Design, Validation, and Implementation of a Rapid-Injection NMR

Jul 30, 2010 - The authors urge interested parties to not embark on the construction of their own instrument and invite those whose research problems ...
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Design, Validation, and Implementation of a Rapid-Injection NMR System Scott E. Denmark,* Bruce J. Williams,*,† Brian M. Eklov, Son M. Pham, and Gregory L. Beutner Roger Adams Laboratory, Department of Chemistry, University of Illinois, Urbana, Illinois 61801 [email protected] Received April 29, 2010

A Rapid Injection NMR (RINMR) apparatus has been designed and constructed to allow the observation of fast chemical reactions in real time by NMR spectroscopy. The instrument was designed to allow the rapid (