PARR INSTRUMENT CO. | Analytical Chemistry

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CONFERENCE PROGRAM

PARR

BOMBS

For rapid combustion a n d fusion reactions w i t h sodium p e r o x i d e , a n d for other laboratory purposes AC2E

11:40

A1ACD

AC4E

AC4E

10:05 10:20

11:10

A116AC

42 ml.

A2AC4

45 ml.

2:00 2:20

2:40 3:00 3:20 3:40 4:00 4:15

4:35

This bomb is the same as AC3E except the cup is 3 % " deep to provide a 45 ml. in­ ternal volume. Cups of stain­ less steel, 94% n i c k e l a n d 99+% nickel are available.

A2AC4

A2AC3

A2AC3

A1MB A1MB

2.5 ml.

This is the smallest of the several Parr peroxide bombs. It has a 94% nickel cup and cover, and is used for treating micro samples.

Ask your PARR Dealer for details, or write

PARR

INSTRUMENT

direct

CO.

1:30 1:50 2:05 2:25 2:45 3:05 3:20

MOLINE, ILLINOIS

3:40 Circle No. 142 on Readers' Service Card 82

A

·

ANALYTICAL CHEMISTRY

(153) Design and Application of Continuous Recording Flame Photometer. J. L. WATERS, Waters Associates. (154) Multi-Channel Flame Spectrometer for Analysis of Biological Fluids to Determine Magnesium, Calcium, Potassium, and Sodium. T. G. ARNOLD, JR., Vanderbilt University Medical School. (155) Chemiluminescent Flame Spectrophotometry. P. T. GILBERT, J R . , Beckman Instruments, Inc. (156) Factors Affecting Excitation in Flame Spectros­ copy. J. H. GIBSON and W. D. Cooke, Cornell Uni­ versity. EXPOSITION RECESS. (157) Direct Flame Spectrophotometric Analysis of Low-Alloy and Stainless Steels. C. A. WAGGONER and M. C. L. Gerry, Pacific Naval Laboratory. (158) Phosphorus Determination by Flame Photometry. F. J. Dinan, A. DAVIS, and L. E. Tufts, Hooker Chemical Corp. (159) Flame Photometric Determination of Phosphorus in Presence of Sodium, Potassium, and Other Cations. D. N. BERNHART, W. B. Chess, and D. Roy, Stauffer Chemical Co. (160) Turbidity Effect in Spectrum Line Photometry. A. ARRAK, Grumman Aircraft Engineering Corp.

INFRARED SPECTROSCOPY—GENERAL Thursday Afternoon—Pittsburgh Room D. S. McKinney, Presiding

8 ml.

This bomb is similar to AC3E except it has a smaller cup with a hemispherical bottom. Sodium peroxide reactions are started by heating with a gas torch. T h e cup is 94% nickel.

Introductory Remarks—W. R. BRODE. (150) Optical and Infrared Masers. CHARLES TOWNES, Institute for Defense Analyses. E X P O S I T I O N RECESS. (151) Spectroscopic Studies in the Thermonuclear Field at the Oak Ridge National Laboratory. J. R. MCNALLY, JR., P. M. Griffin, W. P. Peed, W. R. Skidmore, and G. K. Werner, Oak Ridge National Laboratory. (152) New Frontiers of Astronomical Optics. A. B. M E I N E L , Kitt Peak National Observatory.

EMISSION SPECTROSCOPY—FLAME PHOTOMETRY AND SPECTRUM LINE PHOTOMETRY Thursday Afternoon—Terrace Room William J. Feingold, Presiding

22 ml.

This bomb has a plain cover without electrodes. It is used for sodium peroxide reactions which can be started by heat­ ing with a gas torch. Cups of 94% Ni, 36% Ni, 9 9 + % Ni, carbon steel and stainless steel are available. This bomb is similar to AC2E except all parts are larger and heavier than in the 22 ml. bomb. It will accommo­ date samples twice as large as AC2E and AC3E.

A I T6AC

9:10 9:15

22 ml.

This bomb is similar to AC2E except it has a gas connection for purging with an inert gas. It is used with a Parr 1411 calorimeter for measuring the heats of combustion of ther­ mite and other self-burning pyrotechnic mixtures.

AC3E

AC3I

NEW FRONTIERS IN OPTICS AND SPECTROSCOPY Thursday Morning—Ball Room Wallace R. Brode, Presiding

22 ml.

This bomb is the same as AC2E except it has a 5-inch stem for use in the Parr per­ oxide bomb calorimeter. It is used for measuring heats of combustion, also for chemical analyses following calorimetric tests.

A1ACD

Spectroscopists. T. A. HALE, Eastman Kodak Co. (148) Ratio Recording Infrared Spectrophotometer for Measurement at High Sample Temperatures. G. T. KEAHL and D. G. Rea, Beckman Instruments, Inc. (149) Design and Performance of New Infrared Prism Spectrophotometer for the Cesium Bromide Region. Ε. Ε. BUZZA, Beckman Instruments, Inc.

22 ml.

This is a g e n e r a l - p u r p o s e bomb with electrodes for hot wire i g n i t i o n . It is widely used for determining sulfur, chlorine, p h o s p h o r u s a n d o t h e r elements in a g r e a t variety of c o m b u s t i b l e or­ ganic materials. F u r n i s h e d with a 94% Ni cup and Niplated brass cover. Other cups and covers are available.

AC2E

11:20

(161) Infrared Analysis of Short-Lived, High Tempera­ ture Reaction Intermediates Stabilized at 4° K. L. E. KUENTZEL, Wyandotte Chemicals Corp. (162) Wyandotte—ASTM Punched Card Indexes of Spectral Data—Current Status and New Services. L. E. KUENTZEL, Wyandotte Chemicals Corp. (163) Near Infrared Ν—Η Bands of Primary Aromatic Amines in Chloroform Solution. Κ. Β. WHETSEL, Tennessee Eastman Co. (164) Analytical Aspects of Gas and Vapor Phase In­ frared Spectroscopy. W. F. ULRICH, Beckman Instru­ ments, Inc. (165) Infrared Analysis of Trace Organic Materials in Biological Systems. D. S. EBLEY, DOW Chemical Co. E X P O S I T I O N RECESS. (166) Infrared Microspectrophotometry Using Reflect­ ing Type 6X Beam Condensing Optics in Reference and Sample Beams. M. Sparagana and W. B. Mason, University of Rochester Medical Center. (167) Techniques for Differential Infrared Spectros-