Determination of Very Small Amounts of Carbon in Metals

Determination of Very Small Amounts of Carbon in Metalspubs.acs.org/doi/pdf/10.1021/ac60134a031by RE Fryxell - ‎1958 - ‎Cited by 10 - ‎Related a...
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Determination of Very Small Amounts of Carbon in Metals ROBERT

E.

FRYXELL

General Electric Co., Pittsfield, Mass.

b The precision of methods that involve exposure of crucibles to the atmosphere is normally inferior to the low pressure combustion method a t This limitacarbon levels < O . O O ~ ~ O . tion is the result of residual crucible blank even after prefiring a t 1 100' C. Stabilization of this blank by controlling the combustion temperature with a variable transformer significantly improves the precision of measurement. For the 7 0 analysis of metals containing