precipitation with ignition to Be0 a t 1050’ to 1100’ C. for 1 hour. Alternatively, a double precipitation followed by ignition a t 950’ C. may be made. ACKNOWLEDGMENT
The authors acknowledge the helpful suggestions of L. V. Jones, George Pish, and L. J. Wittenberg. LITERATURE CITED
(1) Brinten, P. H., Ellestad, R. B., J.Am. Chem. SOC.45, 395-8 (1923).
(2) Castro, C. C., in “National Nuclear Energy Series,” C. J. Rodden, ed., Vol. VIII-i; pp. 523-35, McGraw-Hill,’ Sew York, 1950. (3) . , Cook. 0. A.. in “National Kuclear Energy Series,”’ IV-l4B, G. T. Seaborg, J. J. Katz, W. Manning, eds., Part 1, pp. 147-61, McGraw-Hill, New York, 1949.
(4) Hillebrand, W. F., Lundell, G. E. F., “Applied Inorganic Analysis,” 2nd ed., p. 522, Wiley, New York, 1953. (5) Kollock, L. G., Smith, E. F., J . Am. Chem. SOC.23, 607-10 (1901).
(6) Porter, P., N7yld, G., ANAL.CKEM.27, 733-6 (1955). ( 7 ) Smith, E. F.,