pubs.acs.org/joc
Design, Validation, and Implementation of a Rapid-Injection NMR System Scott E. Denmark,* Bruce J. Williams,*,† Brian M. Eklov, Son M. Pham, and Gregory L. Beutner Roger Adams Laboratory, Department of Chemistry, University of Illinois, Urbana, Illinois 61801
[email protected] Received April 29, 2010
A Rapid Injection NMR (RINMR) apparatus has been designed and constructed to allow the observation of fast chemical reactions in real time by NMR spectroscopy. The instrument was designed to allow the rapid (