First Synthesis of Bengazole A. - The Journal of Organic Chemistry

Roger J. Mulder, Cynthia M. Shafer, and Tadeusz F. Molinski*. J. Org. Chem. , 2000, 65 (23), pp 8126–8126. DOI: 10.1021/jo004032g. Publication Date ...
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8126

J. Org. Chem. 2000, 65, 8126

Additions and Corrections Vol. 64, 1999 Roger J. Mulder, Cynthia M. Shafer, and Tadeusz F. Molinski*. First Synthesis of Bengazole A.

Page 4995. The third paragraph, second sentence should begin, “Addition of 2-lithiooxazole (10 equiv, generated from 2,17 n-BuLi, THF, -78 °C, 20:1 v/v THF/ hexanes, 30 min)...”, not “...1:20 v/v THF/hexanes...” as printed. The stereoselectivity of this critical C-C bondforming reaction is highly dependent upon the ratio of the mixed solvent. JO004032G 10.1021/jo004032g Published on Web 10/21/2000