laboratory press

token such students do not re- quire being reminded that “the classical approach to filtration depends on the use of filter paper mounted inside a f...
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ANALYTICAL CHEMISTRY

Circle No. 2116 on Readers' Service Card

Practical experiments are included to illustrate each analytical technique and these are well selected; questions and problems a t the end of the various chapters also have been well selected and should be very beneficial to the student using this text. The introductory chapter to this book is, I think, poorly geared to the students for whom the text is intended ; it is, for example, quite unnecessary to devote major emphasis (and type space) to a discussion of techniques for measuring mass and volume, in a text intended for advanced students; by the same token such students do not re­ quire being reminded that "the classical approach to filtration depends on the use of filter paper mounted inside a fil­ tering funnel" (p. 35) ! The book is overlong. It is inexcusable to include separate chapters on "Acid-Base Titra­ tions and pH" and on "Acidimetry and Alkalimetry" in this book; much space could be saved by combining these chapters. There is no uniformity of approach in this book; detailed treat­ ment is given of theoretical aspects of acid-base analysis but essentially no at­ tention is given to the theoretical as­ pects of redox procedures. It. is puz­ zling, to say the least, why the contrib­ utor of the chapter on "Acidimetry and Alkalimetry" laboriously defines such terms as "titration," "end point," and "equivalent weight" for the relatively advanced students for whom the book is intended. It is also difficult to justi­ fy the use of space to illustrate a set-u~p for column chromatography on page 431 which is essentially identical to that depicted on page 370. The book seems relatively free of factual errors, but the statement that "ultraviolet radiation is thus seen to fa­ cilitate transitions between vibrational and rotational energy levels of different electronic levels . .." (p. 432) is unac­ ceptable; similarly, the representation of the structure of an aldehyde-sodium bisulfite adduct on page 455 is not cor­ rect. This reviewer found several errors of a typographical and/or grammatical nature in this text. For example, "Whasman" filter papers (footnote p. 53), "Miker" flame (p. 55), "quarternary" ammonium halides (p. 237), a resonance "phenomena" (p. 434). On page 414 the sentence, "Butyro-reading to refractive index conversion tables may be seen in previously mentioned references" is meaningless to this re­ viewer. On page 323, in the statement " . . . the acetylene procedure can be de­ termined gasometrically," one should undoubtedly read "production" for "procedure." This book is a mixed bag; with the