Analytical Division Meets at St. Louis

Analytical Division Meets at St. Louis 139th National ACS Meeting to be held in two parts, March 22 to 25 and March 27 to 30. Analysts have heavy schedule DIVISIONAL MEETINGS—All sessions to be held in Kiel A g r i c u l t u r a l and Food Chemistry A N A L Y T I C A L CHEMISTRY M a r c h 2 2 t o 2 5 ^ ^ Μ · ^ Chemistry Cellulose Chemistry Chemical Marketing and Economics Fuel Chemistry History of Chemistry Industrial and Engineering Chemistry O r g a n i c C o a t i n g s and Plastics Chemistry Petroleum Chemistry Polymer Chemistry

HE 139TH NATIONAL ACS MEETING is a split meeting, as

T was the case at Cleveland

in 1960. The Division of Analytical Chemistry, together with 10 other Divisions (set forth in box) will meet during the period Wednesday, March 22 through Saturday noon, March 25. Nine other divisions will meet from Monday, March 27, through Thursday, March 30. The complete program appears in the February 13 issue of Chemical and Engineering News. Technical sessions will all be held in the Kiel Auditorium. Registration facilities will be located in the Kiel Auditorium, the Sheraton-Jefferson, and Statler-Hilton Hotels. The Kardex file of registrants will be at the Kiel Auditorium. The Employment Clearing House will also operate in the Kiel Auditorium from March 21 through March 30. Analytical Division Program. Symposia honoring recipi ents of the Fisher Award in Analytical Chemistry, the Sar gent Award in Chemical Instrumentation, and the Labline Award in Chromatography and Electrophoresis will high light the diversified program scheduled for the Division of Analytical Chemistry. A total of 15 half-day sessions are scheduled. The Wednes day morning sessions will be devoted to the Fisher Award Symposium honoring Dr. Herbert A. Laitinen, University of Illinois. The Wednesday afternoon session will be a sym posium honoring the Sargent Award winner Dr. Marcel J. E. Golay of the Perkin-Elmer Corp. There will be a half-day joint symposium on Thursday morning with the Division of Agricultural and Food Chem istry on Physico-Chemical Methods for Quality Evaluation. Another joint symposium, with the Division of Petroleum Chemistry, will be held on Thursday morning and afternoon on the subject of Gas Chromatography. A Symposium on the Analysis of High Polymers is sched uled for Thursday afternoon and Friday morning. A one-day symposium, to be held on Friday, will deal with Selective Separations by Differential Migration Meth ods. This is in honor of Dr. Η. Η. Strain, recipient of the Labline Award in Chromatography and Electrophoresis. A three-session symposium on Analysis via Functional Groups will start on Friday morning and run through Satur day noon. General Sessions are scheduled for Thursday morning, Friday afternoon, and Saturday morning. The Divisional Dinner will feature as speaker Edward M. Flesh, McDonnell Aircraft Corp. His topic will be "The Challenge of Space." This affair will be held at 6:30 p.m. Thursday, March 23, at the Statler-Hilton Hotel, Missouri Room. 52 A

·

ANALYTICAL CHEMISTRY

March 27 to

Auditonum Biological Chemistry Chemical Education 30 Chemical Literature C o l l o i d and Surface Chemistry Inorganic Chemistry M e d i c i n a l Chemistry O r g a n i c Chemistry Physical Chemistry W a t e r and W a s t e Chemistry

The Divisional business meeting will be held at 4:30 p.m., Thursday, March 23, at the Kiel Auditorium, Assembly Hall 4. Special Events. The General Mixer for the first half of the meeting will be held at the Statler Hilton Ballroom on Thursday, March 23. The Mixer for the second half will be held on Monday, March 27, at the Sheraton-Jefferson Hotel Mezzanine. The General Meeting will be held on Monday, March 27, at the Sheraton-Jefferson Hotel. Priestley Medalist Dr. Louis P. Hammett will present the Award Address "Choice and Change in Scientific Communications." Awards of interests to analytical chemists to be presented at the general meeting include Fisher Award in Analytical Chemistry to be given to Dr. H. A. Laitinen, the ACS Award in Chemical Instrumentation, sponsored by Ε. Η. Sargent & Co., to Dr. Marcel J. E. Golay and ACS Award in Chromatography and Electrophoresis, sponsored by Lab line, Inc., to Dr. Harold H. Strain. Several plant trips have been scheduled. The list of these appears in Chemical and Engineering News, February 13 issue (page 92). The program of the Division of Analytical Chemistry and joint sessions with the Divisions of Petroleum Chemis try and Agricultural and Food Chemistry appear below.

PROGRAM C . N . REILLEY,

Chairman

L. B. ROGERS,

Secretary

Wednesday M o r n i n g , March 22 Kiel A u d i t o r i u m , Assembly H a l l 4 (3rd Floor, 15th St. Entrance) FISHER A W A R D S Y M P O S I U M H O N O R I N G HERBERT A . L A I T I N E N Henry F. Holtzclaw, Jr., Presiding

9:00 Introductory Remarks. H. F. Holtzclaw, Jr., Univer sity oj Nebraska. 9:05 Thermodynamic Constants of Complex Ion Formation Between Hg(II) and Three Alkylamines. D. K. Roe, Shell Development Co., D. B. Masson and C. J. Nyman, Washington State University. 9:20 Study of the Molybdenum Catalyzed Reduction of Perchlorate. G. A. Rechnitz and H. A. Laitinen, University oj Illinois.

9:35

10:00

10:15 10:30 10:55 11 :05

Complex Ion Formation of Mercury (II) Ion and Thiosulfate Ion. C. J. Nyman, Washington State Univer sity, and Teresa Salazar, Bogota, Columbia, South America. Measurement of Separability of Praseodymium and Neodymium by Electrolysis at Amalgam Cathodes in Aqueous Electrolytes. E. I. Onstott, Los Alamos Scientific Laboratory. Electroanalytical Techniques in Molten Lithium Sul fate—Potassium Sulfate. C. H. Liu, Polytechnic In stitute of Brooklyn. An Interpretation of Electrode Reaction Capacitance. C. G. Enhe, Princeton University. Introduction of Herbert A. Laitinen, Fisher Award Winner. / . M. Kolthoff, University oj Minnesota. Electroanalytical Chemistry of Surface Monolayers. H. A. Laitinen, University oj Illinois.

Wednesday Afternoon

11:20

Investigation of the Kinetics and Mechanism of the Anodic Oxidation of Aniline in Aqueous Sulfuric Acid Solution at a Platinum Electrode. D. M. Mohilner, Louisiana State University, W. J. Argersinger, Jr. and R. N. Adams, University of Kansas. 11:40 Tritium Tracers in Anodic Oxidation Studies. Part I. Oxidation of iV,iV-Dimethylaniline. T. Mizoguchi, R. M. White, H. Y. Lee, F. S. Rowland, and R. N. Adams, University of Kansas.

Thursday Morning SECTION Β Kiel Auditorium, Assembly Hall I (2nd Floor, 14th St. Entrance) SYMPOSIUM O N GAS

CHROMATOGRAPHY

Kiel Auditorium, Assembly Hall 4

JOINT WITH DIVISION OF PETROLEUM CHEMISTRY

(3rd Floor, 15th St. Entrance)

R. A. Dinerstein, Presiding

SARGENT A W A R D SYMPOSIUM O N C H E M I C A L INSTRUMENTATION H O N O R I N G MARCEL J . E. GOLAY Van Zandt Williams, Presiding 2:00

Introductory Remarks. Van Zandt Williams, The Perkin-Elmer Corp. 2:05 How Golay Works. J. G. Alwood, The Perkin-Elmer Corp. 2:25 Our Present Understanding of the Gas Chromatographic Process. M. J. E. Golay, The Perkin-Elmer Corp. 3:15 Limitations of Spectroscopic Measurements. John Strong, Johns Hopkins University. 3:50 T h e Use of a Permanent Magnet in High Resolution Nuclear Magnetic Resonance Spectroscopy. Rex Rich ards, Lincoln College, Oxford, England. 4:25 T h e Column in Gas Chromatography. W. W. Brandt, Purdue University.

Thursday Morning

9:00

Introductory Remarks. R. A. Dinerstein. American Oil Co. 9:05 Efficiency of Solvents in Gas Chromatography Cor related with Interaction Forces. Η. Μ. McNair, Esso Research and Engineering Co., and Thomas De Vries, Purdue University. 9:20 Choice of a Substrate in a GLC Separation through Application of the Theory of Solutions. D. E. Martire, Stevens Institute of Technology. 10:05 Evaluation of a Commercial Dye as the Liquid Phase in the Gas Chromatographic Separation of Nitrogen Compounds. C. R. Ferrin, D. R. Latham, and W. E. Haines, U. S. Bureau of Mines. 10:30 Determination of Small Amounts of n-Paraffins by Molecular Sieve-Gas Chromatography. F. T. Eggertsen and S. Groennings, Shell Development Co. 11:00 Double-Column Programmed Temperature Gas Chro matography. E. M. Emery and W. E. Koerner, Mon santo Chemical Co. 11:30 Application of Gas Chromatography to the Analysis of Thermal Degradation Products of Hexadecane. J. Aim, J. L. Driscoll, W. R. Smith, and B. J. Gudzinowicz, Monsanto Chemical Co.

SECTION A

9:00


Thursday Morning


SECTION C

GENERAL

Kiel Auditorium, Committee Room 4C

Charles N. Reilley, Presiding

(4th Floor, 15th St. Entrance)

Introductory Remarks. C. N. Reilley, University of North Carolina. 9:05 Potentiometric Determination of Bromide Ion. R. T. Pflaum and J. O. Frohliger, State University of Iowa. 9:25 Buffer Capacity Titrations. Joseph Glickstein and Bar bara Hunter, Adelphi College. 9:45 An Incremental Approach to Derivative Polarography. Clemens Auerbach, H. L. Finston, and George Kissel, Brookhavpn National Laboratory, and Joseph Glick stein, Adelphi College. 10:05 Determination of Nitrate by Controlled Potential Coulometry. L. R. Duncan, General Electric Co. 10:40 Influence of Structure on the Polarographic Stability of Organic Mercurials. Sister M. L. O'Donnell and C. W. Kreke, Mount Mercy College. 11:00 Voltammetric Studies of Phenol and Aniline Ring Substitution. J. C. Suatoni, R. E. Snyder, and R. O. Clark, Gulf Research and Development Co.

SYMPOSIUM O N PHYSICO-CHEMICAL METHODS FOR FOOD QUALITY EVALUATION JOINT WITH

DIVISION OF AGRICULTURAL FOOD CHEMISTRY

AND

A. Cornwell Shuman, Presiding 9:00 9:05 9:35 10:05 10:35

Introductory Remarks. A. C. Shuman, Shuman Chemi cal Laboratories, Inc. Gas Chromatography in Evaluation of Foods. D. A. M. Mackay and Murray Berdick, Evans Research and Development Corp. Determination of Fluid Foods Shear Strength and Its Influence on Coating Behavior. S. E. Charm, Massa chusetts Institute of Technology. Spectrophotometry Techniques for Measuring Food Quality. K. H. Norris, U. S. Department oj Agriculture. Electrophoresis of Milk Proteins in Their Natural E n VOL 33, NO. 3, MARCH 1961

·

53 A

MEETING PROGRAM

Automatic Protein

11:05

vironment, a Possible Approach to the Study of P r o tein Stability. R. McL. Whitney, University of Illinois. Nuclear Magnetic Resonance Spectroscopy as a Tool for Food Quality Evaluation. W. E. Baltinger, Purdue University.

and/or

Peptide Analyses

Thursday A f t e r n o o n

SECTION A

(Either Individual Samples or Column Effluent)


Quantitate...

(3rd Floor, 15th St. Entrance) SYMPOSIUM O N ANALYSIS OF H I G H POLYMERS

Total Nitrogen by Kjeldahl Total Protein by Biuret Total Protein by Folin—Ciocalteau (Lowry modification) Amino Groups by Ninhydrin Tyrosine by Folin—Ciocalteau Histidine by Pauly Diazo Reaction Arginine by Sakaguchi Glutamic Acid by Decarboxylase Lysine by Decarboxylase Albumin by H A B A Dye [2-(4' hydroxyazobenzene) benzoic acid]

J. Mitchell, Jr., Presiding 2:00

Introductory Remarks. J. Mitchell, Jr., E. I. du Pont de Nemours & Co., Inc. 2:10 Analytical Aspects of Resinography, Especially the Architecture of High Polymers. T. G. Rochow, Ameri can Cyanamid Co. 2:45 Recent Advances in Determining Polymer Molecular Weights. F. W. Billimeyer, Jr., E. I. du Pont de Nemours & Co., Inc. 3:20 Polymer Fractionation by Column Methods. TV. S. Schneider, USA. Quartermaster Research and En gineering Center. 3:45 Differential Thermal Analysis. Bacon Ke, Standard Oil Co. (Indiana). 4:30 Business Meeting. Division of Analytical Chemistry. 6:30 Divisional Dinner—Statler Hilton Hotel. "The Chal lenge of Space" by Edward M. Flesh of McDonnell Aircraft Corp.

Analyze...

Thursday Afternoon

Biological Fluids directly

SECTION Β Kiel Auditorium, Assembly Hall I

Effluent from D E A E or Resin Chromatographic Column Effluent from Poraeth Electrophoretic Column

(2nd Floor, 14th St. Entrance) SYMPOSIUM O N GAS CHROMATOGRAPHY

Electrophoretic Starch Block Fractions

JOINT WITH DIVISION OF PETROLEUM CHEMISTRY

Electrophoretic Paper Chromatogram Segments

W . D. C o o k e ,

Check point stages in Protein Fractionation Counter Current Distributions with

the

TECHNICON®

Any or all of these determinations may be run on the same Auto Analyzer: Takes only two minutes to change from one type of analysis to another. Any combination may be run simultaneously from t h e same sample by adding additional standard AutoAnalyzer modules. T h e response time is such that most of the analyses may be run at 4 0 samples per hour. for information, select area of interest and write to

TECHNICON CHROMATOGRAPHY CORP. 52 R E S E A R C H P A R K · CHAUNCEY, N E W Y O R K

Circle No. 191 an Readers' Service Card

54 A

·


Presiding

Introductory Remarks. W. D. Cooke, Cornell Univer sity. 2:05 Evaluation of the Flame-Ionization Detector and the Micro Argon /3-Ray Detector. Η. Μ. McNair, Esso Research and Engineering Co., K. A. M. G. Cramers and A. I. M. Keulemans, Technical University, Eind hoven, Netherlands. 2:25 Quantitative Aspects of Capillary Gas Chromatography of Hydrocarbons. L. R. Durrett and I. Dvoretzky, Shell Oil Co., and M. C. Simmons, Barber-Colman Co. 3:05 Investigation of the Linearity of a Stream Splitter for Capillary Gas Chromatography. L. S. Ettre and W. Averill, The Perkin-Elmer Corp. 3:25 Low Temperature Gas-Liquid Chromatography. R. S. Porter and J. F. Johnson, California Research Corp. 3:45 Determination of Volatile Hydrocarbons in Aqueous Emulsions and Latexes by Gas Chromatography. F. M. Nelsen, F. T. Eggertsen, and J. J. Hoist, Shell De velopment Co. 4:15 Preparative Separation of Sex Hormones by Gas Chromatography. E. C. Jennings, Jr., and K. P. Dimick, Wilkens Instrument and Research, Inc. 4:35 Gas Chromatography. IV. The Thermodynamics and Kinetics of the Alcoholysis of Acetals. R. S. Juvet, Jr. and Jen Chiu, University of Illinois. 2:00

NOW from...

Friday M o r n i n g

JARRELL-ASH

SECTION A Kiel A u d i t o r i u m , Assembly H a l l 4 (3rd Floor, 15+h St. Entrance) SYMPOSIUM O N ANALYSIS OF H I G H J . M i t c h e l l , Jr.,

POLYMERS

Presiding

9:00

Introductory Remarks. J. Mitchell, Jr., E. I. du Pont de Nemours & Co., Inc. 9:05 X - R a y Characterization of Polymers by Means of a Crystallinity Index. W. O. Station, E. I. du Pont de Nemours & Co., Inc. 9:35 Chemical Structure by Absorption Spectroscopy. J. P. Luongo, Bell Telephone Labs. 10:10 Determination of Molecular Orientation in Polymer Films by Infrared Spectrophotometry. J. A. Gailey, Hercules Powder Co. 10:40 Pyrolysis Techniques. D. A. Vassallo, E. I. du Pont de Nemours & Co., Inc. 11:15 The Role of Carbon-14 Tagged Standards in the Anal ysis of Acrylonitrile-Vinyl Acetate Copolymers. M. E. Gibson, Jr., and R. H. Heidner, Chemstrand Research Center. 11:45 Chemical Analysis of Polymers. F. E. Critchfield, Union Carbide Chemicals Co. Friday M o r n i n g

• Separate heaters and temperature controls for injector block, oven and detector.

SECTION Β Kiel A u d i t o r i u m , C o m m i t t e e Room C (2nd Floor, 15th St. Entrance) S Y M P O S I U M H O N O R I N G Η. Η. STRAIN AS RECIPIENT O F T H E LABLINE, I N C . A W A R D I N C H R O M A T O G R A P H Y A N D ELECTROPHORESIS S E L E C T I V E S E P A R A T I O N S BY D I F F E R E N T I A L MIGRATION METHODS W . M . Manning,

Presiding

9:00

Introductory Remarks. W. M. Manning, Argonne Na tional Laboratory. 9:05 Hydrogénation of Linolenate. V. Comparison of Products from Triglyccryl- and Monomethyl-esters. C. R. Scholfield, E. P. Jones, and H. J. Button, Northern Regional Research Laboratory. 9:25 Silica Gel Structure and the Chromatographic Process. P. D. Klein, Argonne National Laboratory. 9:45 Role of Porous Support Media in Differential Migration Methods. J. C. Giddings, University of Utah. 10:05 Separation of Biologically Active Materials by Countercurrent Distribution. E. M. Bickoff, Western Regional Research Laboratory. 10:25 Electrochromatography in the Fractionation of Biological Systems. Arthur Karler, N. V. Carroll, and R. C. Batterman, Institute for Clinical Pharmacology and Medical Research. 11:00 The Basis of Selectivity in Chromatography, Electrochromatography, and Continuous Electrochromatography. / / . / / . Strain, Argonne National Laboratory.

SECTION C Kiel A u d i t o r i u m , C o m m i t t e e Room 3D (3rd Floor, 15th St. Entrance) on page 56

• Column oven accommodates a variety of high efficiency columns. • Columns may be quickly and easily changed. • Separately heated injection block for " f l a s h " vaporization of sample from room temperature to 350° C. • Convenient micrometrically adjustable sample splitter divides the sample into reproducible ratios. • Column oven may be* maintained within 0.5° C with boost control for rapid heating or temperature programming to 250° C. • Detector may be set for any temperature range from room to 250° C. • It is available with a choice of interchangeable detectors: micro argon diode and triode detectors with choice of Ra 226, Sr 90 or tritium emitters; flame; even the experimental electron capture detectors are available for interchangeable use in the detector mount. • This latest Jarrell-Ash contribution to the field of gas chromatography is now priced for even the most modest laboratory budget. All of the Jarrell-Ash detectors, ovens, injection blocks, columns, sample splitters etc., are available as separate components for those who may wish to modify or modernize existing equipment or assemble their own chromatographs. For those engaged in the study of lipid metabolism or fatty acid chemistry, remember that our W. G. Pye Argon Chromatograph is the standard instrument for this work. Write us today for further information on the equipment or component that suits your needs.

Jarrell J A R R E L LAsh -ASH

Friday M o r n i n g

{Continued

Compare the features of the Jarrell-Ash GLC-6 Chromatograph with any other. You'll see that it offers the latest proven advances in chromatography.

A)

COMPANY

2 6 Farwell Street, Newtonville 6 0 , M a s s a c h u s e t t s COSTA MESA, CALIF. ATLANTA, GEORGIA DEARBORN, MICHIGAN SAN MATEO, CALIF. PITTSBURGH, PENN. NEW BRUNSWICK, N. J. LOMBARD (CHICAGO) ILL. DALLAS, TEXAS TORONTO, CANADA ZURICH, SWITZERLAND Circle No. 191 on Readers' Service Card VOL. 3 3 , N O . 3, MARCH 1961

·

55 A

MEETING PROGRAM

(Continued

from page 55 A)

SYMPOSIUM O N ANALYSIS VIA FUNCTIONAL GROUPS J. S. Fritz, Presiding 9:00

Introductory Remarks. / . S. Fritz, Iowa State Univer sity. 9:05 The Role of Separations in Organic Analysis. L. D. Metcalfe, Armour and Co. 9:45 Indirect Acid-Base Methods. F. E. Critchfield, Union Carbide Chemicals Co. 10:40 Oxidation-Reduction Methods. K. G. Stone, Michigan State University. 11:20 Nonaqueous Acid-Base Titrations. J. S. Fritz, Iowa State University.

Friday Afternoon SECTION A Kiel Auditorium, Assembly Hall 4 (3rd Floor, 15th St. Entrance) GENERAL Samuel M. Tuthill, Presiding 2:00

DIRECT READING... NO VERNIERS ON

VDF MICRO TORQUE BALANCES VDF Micro Torque Balances are widely used in science and industry for repetitive weighings of small samples. These balances are extremely fast, yet accurate and simple to oper ate. Service requirements are negligible due to the absence of moving parts, bearings, springs and other complicated mechanisms. Select from 14 different models,- all at surpris ingly low, economy prices. SPECIAL FEATURES: • No bearings—no friction • Combined torsion/suspension wire • No delay in reading, oscillation stops instantly • Direct reading, no reading errors • No fatigue, dial at eye level is adjustable • No parallax—special straight view pointer • Considerable overload tolerance For descriptive literature write for Bulletin 66

Introductory Remarks. S. M. Tuthill, Mallinckrodt Chemical Works. 2:05 Resolution in Programmed Temperature Gas Chroma tography. J. F. Fryer and H. W. Habgood, Research Council of Alberta, and W. E. Harris, University of Alberta. 2:25 Fluorescent Indicator Adsorption (FIA) Analysis of Gasoline on Partially Deactivated Silica Gel Columns. T. A. Norris, J. H. Shively, and C. S. Constantin, Texaco Research Center. 2:45 Iron-55 X - R a y Absorption Analysis of Organically Bound Chlorine Using Conventional Proportional Counting Facilities. L. H. Griffin, Shell Chemical Co. 3:20 Assay of ρ,ρ'-Bisphenol-A by Isotope Dilution Analysis. L. Ή. Griffin, Shell Chemical Co. 3:40 Determination of Resorcinol in Gamma Irradiated Phenol Solutions. Maurice Codell and Leonard Teitell, Frankford Arsenal, and Edgar Howard, Jr., Temple Uni versity. 4:00 Ultraviolet Spectrophotometric Determination of Benzoic Acid in Refined Phthalic Anhydride. Raita Murnieks and C. E. Gonter, Pittsburgh Chemical Co. 4:20 Colorimetric Determination of Naphthylamines. H. O. Spauschus, General Electric Co.

Friday Afternoon SECTION Β Kiel Auditorium, Committee Room C (2nd Floor, 15th St. Entrance) SYMPOSIUM H O N O R I N G Η. Η. STRAIN AS RECIPIENT OF THE LABLINE, I N C . AWARD IN CHROMATOGRAPHY AND ELECTROPHORESIS MODIFICATIONS AND APPLICATIONS OF DIFFERENTIAL MIGRATION METHODS

BRINKMANN

2:00

INSTRUMENTS, INC.

2:05

115 Cutter Mill Road, Great Neck, N.Y. Philadelphia · Cleveland · Houston · Miami · Menlo Park, Cal. Circle No. 37 on Readers' Service Card 56 A

·


R. F. Buchanan,

Presiding

Introductory Remarks. R. F. Buchanan, Argonne Na tional Laboratory. Recent Work on Centrifugally Accelerated Chromatog raphy and Planar Electrophoresis. H. J. McDonald, Loyola University.

2:25 2:45 3:05 3:25 4:00 4:20

4:40

Separation of Amino Acids on Ion-Exchange Resin Paper. M. M. Tuckerman, Temple University. Chromatography of Macro-molecules of Biological Origin. H. A. Sober and E. A. Peterson, National In stitutes oj Health. Experience in the Purification of Protochlorophyll Holochrome by Differential Migration Methods. J. II. C. Smith, Carnegie Institution of Washington. The Radiochromatography Method. A. A. Benson, Pennsylvania Slate University. Theory of Ion Solvation. I I . Spectral Investigation of Electrolyte Solvation in Acetonitrile. E. R. Night ingale, Jr., Esso Research and Engineering Co. Continuous Separation of Gaseous Mixtures by Ther mal Gravitational Diffusion. / / . H. Strain, II. D. Frame. Jr., J. R. Kuszewski, and J. F. Binder, Argonne National Laboratory. Selective Absorption of Various Phosphorus Compounds by Chlorella pyrenoidosu. T. R. Sato, Argonne Na tional Laboratory.

Eliminate M a n y o f Y o u r Vacuum Problems W i t h — ®

Kinney

HIGH

V A C U U M VALVES GLOBE TYPE VACUUM VALVES Of advanced design, these Se ries BB Valves are preferred for application with brazed or soldered manifolding. Bellows a s s e m b l y e a s i l y removed for cleaning without disturbing con nections. Sizes 1" to 3"—manual and air operated models. Write for Bulletin 3421.1A

Friday Afternoon SECTION C Kiel Auditorium, Committee Room 3D (3rd Floor, 15th St. Entrance) SYMPOSIUM O N ANALYSIS VIA FUNCTIONAL GROUPS

BRONZE BELLOWS SEALED VACUUM VALVES Widely used at low absolute pres sures developed by KINNEY Me chanical High Vacuum Pumps. All bronze with Vacuum tight bronze bellows — rising stem de sign. 1" to 3" sizes with American S t a n d a r d Pipe Thread connec tions. \W, 2" and 3" Flanged connections. Write for Bulletin 3420.1

John A. Riddick, Presiding 2:00 2:40 3:20

3:40

4:00 4:20 4:40

Differential Kinetic Analysis. G. S. Hammond, Cali fornia Institute of Technology. Determination of Functional Groups by Absorption Spectroscopy. Sidney Siggia, Olin Matheson Chemical Corp. Acid-Base Titrimetric Characterization of Amino Alcohol-Carboxylic Acid Reaction Products via Func tional Groups. A. L. Baxter and J. A. Riddick, Com mercial Solvents Corp. Evaluation of Amides, Ethers, and Related Compounds as Weak Bases in Acetic Acid. C. H. Barnstein, H ossein Ghassemi, W. E. Perez, and Takeru Higuchi, University of Wisconsin. Alkoxyl Group Determination—A Simplified Procedure. R. II. Cundiff and P. C. Markunas, R. J. Reynolds Tobacco Co. Tetracyanoethylene Chemistry. I. Photometric and Visual Titration of Diels-Alder Active Dienes. Mara Ozolins and G. II. Schenk, Wayne State University. Tetracyanoethylene Chemistry. II. Photometric Complexometric Titration of Aromatic Hydrocarbons. G. II. Schenk and Mara Ozolins, Wayne State Univer sity.

Saturday Morning


Write for Bulletin 3440.1A

KINNEY

VACUUM

AIR B R A K E

COMPANY

3534C W A S H I N G T O N

STREET · BOSTON

30 · MASS.

•

GENERAL

N E W YORK

DIVISION

3421.1A

Π 3400.1

Π 3420.1

Π3440.1Α

Name

William A. Ziegler, Presiding W. A. Ziegler,

GATE VACUUM VALVES These Valves feature minimum flange to flange dimension, maxi mum conductance and very short flow path. Provide seal in either direction . . . sizes through 12" operate under any combination of A t m o s p h e r e / V a c u u m . Handwheel, Toggle a n d Pneumatic operation. Sizes 2" to 32".

P l e a s e s e n d m e the following Bulletins:


Introductory Remarks. Chemical Works.

Write for Bulletin 3400.1

THE

SECTION A

9:00

DIAPHRAGM SEALED VACUUM VALVES Designed to meet the needs for rugged, dependable and inexpen sive Valves operating at pressures of 1 micron or higher. Cast iron Y body . . . neoprene diaphragm and Buna-N valve disc. Sizes W to 6" . . . m a n u a l or pneumatic operation.

Company. Mallinckrodt

Address

City

-Zone.

-State-

Circle No. 13S on Readers' Service Card

VOL. 33, NO. 3, MARCH 1961

57 A

MEETING PROGRAM

NEW high temperature forced draft ovens

9:05

9:25

to 280°C

9:45

10:05

10:40 11:00 11:20 11:40

A Complete Separation of a Mixture of F e ( I I I ) , C o ( I I ) , M o ( V I ) , A l ( I I I ) , and X i ( I I ) by Ion Exchange. Carl Michaelis, University oj Dayton, and N. S. Tarlano, Chemical Abstracts, Columbus, Ohio. Spectrophotometric Determination of Molybdenum in the Presence of Large Amounts of Tungsten by a Thioeyanate Method. H. J. Scim, R. C. Jensen, D. A. Douglass, and T. L. Lambert, University oj Nevada. The Spectrophotometric Determination of Cobalt with Sodium 2-Nitroso-l-naphthol-5-sulfonate. A. L. Caskey, G. E. Brown, D. W. Golightly, Southeast Missouri State College, and V. G. Mossotti, Iowa Stale Univer sity. Spectrophotometric Determination of Cobalt with the p-Nitrophenylhydrazone of Diacetylmonoxine (Cooxime). R. M. Pearson, Aerojet-General, and H. J. Scim, University oj Nevada. The Ultraviolet Determination of Uranium in Concen trated Hydrochloric Acid. C. M. Callahan, U. S. Naval Radiological Defense Laboratory. Chemical Microscopy of the Platinum Metals: R e actions with 4-Bromoisoquinoline and 4-(p-Nitrobenzyl) Pyridine. H. F. Schaeffer, Westminster College. Some Matrix Effects in X-Ray Fluorescence Analysis. Susan Meschel and Donald Rosenthal, University oj Chicago. Flame Spectrophotometric Study of Nickel. / . A. Dean, University oj Tennessee, and H. C. Eshelman, University oj Southwestern Louisiana.

MODEL 1303

Lowest Cost Working Area per cu. ft.

Saturday Morning

With Highest Degree of Uniformity! Through Hotpack's scientific horizontal con vection system, heated air is gently and uniformly «inverted across all shplves (re gardless of load) and throughout entire chamber area. Rear mounted blower motor and perforated side walls assure you abso lute floor to ceiling Circulation and rapid heating! Temperatures are uniform to within • r C .

SECTION Β Kiel Auditorium, Committee Room C (2nd Floor, 15th St. Entrance) SYMPOSIUM O N ANALYSIS VIA FUNCTIONAL GROUPS L D. Metcalfe, Presiding

• 4 cubic feet of useable working space • 3-heat selector switch . . . low, lrfedium, high • polished stainless steel chamber and shelv ing for lasting durability

9:00 9:20

• ball-bearing blower motor pre-lubricated for maintenance-free use • optional LimiUtat control automatically prevents excessive temperatures and darnagtOviui» feature Hotpack's recessed, illumi nated control panel with safety plexiglass cover! For complete

Laboratory oven write today:

brochure,

9:40

10:00

10:20 10:40

OVENS

SAFETY OVENSt

[FURNACES

11:00 11:20 11:40

THE ELECTRIC HOTPACK CO., INC. 5077 COTTMAN AVENUE · PHILA. 35, PA. circle NO. 176 on Keaoers1 service Caro

58 A

•


Determination of Aldehydes in Aromatic Acids and Anhydrides. K. E. Lorentzen, R. H. Wise, and F. J. Piehl, American Oil Co. Titrimetric Determination of Small Amounts of Alde hydes and Ketones. J. E. Ruch, J. B. Johnson, and F. E. Critchfield, Union Carbide Chemicals Co. Rapid Determination of Organic Hydroxyl Groups with 3,5-Dinitrobenzoyl Chloride. W. T. Robinson, Jr., R. H. Cundiff, and P. C. Markunas, R. J. Reynolds Tobacco Co. Determination of Small Amounts of Tertiary Amines in the Presence of Primary and Secondary Amines. J. E. Ruch and F. Ε. Critchfield, Union Carbide Chemicals Co. Spectrophotometric Determination of Secondary Amines. G. R. Umbreit, The Upjohn Co. Water Determination with 2,2-Dimethoxypropane. F. E. Critchfield and Ε. Τ. Bishop, Union Carbide Chemi cals Co. Analysis of Some Organic Derivatives of Hydrazine. W. R. McBride and W. M. Ayres, U. S. Naval Ordi nance Test Station. Chemical Aspects of Oxirane Oxygen Analysis. A. J. Durbetaki, Food Machinery and Chemical Corp. Spectrophotometric Determination of Aliphatic Alde hydes. A. M. Albrecht, W. I. Scher, Jr., and H. J. Vogel, Institute of Microbiology, Rutgers, The State University.

Analytical Division Meets at St. Louis

Recommend Documents