APPLIED RESEARCH LABORATORIES, INC. - ACS Publications

May 17, 2012 - APPLIED RESEARCH LABORATORIES, INC. Anal. Chem. , 1961, 33 (7), pp 102A–102A. DOI: 10.1021/ac60175a763. Publication Date: June ...
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INSTRUMENTATION

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102 A



ANALYTICAL CHEMISTRY

engineered for production. This is a development, which will be watched with interest by all microanalysis. B o i l e r W a t e r . Some time ago we described the extraordinary means which are employed to assure the p u r i t y of boiler teed water in modern power plants, mid had referred to t h e work of W . A. Crandall in this connection. I t was therefore rewarding to hear his discussion on the opening day on a pilot plant for analytical instrumentation. These determinations are all automatic and must possess a high degree of pre­ cision and reliability. T h e importance of reliability cannot be overestimated because "down-time" on boilers or t u r ­ bines can b e disastrously expensive. T h e research analyst is likely to dismiss this sort of boiler chemistry as some­ thing crude a n d n o t in t h e same class as his careful researches. T h e simple fact is t h a t few analysts have ever seen or used distilled water as pure as t h a t required in huge quantities in a modern high pressure boiler. Impurities such as oxygen, silica, etc., must be known and k e p t in t h e p a r t p e r billion range, and a n y mistakes or even short term fluctuations can be ruinous. G a s C h r o m a t o g r a p h y . Progress in gas c h r o m a t o g r a p h y can now b e fol­ lowed only b y t h e experts because there a n ; so m a n y aspects of t h e tech­ nique. T h e several concurrent sessions emphasized this. Despite widespread applications in all fields, there is still intensive research on improved detec­ tors, better columns, t h e recording a n d integration of peaks, d a t a collation a n d ret riev.nl. I t ' s all a very long way from weigh­ ing barium sulfate precipitates or titrating hydrochloric acid. We begin to feel sorry for the analytical student of tomorrow in contemplation of all he will have to learn. Exhibits. T h e exhibit of instru­ ments was meager, b u t choice. This was not a national meeting, where t h e displays are vast, b u t devoted primarily to t h e limited purpose of the sym­ posium. In future columns we hope to describe; some of t h e newer instru­ ments which were exhibited. T h e ollic.ers of t h e Analysis I n s t r u ­ mentation Division of t h e I .S.A. a r e to he congratulated for their efforts in this seventh symposium, particularly M . D . Weiss of Union Carbide Olefins, 1!. D . lianes of Leeds & N o r t h r u p , T . J . Kehoe of Beckman I n s t r u m e n t s , a n d R. V. Wall of Monsanto. Among t h e many competent experts who con­ tributed to t h e program, it was pleasant to hear again from such progressive analysts well known to readers of A N A ­ LYTICAL C I I K M I S T K Y as W a y n e

Karle Serfass and Roger Bates.

Meinke,