Business: Growing by columns - ACS Publications

at a satisfactory stage of development to fulfill this role. David Bradley. Growing by columns. Agilent Technologies solidified its position in the se...
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ment deadline was not met. Four

According to the NPL, a “robust

undertaking such work should not be

NMRMs that were identified as poten-

framework of radioactivity metrology

underestimated. Certified NMRMs, it

tially useful were not finalized in the

is essential to support the ongoing

says, are a “vital part of traceability in

allocated period of time, although the

exploitation of nuclear processes and

analytical science.” Without these stan-

LGC says the U.K.’s National Physical

products.” This makes accurate and

dards, there is no absolute method of

Laboratory (NPL) may ultimately take up

traceable measurements based on stan-

checking the validity of any measure-

the reins in developing these further.

dard references critical to research and

ments recorded in the field.

The need for NMRMs was highlight-

environmental monitoring, which must

The DOE is now considering how to

ed as long ago as 1977 at a meeting of

stand up to serious public scrutiny. In

move forward with the four LGC materi-

the International Committee on Radionu-

recent years, comparisons of environ-

als. Experts say that there is obviously a

clide Metrology. V. T. Bowen of Woods

mental radioactivity measurements have

need for reproducibility and the mutual

Hole Oceanographic Institute pointed

sadly shown discrepancies due to inad-

acceptance of test data without which

out that natural-matrix materials spiked

equate radiochemical techniques and

the usefulness of measurements are

with radionuclides were inadequate for

uncertified methodology.

severely restricted. However, the four

various reasons and the environmental

The LGC carried out a survey of cur-

materials from LGC are not, at this time,

radiochemistry community must urgently

rently used NMRMs in western Europe

at a satisfactory stage of development to

develop homogeneous natural-matrix

and correlated this with the U.K.’s envi-

fulfill this role. David Bradley

samples, each naturally contaminated

ronmental monitoring needs.

by a range of radionuclides at various

Having identified four suitable

concentration levels.

matrixes, it was then impossi-

BUSINESS ble to find enough independ-

Growing by columns

or are under current development by the

ent laboratories to take part

likes of the National Institute of Stan-

in the study, so time ran out

dards and Technology, the NPL, and the

on the contract.

Agilent Technologies solidified its position in the separations market with the acquisition of J&W Scientific—the largest manufacturer and supplier of capillary GC columns—on March 29. According to the company, the takeover makes Agilent the largest supplier of GC instruments, consumables, and columns. J&W also manufactures CE and solid-phase extraction products.

Radio-NMRMs have been developed

LGC using materials such as river and

The DOE points out in its

lake sediments, soils, human tissues,

report that the time required

and bone ash.

and the costs involved in

J U N E 1 , 2 0 0 0 / A N A LY T I C A L C H E M I S T R Y

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