldwin, J. D. Navratil 9:55 Nonaqueous Processes for Plutonium Metal Recovery and Puri fication. M. S. Coops 10:30 Extraction of Pu(III) and Pu(IV) from Nitric Acid Media Using Carbamoylmethylphosphoryl Deriva tives and Its Significance in the Pro cessing and Recovery of Plutonium. E. P. Horwitz, H. Diamond 11:00 Further Aspects of Pu(IV) Hydrous Polymer Chemistry. L. M. Toth, M. M. Osborne 11:25 Reactions of Plutonium Ions with the Products of H2O Radiolysis. J. C. Sullivan SECTION Ε Symposium on the Applications of Stable Isotopes. Joint with Divisions of Nuclear Chemistry and Technology and Physical Chemistry

R. M. Lambrecht, Presiding 9:00 Separation of Selected Stable Isotopes by Liquid-Phase Thermal Diffusion and by Chemical Exchange. W. Μ. Rutherford, Β. Ε. Jepson, Ε. D. Michaels 9:25 Direct Determination of Ionic Hydration by Neutron Scattering with Enriched Isotopes. R. L. Hahn, A. H. Narten 9:50 Validation of In Vivo Stable Isotope Tracing of Zinc. G. E. Gor don, I. Gokmen, N. K. Aras, R. I. Henkin, R. L. Aamodt, W. Rumble 10:15 Determination of Ca-46 in Fecal Samples by Measurement of Ca-47 to Ca-45 Ratios after Neutron Activation. S. E. Schlegel, D. E. Troutner SECTION F

9:20 Neutron Activation of Mesoamerican Obsidian Sources: Analysis and Data Interpretation. J. R. Vogt, R. H. Cobean, C. C. Graham, M. D. Glascock 9:40 Use of Rare Earth Element Analysis To Study the Utilization and Procurement of Soapstone along the Labrador Coast. R. Allen, H. Hamroush 10:00 Multielement Examination of Excavated Human Bone. J. B. Lambert, J. E. Buikstra, S. M. Vlaska 10:20 Establishing Environmental Baselines Using Prehistoric/Archaeolo gical Materials. E. A. Coughlin, C. P. Claassen 11:00 Dexter Award Address. Kekulé's Dreams: Fact or Fiction? J. H. Wotiz SECTION G Symposium on Chlorinated Dioxins and Dibenzofurans in the Total Environment. Joint with Division of Environmental Chemistry

L. H. Keith, Presiding 8:55 Introductory Remarks. 9:00 Dioxins: A Canadian Perspective. H. M. Tosine 9:40 Dioxins and the Regulatory Process at EPA. J. A. Todhunter 10:05 Characterization of Tetrachlorodibenzofurans. T. Mazer, F. D. Hileman, R. W. Noble, J. J. Brooks 10:30 Synthesis of UL- 13 C Polychlorinated Dibenzofurans. R. A. Bell 11:00 Off-Site Transport of 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD) from a Herbicide Production-Disposal Facility. L. J. Thibodeaux 11:25 Survey of Great Lake Commercial Fish for 2,3,7,8-Tetrachlorodibenzo-p-dioxin Residues. J . J . Ryan, B. Lau, J. C. Pilon, D. Lewis, H. McLeod 11:50 New GC Detector for Screening TCDD Samples. L. H. Keith, R. C. Hall, R. C. Hanisch, A. E. Jones

Tuesday Afternoon

Symposium on Archaeological Chemistry. Joint with Division of the History of Chemistry

J. B. Lambert, Presiding 8:50 Introductory Remarks. 9:00 Provenience Studies of Mid dle Eastern Obsidian from Sites in Highland Iran. M. J. Blackman

SECTION A Symposium on Trends in Liquid Chromatography

J. W. O'Laughlin, Presiding 1:30 HPLC Determination of Ben-


zidine and Its Congeners in Direct Dyes. F. E. Pallas, D. E. DuSold, E. A. Murrill, C. W. Jameson 1:50 HPLC Determination of Benzo(a)pyrene and Benzo(e)pyrene in Mouse Tissues. C. B. Fanska, L. W. Pittman, E. A. Murrill, C. W. Jameson, M. P. Dieter 2:10 Surface Characterization of Small Particles by Diagnostic Chromatography. J. G. Eckhardt, M. F. Burke, C. D. Wilcox 2:30 HPLC Separation of 15Methyl PGF 2 „ Methyl Ester Isomers. S. M. Plaisted, B. G. Snider 3:10 Liquid Chromatographic Separation of Methyl Complexes with 1,10-Phenanthroline and Mixed Ligand Complexes. J. W. O'Laughlin 3:30 Determination of Chloride in Technical-Grade Sulfuric Acid by Ion Chromatography. R. E. Smith 3:50 Microbore High-Performance Liquid Chromatography with On-Line Fourier Transform Infrared Detection. R. S. Brown, C. C. Johnson, L. T. Taylor 4:10 HPLC Detection Using a Polarimeter Flow Cell. D. L. Dunn, B. S. Scott, E. D. Dorsey 4:30 Pressure Release Valve and Pressure Gauge Protector for Liquid Chromatography. J. G. Nikelly

SECTION Β Symposium on Remote Sensing of Physical Chemical Parameters over Optical Fibers

T. Hirschfeld, Presiding 9:00 Fiber Optics for Visualization and Position, Temperature, and Strain Sensing. E. Snitzer, J. Dunphy, W. Glenn, G. Meltz, W. Morey 9:20 Anomalous Dispersion in Waveguides for Ionizing Radiation Dosimetry. S. Kronenberg 9:40 Time Domain Optical Spec trometry with Fiber Optic Wave guides. W. B. Whitten 10:00 Fiber Optic Temperature Sensors Using Optical Fibers. G. B. Brandt, M. Gottlieb 10:40 Remote Analysis with Fiber Optics. T. Hirschfeld, T. Deaton, R. Malstrom, F. Milanovich 11:00 On-Line Uranium Analysis Using Remote Fiber Fluorimetry. R. Malstrom, T. Hirschfeld, T. Deaton 11:20 Fiber Optics for Use in InLine Process Photometric Measure ments. D. McCue, D. Bostick 11:40 Radiometry with Fiber Op-

News tics for Analytical Applications. J. Knight, W. O'Brien, L. Waszak SECTION C Symposium on Analytical Chemistry of Nuclear Safeguards. Joint with Division of Nuclear Chemistry and Technology

P. J. Persiani, Presiding 1:50 Applications of Inductively Coupled Plasma-Atomic Emission Analysis to Nuclear Safeguards. M. C. Edelson, V. A. Fassel 2:10 Nuclear Safeguards Account ancy: A Case for Certified Reference Materials. Ν. Μ. Trahey 2:30 Los Alamos Program of Chemical Methods Development for Safeguards. S. F. Marsh, R. M. Abernathey, R. M. Hollen, D. D. Jackson, J. E. Rein, N. M. Saponara 3:20 Total Uranium Analysis Using Nondestructive Passive Gamma-Ray Techniques. R. C. Hagenauer, K. Lewis 3:40 Advanced Automated Controlled-Potential Coulometric Analyz er Using an Improved Method for Plu tonium Determination. R. M. Hollen, D. D. Jackson, J. E. Rein 4:00 Colorimetric Determination of Reducing Normality in the Purex Process. E. W. Baumann SECTION D Symposium on the Chemistry of Plutonium—A Profile of Development and Future Directions. Joint with Division of Nuclear Chemistry and Technology

J. L. Burnett and J. C. Sullivan, Pre siding 2:00 Introductory Remarks. 2:05 Behavior of Plutonium in Natural Waters. B. Allard, J. Rydberg 2:35 Solubility Controlled Pluto nium Concentrations in Solutions Containing Pu-Doped Glass. D. Rai, R. G. Strickert 3:05- Groundwater Composition and Its Relationship to Plutonium Transport Processes. J. M. Cleve land, T. F. Rees, K. L. Nash 3:40 Complexation of Pu Ions in Carbonate-Bicarbonate Solutions: Ki netics of Redox and Disproportionation Reactions. J . I. Kim, C. Lierse, F. Baumgârtner 4:10 Plutonium in Near-Neutral

Aqueous Solutions. H. Nitsche, Ν. Μ. Edelstein 4:40 Stability Constants, Enthal pies, and Entropies of Pu(III) and Pu(IV) Sulfate Complexes. K. L. Nash, J. M. Cleveland

SECTION Ε Symposium on Archaeological Chemistry. Joint with Division of the History of Chemistry

J. B. Lambert, Presiding 2:00 Modern Neutron Activation Analysis and Ancient History. I. Perlman 2:40 Chemical Compositions of Copper-Based Roman Coins VII. Claudian Quadrantes, 41-42 A.D. G. Carter 3:00 Mass Spectrometry as a His torical Probe: Quantitative Answers to Historical Questions in Metallurgy. M. C. Usselman 3:20 Trace Element Analysis of Copper Trade Goods from the Pacific Northwest. D. C. Stapp 3:40 Trace Element Discrimina tion of Distinct Sources of Native Copper. G. Rapp, Jr., J. Allert, E. Henrickson 4:00 Archaeometric Perspectives on Early Metallurgy. U. M. Franklin 4:40 Trace Element Composition of Longquan Porcelain. L. H. Hon

SECTION F Symposium on Chlorinated Dioxlns and Dibenzofurans in the Total Environment. Joint with Division of Environmental Chemistry

G. Choudhary, Presiding 2:00 Introductory Remarks. 2:05 Polychlorinated Dioxins, Di benzofurans, and Other Polynuclear Aromatics Formed During Incinera tion and PCB Fires. C. Rappe, S. Marklund, P. A. Bergqvist, M. Hansson 2:45 Assessments of Incineration Processes as Sources of Supertoxic Chlorinated Hydrocarbons: Concen trations of CDDs/CDFs and Possible Precursor Compounds in Incinerator Effluents. M. L. Taylor, T. O. Tiernan, J. G. Solch, J. H. Garrett, G. F. VanNess 3:10 Determination of 2,3,7,8-


TCDD in Industrial and Municipal Wastewaters, Method 613, Part 1— Development and Detection Limits. D. L. Foerst, J. E. Longbottom, R. J. Wesselman, C. R. McMillin, R. W. Noble, D. Wood 3:35 Determination of 2,3,7,8TCDD in Industrial and Municipal Wastewater, Method 613, Part 2— Performance Evaluation and Method Study Results. C. R. McMillin, F. D. Hileman, D. E. Kirk, T. Mazer, B. J. Warner, J. Longbottom, R. Wes selman 4:10 Occurrence of TCDD in Envi ronmental Samples from Southwest Missouri. R. D. Kleopfer, W. W. Bunn, K. T. Yue, D. J. Harris 4:35 Composition of PCDF and PCDD Residues in Sediments of the Hudson and Housatonic Rivers. J. D. Petty, L. M. Smith, P. Bergquist, J. N. Johnson, D. L. Stalling, C. Rappe

SECTION G Symposium on Identification and Analysis of Organic Pollutants in Air— Sampling Techniques. Joint with Division of Environmental Chemistry

L. H. Keith, Presiding 1:55 Introductory Remarks. 2:00 Overview of the Environmen tal Monitoring Systems Laboratory's (EMSL/RTP) Present and Future Method Development Activities for the Analysis of Air Pollutants. T. R. Hauser 2:50 Applicability of Passive Sam pling Techniques to the Analysis of Specific Vapors in Air. R. H. Brown, P. C. Cox, C. J. Purnell, N. G. West, M. D. Wright 3:10 Diffusional Sampling for Toxic Substances. D. M. Coulson, S. J. Selover, E. C. Gunderson, B. A. Kingsley 3:30 Vapor-Phase Sampling of Or ganic Compounds. G. A. Junk, J. J. Richard 4:00 Comparison of Tenax-GC and XAD-2 as Polymer Adsorbents for Sampling Combustion Exhaust Gases. R. L. Hanson, C. R. Clark, R. L. Carpenter, C. H. Hobbs 4:20 Synthesis and Characteriza tion of Porous Polyimides for Air Sampling of Volatile Organic Com pounds. B. A. Demian, K. K. Lam, A. Schindler, E. D. Pellizzari 4:50 Collection of Vapor-Phase Polycyclic Aromatic Hydrocarbons in Ambient Air. C. Keller, T. F. Bidleman

News Wednesday Morning SECTION A

Symposium on Validation of Data at the Trace Level

L. B. Rogers, Presiding 8:30 Inexact Science of Trace Analysis. L. B. Rogers 8:50 Validation of Analytical Methods. J. K. Taylor 9:10 Principles of Validation of Analytical Systems. W. Horwitz 9:30 Detection Limits, Regulatory Limits, and Interlaboratory Measure ments. L. A. Currie 9:50 Method Standardization and Interlaboratory Compatibility of Serum Polychlorinated Biphenyl Analysis. J. A. Liddle 10:10 Data Validation in a Large, Multilaboratory Environmental Moni toring Project. W. L. Budde, R. L. Prairie, P. W. Britton, B. P. Almich 10:45 Panel Discussion. Partici pants are symposium speakers. SECTION Β

Symposium on Image Devices in Spectroscopy. Joint with Division of Physical Chemistry

Y. Talmi, Presiding 9:00 Image-Intensified Linear and Area Arrays as Detectors for Spectros copy. R. E. Blank, C. B. Johnson 9:30 Recent Advances and Appli cations of Electro-optical Ion Detection Mass Spectrometry (EOIDMS). H. G. Boettger 10:15 Multichannel Spectroscopy for Tokamak Plasma Diagnostics. R. J. Fonck, A. T. Ramsey 10:45 Current Developments in High-Resolution X-ray Measure ments. D. T. Attwood 11:20 Spectrometers for Rocket, Balloon, and Spacecraft Experiments Using Multichannel Imaging Detec tors. A. Matsuzaki, Y. Nakamura, T. Itoh SECTION C

Symposium on the Chemistry of Plutonium—A Profile of Development and Future Directions. Joint with Division of Nuclear Chemistry and Technology

J. Fuger and D. Rai, Presiding 9:00 Introductory Remarks.

9:05 Measurement and Interpreta tion of Plutonium Spectra. J. Blaise, M. S. Fred, W. T. Carnall, H. M. Crosswhite, H. Crosswhite 9:30 Electronic Spectra and Fluo rescence of Plutonium(V) in Complex Fluorides. L. R. Morss, C. W. Williams, W. T. Carnall 9:50 Some Thermodynamic As pects of the PuU2-x Systems. M. Tetcnbaum 10:10 Vapor Pressures and Vapor Compositions in Equilibrium with Hypostoichiometric Plutonium Dioxide at High Temperature. D. W. Green, J. K. Fink, L. Leibowitz 11:00 Round-Table Discussion on the Status of Pu Chemistry: Accom plishments, Requirements, and New Directions. R. A. Penneman, discus sion leader SECTION D

Symposium on Archaeological Chemistry. Joint with Division of the History of Chemistry

G. F. Carter, Presiding 9:00 Pigment Analysis of Cilician Gospel Books of the 13th and 14th Centuries. D. E. Cabelli, M. V. Orna 9:20 Nondestructive Scanning Auger Microscopy for Dating of Man uscript Inks. R. J. McNeil 9:40 Technological Examination of Egyptian Blue. M. S. Tite, M. Bimson, M. R. Cowell 10:20 X-ray Diffraction Analysis of Ancient Glass. M. Ripinsky 10:40 Major, Minor, and Trace Ele ment Analysis of Medieval Stained Glass by Flame Atomic Absorption Spectrometry. Ν. Η. Tennent, P. McKenna, G. McLean, K. Lo, J. M. Ottaway 11:00 Provenance Studies of Mex ican Majolico Using Elemental and Phase Analysis. J. S. Olin, M. Maggetti, F. Lister, R. Lister 11:20 Study on the Provenance of Five Orange Mayan Figurines from Jaima and Jonuta by Atomic Absorp tion Spectrometry. L. Torres, A. Arie, B. Sandoval 11:40 Application of Geochemical Techniques to the Investigation of Predynastic Sites in Egypt. R. Allen, H. Hamroush SECTION Ε

Symposium on Chlorinated Dioxins and Dibenzof urans in the Total Environment. Joint with Division of Environmental Chemistry


C. Rappe, Presiding 9:00 Introductory Remarks. 9:05 Analytical Chemistry of the Chlorinated Dibenzodioxins and Dibenzofurans—A Review of the Cur rent Status. T. O. Tiernan 9:45 Parameters for Identifica tion and Confirmation in Trace Anal yses of Polychlorinated Dioxins and Dibenzofurans. C. Rappe, S. Marklund, M. Nygren, A. Gara 10:10 Quality Assurance Samples for the Dioxin Monitoring Program. R. K. Robeson, J. R. Donnelly, A. E. Dupuy, Jr., R. L. Harless, W. L. Budde 10:45 Validation Study for the GC-Atmospheric Pressure Ionization MS Method for the Isomer-Specific Determination of 2,3,7,8-TCDD. R. K. Mitchum, W. A. Korfmacher, G. F. Moler 11:10 Confidence Limits for the Isotope Dilution/Gas Chromatographic-Mass Spectrometric Determina tion of 2,3,7,8-Tetrachlorodibenzo-pdioxin in Environmental Samples. G. F. Moler, R. R. Delongchamp, R. K. Mitchum, W. A. Korfmacher, B. A. Pearce 11:35 Evaluation of Interferences from Seven Series of Polychlorinated Aromatic Compounds in GC/MS De terminations of Polychlorinated Di benzofurans and Dioxins. L. M. Smith, J. L. Johnson

SECTION F

Symposium on the Identification and Analysis of Organic Pollutants in Air— Analytical Techniques. Joint with Division of Environmental Chemistry

L. H. Keith, Presiding 9:25 Introductory Remarks. 9:30 Profiling PAH Emissions by Open-Tubular Column GC with Liq uid Crystal Stationary Phases. K. D. Bartle, A. El-Nasri, B. Frere 9:55 Purge and Cryogenic Trap ping Technique Used To Correlate Am bient Air Organics with Wastewater Emissions. K. W. Lee, R. D. Cox, R. F. Earp 10:25 Identification of Organics in Ambient Air Using Multiple Gas Chromatographic Detectors. R. F. Earp, R. D. Cox, K. W. Lee 11:00 Development of Preconcentration and Chromatographic Proce dures for the Continuous and Unat tended Monitoring of Hydrocarbons

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in Ambient Air. L. D. Ogle, R. C. Hall, W. L. Crow, E. Jones, J. P. Gise 11:30 Survey Methods for the De termination of Principal Organic Haz ardous Constituents in Incinerator Ef fluents. R. H, James, H. C. Miller, W. R. Dickson

Wednesday Afternoon SECTION A

Symposium on General Topics

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J. P. Foley, Presiding 1:30 Allerton Analytical Confer ences. T. J. Logan 1:50 Quality Assurance Tech niques for Reference Laboratory Anal ysis of Dosage Formulations. C. W. Jameson, C. A. Castro, G. 0. Kuhn, E. A. Murrill 2:10 Accurate Equations for Chro matographic Figures of Merit for Ideal and Skewed Peaks. J. P. Foley, J. G. Dorsey 2:30 Reliability of Factor Analysis in Presence of Random Noise or Outlying Data. R. F. Hirsch, G. Lam, P. C. Tway 3:10 High-Performance Liquid Chromatography by Derivatization— Sulfur Mustards and Their Decompo sition By-products. P. C, Bossle, J. J. Martin, E. W. Sarver 3:30 Investigation of the Selectivity and Sensitivity of the Helium-Neon Laser Intracavity Absorption Detec tor. J. D. Parli, R. B. Green 3:50 Use of Lanthanide Ions as Luminescence Probes for Small Mole cules. L. M. Hirschy, E. V. Dose, J. D. Winefordner 4:10 Analysis of Volatiles from Preprinted Forms. J. D. Witt, C. D. Wilcox, D. A. Loy SECTION Β

Symposium on Image Devices in Spectroscopy. Joint with Division of Physical Chemistry

Y. Talmi, Presiding 1:30 Digicon Progress Report. E. A. Beaver, R. O. Ginaven, R. D. Smith 2:00 Ideal and Practical Perfor mance of Photon Limited Array De tectors. D. G. Currie 2:45 Remote Two-Dimensional Imaging on a Spectrograph with a One-Dimensional Optical Fiber Array. C. E. Iverson, M. A. Nelson

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News 3:15 Evaluation of Charge Injection Devices as Detectors for Atomic Emis sion Spectroscopy. G. R. Sims, M. B. Denton, H. A. Lewis 3:45 Operation Characteristics and Considerations When Employing Charge Injection and Charge-Coupled Devices in Practical Chemical Analy sis. M. B. Denton, H. A. Lewis, G. R. Sims 4:15 Automatic Optimization of Integration Time for Linear Diode Array Detectors. P. J. Aiello, C. Enke SECTION C Symposium on New Physical Methods in Medical Chemical Research. Joint with Division of Medicinal Chemistry

A. Makriyannis, Presiding 2:00 Introductory Remarks. 2:05 Mass Spectrometry and Drug Metabolism. N. Castagnoli, Jr. 2:35 Use of NMR Spectroscopy To Study the Geometric Requirements for Drug Membrane Interactions. A. Makriyannis 3:05 From Recognition to Activa tion: A Theoretical Study of Molecu lar Events in Pharmacological Mecha nisms. R. Osman, S. Topiol, L. Rubenstein, H. Weinstein 3:35 Interactive Three-Dimensional Computer Graphics. R. Langridge 4:05 Discussion. 4:15 Poster Session: NMR Studies on the Antibiotic Avoparcin: Interactions with Model Re ceptors of Bacterial Cell Walls. S. W. Fesik, I. M. Armitage, G. A. Ellestad, W. J. McGahren Applications of Two-Dimensional NMR Spectroscopy in Complex Spec tral Assignments. G. E. Martin, M. R. Willcott III, S. L. Smith, M. L. Lee, M. Iwao, R. N. Castle On-Line Ion-Pair Extraction and Derivatization for HPLC-MS. M. J. Hayes, E. Lankmayr, B. L. Karger, P. Vouros Use of NMR, Circular Dichroism, and Raman Spectroscopies for Studies of Conformation-Activity Relations of Peptide Agonists and Antagonists. V. J. Hruby, H. I. Mosberg, T. W. Rockway Crystallographic Structure of a Penicillin-Sensitive Enzyme and Lo cation of the Antibiotic Binding Site. J. R. Knox, J. A. Kelly, P. C. Moews Computer-Assisted Vibrational Spectroscopy in Medical Chemical Research. L. G. Tensmeyer, J. B. Deeter, H. L. Hunter

SECTION D Symposium on Archaeological Chemistry. Joint with Division of the History of Chemistry

G. F. Carter, Presiding 2:00 Soil Chemical Investigations in Illinois Archaeology: A Personal Retrospective. W. I. Woods 2:20 Chemical Analysis of Archaeological Soils from Yogi Site, Japan. R. G. V. Hancock, C. A. Stimmell, A. M. Davis 2:40 Evaluation of the Thermolu minescence (TL) Dating of Loess. R. M. Rowlett 3:00 Technical Examination of Oriental Lacquer. G. W. Carriveau 3:20 Examination of the Phenom enon of Textile Fabric Pseudomor phism. K. A. Jakes, L. R. Sibley 3:40 Analysis of Exudate Plant Gums in Their Artistic Applications. J. W. Twilley 4:00 Radiocarbon Dating by Parti cle Accelerators: An Archaeological Perspective. R. E. Taylor 4:20 Formation of the Image on the Shroud of Turin by X-rays: A New Hypothesis. G. F. Carter 4:40 Comprehensive Examination of the Various Stains and Images on the Shroud of Turin. E. J. Jumper, A. D. Adler, J. H. Heller, S. F. Pellicori, J. P. Jackson SECTION Ε Symposium on Chlorinated Dioxins and Dibenzofurans in the Total Environment—Occupational Exposure. Joint with Division of Environmental Chemistry

G. Choudhary, Presiding 2:00 Introductory Remarks. 2:05 Occupational Exposure to Chlorinated Dioxins and Dibenzofu rans: A Perspective. G. Choudhary 2:30 Occupational Exposure to Polychlorinated Dioxins and Dibenzo furans. C. Rappe, M. Nygren, G. Gustafsson 2:55 Epidemiological Studies on Soft-Tissue Sarcoma, Malignant Lym phoma, Nasal, and Nasopharyngeal Cancer and Their Relation to Phenoxy Acid or Chlorophenol Exposure. L. Hardell 3:30 Polychlorinated Dibenzofu rans in the Tissue of Patients with Yusho and Their Enzyme-Inducing Activities on Aryl Hydrocarbon Hy


droxylase. Y. Masuda, H. Kuroki, J. Nagayama 3:55 Nonmutagenicity of Phenoxy Acid Herbicides 2,4-D and MCPA. K. Linnainmaa, H. Vainio 4:20 Comparison of the Immunodepressive Effect of 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD) and 2,3,7,8-Tetrachlorodibenzofuran (TCDF) in Mice. A. Vecchi, M. Sironi, M. A. Canegrati, S. Garattini 4:45 Concluding Remarks. SECTION F Symposium on the Identification and Analysis of Organic Pollutants in Air— Analytical Techniques. Joint with Division of Environmental Chemistry

R. M. Barkley, Presiding 2:00 Introductory Remarks. 2:05 Prospects for the Analysis of Mixtures of Polycyclic Aromatic Com pounds by Differential Pulse Voltammetry. N. Taylor, K. D. Bartle, D. G. Mills, C. Gibson, D. Servante 2:30 Sampling and Analytical Methods for Airborne Dialkyl Phthalates. S. J. Selover, E. C. Gunderson, C. W. Beeman, P. A. Boland, D. M. Coulson. 2:55 Sampling and Analysis of Diisopropyl Sulfate in Air. B. A. Kingsley, E. C. Gunderson, D. M. Coulson 3:30 Multiresidue Analysis of Trace Organic Pesticides in Air. T. A. Wehner, J. E. Woodrow, Y.-H. Kim, J. N. Seiber 3:55 Liquid Chromatographic Methods for the Determination of Polycyclic Aromatic Hydrocarbons in Air Particulate Extracts. W. E. May, W. F. CuthreU, R. E. Rebbert, S. A. Wise 4:20 Air Pollution: The Applica tion of Simple Luminescence Tech niques for Monitoring Polynuclear Ar omatic Pollutants. T. Vo-Dinh

Thursday Morning SECTION A Symposium on Investigations in Gas Chromatography and Mass Spectrometry

M. M. Bursey, Presiding 9:00 Quick Screening Method for Aroclor 1254. S. S. Que Hee, W. M. Tabor, R. R. Suskind, J. Ward 9:20 Determination of Chlorinated Biphenyls (Incidental PCBs) in Chlo-

News rinated Hydrocarbon Process and Waste Streams by Selected Ion Moni toring GC/MS. R. S. Collard, M. M. Irwin, Jr. 9:40 Comparison of Two Mass Spectrometric Techniques for the Analysis of Involatile Organometallic Complexes. R. L. Cerny, M. M. Bursey 10:00 Reactions of Organics and Metals in a Spark Source Mass Spec trometer. W. L. Grady, M. M. Bursey 10:40 Mass Spectral Characteriza tion of Isomeric Oxygen-Containing Aromatic Compounds Using Methanol Chemical Ionization. M. V. Buchan an, G. L. Kao 11:00 Mass Spectral Investigation of the Effects of Sample Matrices in Graphite Atomizers. G. D. Rayson, J. A. Holcombe 11:20 Analysis of Sulfur in NBS Standard Reference Materials by Thermal Ionization Mass Spectromet ric Isotope Dilution. P. J. Paulsen, W. R. Kelly 11:40 Ion Chemistry of (C 6 H 5 )++. R. J. Doyle, Jr., J. E. Campana

try of Microbial Metabolism. R. Lovrien, S. Parquette, P . Chapman 9:20 Comparison of Experimental and Theoretical Molecular Ion Distri butions of Middle Molecules. J . Yergey, D. Heller, C. Fenselau, R. Cotter 9:40 Molecular Weight Distribu tion of Pine Kraft Lignin by GPC. L. K. Swofford, S. L. Ivy 10:00 Synthesis and Characteriza tion of Phosphoric-Acid-Ester Cat ion-Exchange Resins. R. B. Selzer, D. G. Howery 10:40 Flow Injection Technique for the Determination of Diffusion Coefficients. G. A. Gerhardt, R. N. Adams 11:00 Volumetric Determination of Adsorption Isotherms for Condens able Vapors on Porous Adsorbents of High Surface Area. S. B. Smith 11:20 HPLC Analysis of Aflatoxins in Raw Peanuts. W. J. Hurst, R. A. Martin, Jr. 11:40 Assay of Five α-Keto and Hydroxy Analogs of Essential Amino Acids in Enteral Diets by HPLC. J. H. C. Wang, F. Caporaso, S. D. Hersh, K. L. Wong, S. J. Saxena, R. M. Kiral

SECTION Β

Symposium on Image Devices in Spectroscopy. Joint with Division of Physical Chemistry Y. Talmi, Presiding 9:00 Luminescence Measurements with an Intensified Diode Array. J. D. Ingle, Jr. 9:30 Analytical Chemistry with Spatial Resolution. J. B. Callis, D. H. Burns, C. J. Webb, G. D. Christian 10:15 Pulsed Laser Excitation Fluorometer with Intensified Diode Array Detector for Real-Time Charac terization of HPLC and Capillary GC Effluents. J. B. Callis, D. B. Skoropinksi, B. V. Pepich, J. D. S. Danielson, G. D. Christian 10:45 Comparison of a Multiple Entrance Slit Vidicon Spectrometer with a Time-Multiplexed Multiple Entrance Slit Spectrometer. K. W. Busch, L. D. Benton 11:15 Evaluation of Array Detec tors in ICP-AES. Γ. Grabau, V. A. Fassel, Y. Talmi SECTION C

Symposium on General Topics J. G. Nikelly, Presiding 9:00 New Method in Dilute Aque ous Organic Analysis: Microcalorime-

SECTION D

Symposium on the Identification and Analysis of Organic Pollutants in Air— Emissions, from Combustion Sources. Joint with Division of Environmental Chemistry

C. L. Haile, Presiding 9:00 Introductory Remarks. 9:10 Effect of Oxidizing Species in Combustion Gas on Sampling and Analysis of Trace Organics. J. C. Har ris, A. J. DeMarco, R. P. O'Neil 9:35 Standards Preparation for Solid Sorbent Cartridges. J. G. Wind sor, Jr., J. R. Mease, J. A. Stikeleather, R. E. Means 10:00 Quality Assurance Program for Combustion Source Studies. J. S. Stanley, C. L. Haile, A. M. Small, R. V. Northcutt 10:35 Sampling and Analysis Methods Used in a Trial Burn at a Hazardous Waste Incinerator. G. Jungclaus, S. Swanson, P. Gorman 11:00 PCB Emissions to the At mosphere from Municipal Landfills and Incinerators. T. J. Murphy, L. J. Formanski, B. Brownawell, J. A. Meyer 11:25 Emissions of Organic Pollu tants from Coal-Fired Utility Boiler Plants. C. L. Haile, J. S. Stanley, A. M. Small, R. V. Northcutt


Thursday Afternoon SECTION A

Symposium on Studies Relating To Electrochemistry K. Kiss, Presiding 1:30 Microbeam Characterization of Corrosion-Protective Coatings on Steel. K. Kiss, M. Coll-Palagos 1:50 Nonadiabatic Electron Transfer Reactions. C. A. Koval, M. E. Ketterer, R. L. A. Pravata, C. M. Reidsma 2:10 Electrochemical Studies of the Formation and Decomposition of Alkyl Aryl Ether Radical Anions. D. E. Bartak, M. D. Koppang, N. F. Woolsey 2:30 Electrochemical Oxidation of Aromatic Compounds Adsorbed on Platinum Electrodes: The Influence of Molecular Orientation. M. P. Soriaga, J. L. Stickney, A. T. Hubbard 3:10 Cleavage of Halogen from Substituted Biphenyls via Electrocatalytic Reduction. J. F. Rusling, T. F. Connors, J. Arena, M. T. Carter 3:30 Electrochemistry on Brain Slices. M. E. Rice, R. N. Adams 3:50 Surface Studies of Gold Elec trodes Subjected to Deposition and Stripping of Mercury in Acidic Solu tion. W. R. Hussein, L. A. Schadewald, D. C. Johnson 4:10 Liquid Membrane Dicyanorgentate Ion Electrodes Based on Qua ternary Ammonium Sites. Y. Ru-qin, H. Sha-sheng SECTION Β

Symposium on Image Devices in Spectroscopy. Joint with Division of Physical Chemistry Y. Talmi, Presiding 1:30 Multichannel Detection of Resonance Raman Spectra of a Pi cosecond Intermediate in the Photoly sis of Oxyhemoglobin. M. F. Nicol, M. Nagumo, M. A. El-Sayed 2:00 Methods of Picosecond Ab sorption, Emission, and Raman Spec troscopy and Applications to Chemi cal Systems. E. F. Hilinski, S. V. Mil ton, P. M. Rentzepis 2:45 Picosecond Emission Spec troscopy with Intensified Photodiode Array. P. F. Barbara, S. H. Courtney, K. Ding 3:45 Jitter-Free Signal Averaging Streak Camera and Applications in

News Picosecond Fluorescence Spectroscopy. W. Knox, G. Mourou SECTION C

Symposium on General Topics J. F. Pankow, Presiding 1:30 Effects of Linear Flow Velocity and Residence Time on the Retention of Nonpolar Analytes by Cartridges of Tenax-GC. J. F. Pankow, L. M. Isabelle, T. J. Kristensen 1:50 Interfacing of Capillary Column Gas Chromatography with Adsorption/Thermal Desorption (ATD) with Tenax-GC in the Analysis of Trace Organics. J. F. Pankow, L. M. Isabelle, T. J. Kristensen 2:10 Sepharose-Linked Ascorbic Acid Oxidase for Flowing-Stream Analyses. C. W. Bradberry, R. N. Adams 2:30 Flow Injection Determination of Total Bilirubin in Serum. T. S.-C. Wang, J. D. Defreese 3:10 GC-EC Determination of a Potential Antidepressant Drug and Its

N-Demethylated Metabolites in Serum. D. B. Lakings, R. B. Stryd, T. J. Gilbertson 3:30 Electronic Properties of Benzimidazole and Thiabendazole and Their Homologues. Effect of Substituents and Solvent on the Nature of the Transition. L. J. Cline Love, P. C. Tway. 3:50 Chloride, Ammonia, and Bicarbonate Interferences in an Automated Phenol Red Method for Bromide Determination in Water. C. L. Basel, J. D. Defreese, D. O. Whittemore 4:10 Matrix Correction Method for the X-ray Fluorescence Analysis of Biological Samples. G. S. Kuntz, R. L. R. Towns SECTION D

Symposium on the Identification and Analysis of Organic Pollutants in Air— Case Studies. Joint with Division of Environmental Chemistry J. P . Lodge, Presiding

1:45 Analysis of Individual Hydrocarbon Species in Ambient Atmospheres: Techniques and Data Validity. H. Westberg, W. Lonneman, M. Holdren 2:10 Characterization of the Mutagenic Fractions of Organic Constituents in Rice Straw Smoke. T. J. Mast, H. E. Olsen, D. P. Hsieh, J. N. Seiber 2:35 Measurement of Monoterpene Hydrocarbons in Rural Atmospheres. R. E. Sievers, J. M. Roberts, F. C. Fehsenfeld 3:00 New GC Method for the Measurement of Volatile Nitrosamines in Air Samples at Sub-ppb Concentrations. C. H. Williams, A. E. Jones, J. C. Butler, R. C. Hanisch 3:30 Characterization of Polycyclic Organic Matter in Urban Air Particulate Matter by Gas Chromatography-Electron Impact and Negative Ion Chemical Ionization Mass Spectrometry. T. Ramdahl, G. Bêcher, A. Bj0rseth 3:55 Characterization of Biogenic and Petroleum-Derived Organic Matter in Aerosols over Remote, Rural, and Urban Areas. M. A. Mazurek, B. R. T. Simoneit

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News was named an honorary member of the society. He has served on the advi-

4:20 GC-MS-DS Analysis of Organic Pollutants Produced during the Disposal of Missiles by Burning. D. C. Lane, E. D. Erickson, H. F. Cordes 4:45 Importance of Identifying Organic Pollutants in Air. G· A. Holton, F. O. Hoffman 5:05 Concluding Remarks.

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Fassel Receives Chemical Instrumentation Award Velmer A. Fassel, deputy director of Ames Laboratory and professor of chemistry at Iowa State University, has been named 1983 recipient of the Chemical Instrumentation Award. Sponsored by the Dow Chemical Company and administered by the Division of Analytical Chemistry of the American Chemical Society, the award is given annually to recognize and encourage achievement in the origination or improvement of analytical instrumentation. Fassel will receive a plaque, $2500, and travel expenses to the 1983 ACS National Meeting in Seattle, Wash., where the award will

Velmer Fassel be presented during a symposium held in the recipient's honor. Fassel's research focuses on atomic emission, absorption, and fluorescence spectrometry, X-ray excited optical luminescence, and other analytical techniques for ultratrace analysis. He has been the recipient of several major awards, including the ACS Award in Analytical Chemistry in 1979 and the Anachem Award in 1971. Fassel recently was awarded the Japan Society of Analytical Chemistry Medal and

Anachem Award—James N. Shoolery of Varian Associates, Palo Alto, Calif., will be presented with this year's Anachem Award at the upcoming September meeting of the Federation of Analytical Chemistry and Spectroscopy Societies. The award, sponsored by the Detroit Association of Analytical Chemists, is given annually in recognition of service to analytical chemistry through research, administration, teaching, and other activities. Shoolery joined the Varian staff in 1952, and since that time has devoted considerable effort to developing chemical applications of high-resolution nuclear magnetic resonance spectrometry. His current research interests focus on quantitative aspects of Fourier transform NMR, 13 C NMR of petroleum oils and edible oils of plant

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