Tenth Detroit Anachem Conference - Analytical Chemistry (ACS

May 17, 2012 - Tenth Detroit Anachem Conference. Anal. Chem. , 1962, 34 (8), pp 47A–55A. DOI: 10.1021/ac60188a740. Publication Date: July 1962...
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ANALYTICAL CHEMISTRY

NEWS

Tenth Detroit Anachem Conference T h e T e n t h Detroit Anachem Con­ ference will be held October 22 to 24 at the McGregor Memorial Center, W a y n e State University. T h e sessions will cover 65 papers on emission, x-ray, a n d flame spectroscopy, analytical a n d electroanalytical bio­ chemistry, atomic absorption spectros­ copy, gas chromatography, analytical absorption spectroscopy, electroana­ lytical chemistry, and general analytical chemistry. The Anachem Conference Address will be given b y H a r v e y Diehl, D e p a r t ­ ment of Chemistry, Iowa State Uni­ versity, who will speak on " T h e W e t Oxidation of Organic M a t t e r with Perchloric Acid." H . H . Willard, Uni­ versity of Michigan, will be Presiding Chairman. D r . Paul K . W i n t e r will receive the Anachem Award for 1962 on Tuesday, October 23. D r . D a v i d F . Boltz, D e p a r t m e n t of Chemistry, W a y n e S t a t e University, is P r o g r a m C h a i r m a n a n d D r . Jack L. Johnson, Research Laboratories, Gen­ eral M o t o r s Corp., 12 Mile and M o u n d

Roads, W a r r e n , Mich., is Registration Chairman.

Managing Editor Leaves A n a l y t i c a l Chemistry

lications, and of associate editor in charge of the Washington News Bureau. F r o m 1948 t o 1954 he wrote a weekly column " P o t o m a c Postscripts" on ac­ tivities of interest to chemists in the different government branches. He also did special editorial work on the F a c t s and Figures issues of Industrial and Engineering Chemistry and the Chemical and Engineering Neios Index. Prior to his ACS work, M r . Gibbs worked for 10 years as a special agent with the F B I at several posts in the U . S. and abroad. M r . Gibbs gradu­ ated with a B.S. in Chemistry from Clark University in 1938 and did p a r t time work a t the George Washington University. M r . Gibbs and his family are moving to Lewes, Del. where he is heading the Gibbs Chemical Co., Inc.

R o b e r t G. Gibbs, managing editor of ANALYTICAL

CHEMISTRY

since

May

1956, has resigned to s t a r t a business of his own. T h e new company will manufacture paints and retail and in­ dustrial finishes including marine t y p e s . M r . Gibbs' association with the ACS included the positions of administrative assistant to the late D r . W a l t e r J. M u r p h y , editorial director, ACS p u b ­

PROGRAM M o n d a y M o r n i n g , O c t o b e r 22 Emission, X-Ray, and Flame Spectroscopy

W. R. O'Neill, Presiding 8:45 Welcome to Conference and Con­ ference Announcements. 9:00 Excitation Processes in Flame Spectroscopy. James H. Gibson, William E. L. Grossman and W. D. Cooke, Department of Chem­ istry, Cornell Universitv, Ithaca, Ν. Ϋ. 10:20 The Determination of Microgram Quantities of Zinc in Paper Chromatograms by X-Ray Fluor­ escence. Bernard E. Nagel, Re­ search Laboratories, General Motors Corp., Warren, Mich. 10:45 Microanalysis on Controlled Spot Test Paper by X-Ray Fluor­ escence, Jack L. Johnson and Bernard E. Nagel, Research Lab­ oratories, General Motors Corp., Warren, Mich. 11:10 Quantitative Analysis with an Electron Microprobe. E. J. Semer and H. A. Domian, Scien­

NMR Symposium T h e Division, of Physical Chemistry, ACS, and the U. S. A r m y Research Office ( D u r h a m ) are cosponsoring a symposium on high resolution N M R spectroscopy at the University of Colorado, Boulder,,July 2 to 4. T h e program consists of 28 invited papers. M a x T . Rogers, Michigan State University, is General Chairman

tific Laboratory, Ford Motor Co.. Dearborn, Mich. 11:35 The Spectrochemical Determina­ tion of Molybdenum and Vana­ dium in Uranium Tetrafluoride. M. G. Atwell and Η. Η. Heller, National Lead Co. of Ohio, Cin­ cinnati, Ohio. 11:55 The Determination of Lithium and Sodium in Aluminum by Flame Photometry. (Utilization of Organic Solvents and Vac­ uum Distillation for Submilligram Amounts.) W. E. Pilgrim, W. R. Ford, and Ε. Μ. Smith, Reynolds Metals Co., Metallurgi­ cal Research Division, Richmond, Va. 12:20 Improved Accuracy in Analysis of Steel Effected by Direct Read­ ing Polychromators. John Schuch and Stanley Smith, Jr., Jarrell-Ash Co., Newtonville, Mass. Monday Morning Analytical Biochemistry Bennie Zak, Presiding 10:20 A Study of the Oxygen Flask Combustion Procedure. C. E. Childs, E. E. Meyers, and Joanne Cheng, Research Laboratory, (Continued on page 4S A)

of the meeting. F u r t h e r details are available from Melvin H a n n a , D e p a r t ­ m e n t of Chemistry, University of Colo­ rado, Boulder, Colo.

PROGRAM Monday Morning Introductory Remarks. M. T. Rogers. A Molecular Orbital Theory of Diamagnetism and Chemical Shifts. J. A. Pople. Chemical Shifts and Electron Densi­ ties. B. P . Dailey. Chemical Shifts and Substituent Ef­ fects in Five-Membered Heteroaromatic Compounds. Sal ο Gronowitz. Monday Afternoon Solvent Effects in N M R . H. J. Bern­ stein. The Estimation and Application of Anisotropy Effects in High-Resolution NMR Spectroscopy. J. H . Goldstein. NMR Determination of Electron Den­ sity Distribution in Aromatic Systems. W. G. Schneider. Application of NMR to the Study of the Stereochemical Configuration of Trifluorochloroethylene Polymers. C. V. D. Tiers and F. A. Bovey. Analysis of Complex NMR Spectra by an Iterative Method. J. W. Swalen. Tuesday Morning Theoretical Interpretation of Spin Coupling. M. Karplus. VOL. 3 4 , N O . 8, JULY 1962

·

Spin-

47

A

NEWS Valence Bond Studies of Internuclear Coupling. H . S. Gutowsky. The NMR and Double Resonance Spectra of Fluorocarbons in the Gas Phase. J. D. Baldesehwieler and G. W. Flynn. Proton-Proton Double Resonance Studies. W. Anderson and R. Freeman. The Relative Signs of FluorineFluorine Coupling Constants. S. Manatt and D. D. Elleman.

NMR Spectra of Acetylene, Ethylene, and Ethane Substituted with Cla Nuclei. X. Sheppard. C u NMR Studies Using the Absorp­ tion Mode. J. N. Shoolery. O17 NMR Spectroscopy. P. Diehl. C13 Studies of Steric Effects on Con­ jugation in Substituted Benzenes. P. C. Luulerbur.

Wednesday Morning

Wednesday Afternoon

Tuesday Afternoon

NMR Relaxation Methods in the Study of Chemical Kinetics. S. Meibooiu. Studies of Six-Membered Saturated Ring Systems by NMR. L. W. Reeves.

Some Measurements of the Proton Resonance Spectra of Paramagnetic Complex Ions in Aqueous Solution. L. Pratt. Determination of Chemical Groups Involved in the Formation of Molec­ ular Complexes from the Differential Broadening of NMR Lines. 0 . Jardetskv. F1" Contact Interaction Shifts: Ef­ fects of Fluorine Conjugation. W. D. Phillips. D. R. Eaton, A. D. Josey, and R. E. Benson. The Structure of Anilinium Salts in Solution. Gideon Fraenkel. Conjugate Acids of Pyrroles and In­ doles. Ε. Β. Whipple.

Some Applications of Nuclear Mag­ netic Resonance in Organic Chemistry. J. D. Roberts.

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ANALYTICAL CHEMISTRY

Use of Remote Deuteration for the Determination of Coupling Constants and Conformational Equilibria in Cyclohexane Derivatives. F. A. L. Anet. Hindered Rotation about B-N Bonds. J. Lee. Rotation about the Bond Joining Trigonal and Tetrahedral Carbon. A. Bothner-By.

Anachem Conference

10:40

11:00

11:30

12:00

12:20

Parke, Davis, & Co., Ann Arbor, Mich. Chromatographic Densitometry and Automated Flow Spectro­ photometry of Ketosteroids, Em­ manuel Epstein and Bennie Zak, Departments of Pathology, St. Joseph Mercy Hospital, Pontiac, Mich., Wayne State University, College of Medicine, and Detroit Receiving Hospital, Detroit, Mich. New Trends in Determination of Pesticide Chemical Residue in Foods and Commodities. D. R. Schultz and Louis Lykken, Shell Chemical Co., New York 20, N.Y. The Use of Solubility Analysis in Pharmaceutical Stability Studies. J. P. Comer and L. D. Howell, Analytical Research and Develop­ ment, Eli Lilly and Co., Indian­ apolis 6, Ind. Colorimetric Determination of Serum Magnesium Using Magon. A. J. Boyle, P. J. Burcar, and R. E. Mosher, Department of Chem­ istry, Wayne State University, and Department of Research, Providence Hospital, Detroit, Mich. A New Method and Quantitative Aspects of Sulfated Mucopolysac­ charides. G. Zdybek, D. S. McCann, and A. J. Boyle, Depart­ ment of Chemistry, Wayne State University, Detroit 2, Mich.

Monday Afternoon Electroanalytical Biochemistry

Bennie Zak, Presiding 2:20 A New Method for Scanning Agar-Gel Electrophoresis Sam­ ples. Jon J. Kabara, Norman R. Spafford, and Diana Zyskowski, Department of Chemistry· Univer­ sity of Detroit, Detroit, Mich. 2:10 A Simple, Improved Microdensitometric Recording Method for Slide Mounted-Electropho-

NEWS

2:55

3:15

4:10

4:35

5:00

5:20

Meet the CHROMAD

retic Systems. John D . Johnson and William H . Starkweather, General Medical Research Unit, U. y. Veterans Administration Hospital, Ann Arbor, Mich. A Rapid Spectrophotometry D e termination of Multiple Dehydrogenases Following Agar Gel Electrophoresis. William H. Starkweather, John D . Johnson, Henry K. Schoch, and Elizabeth L. Schwartz, General Medical R e search Unit, U. S. Veterans Administration Hospital, Ann Arbor, Mich. Electrophoresis and ImmunoElectrophoresis on Agar GelPaper. Lawrence M. Werner and Bonnie Zak, Departments of Microbiology and Pathology, Wayne State University, Detroit, Mich. Amperometric Titration of Cyanocobalamin. Stanford L. Tackett and Justin W. Collât, Department of Chemistry, The Ohio State University, Columbus, Ohio. Amperometric Measurement of Reaction Rates: Enzymatic Determination of Glucose, H . L. Pardue, Department of Chemistry, Purdue University, Lafayette, Ind. Specific and Quantitative Autoradiography. Jon J. Kabara, Roberta Glock, Norma R. Spafford, and John Smeggil, Department of Chemistry, University of Detroit, Detroit, Mich. An Automatic Recording Instrument for the Measurement of Circular Dichroism. George Ogden, Baird-Atomic, Inc., Cambridge, Mass.

Monday Afternoon Emission, X-Ray, and Flame Spectroscopy E. F . Runge, Presiding 2:00 The Application of X-Ray E m i s sion Spectroscopy to the Analysis of Ferrous Alloys, A. C. Ottolini, Research Laboratories, General Motors Corp., Warren, Mich. 2:30 The Determination of Trace E l e ments Using the Vacuum Cup Solution Technique. Carl Leistner, United Carbon Products Co., Bav Citv, Mich.

Monday Afternoon Atomic Absorption Spectroscopy

T. P . Schrciber, Presiding 3:30 Hollow Cathode Tubes for Atomic Absorption Spectroscopy. J. C. Burger, W. Gillies, and G. K. Yamasaki, Westinghouse Electric Corp., Electronic Tube Division, Elmira, Ν . Υ. 3:55 Determination of the Alkaline E a r t h Metals by Atomic A b ­ sorption Spectrophotometry. Walter Slavin and David C. Manning, Perkin-Elmer Corp., Norwalk, Conn. 4:20 Design Features of a MultiChannel Atomic Absorption Photometer. Dorman E. Priest, Research and Control Instru­ ments, Inc., Woburn, Mass. 4:45 Analysis of Various Solutions by Atomic Absorption Spectroscopy. John J. Devaney, Jarrel-Ash Co.. Xewtonville 60, Mass.

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A

NEWS

Tuesday Morning, October 23 11:20

Anachem Award Symposium

M. D . Cooper, Presiding 9:00 Presentation of Anachem Award to Dr. P . K . Winter. Dr. Β. Ε. Tiffany, Ford Motor Co., Chair­ man, Anachem Award Committee. 9:15 Anachem Award Address, The Contributions of Analysts in a Nonchemical Industry. P. K. Winter, General Motors Corp. 10:40 The Analyst in the Automotive Industry—His Role in the Sup­ plier Industries—Ferrous Alloys.

Hugh F . Beeghly, Jones and Laughlin Steel Corp. Autos, Analysts, and Aluminum. M. L. Moss, Aluminum Co. of America.

Tuesday Afternoon 1:45

2:25

The Continuing Challenge of Nonferrous Metal Analysis. Runyan G. Ernst, American Metal Climax, Inc. Analytical Chemistry in the Paint, Plastics, and Rubber In­ dustries. S. S. Lord, E. I. du Pont de Nemours and Co., Inc.

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Application of Analytical Tech­ niques to Ceramics. Willard E . Hauth, AC Spark Plug Di­ vision, General Motors Corp. The Analyst's Role in the De­ velopment and Improvement of Fuels and Lubricants for the Automotive Industry. Charles M. Gambrill, Ethyl Corp.

Wednesday Morning, October 24 Gas Chromatography

T. O. Morgan, Presiding 8:45 Electron Capture Detection Sys­ tems. Albert Zlatkis, Depart­ ment of Chemistry, University of Houston, Houston, Tex. 9:10 Application of Golay Columns with Different Diameters at Both Isothermal and Programmed Temperature Conditions. L. S. Ettre and W. Averill, The Perkin-Elmer Corp., Norwalk, Conn. 9:35 Gas Chromatographic Analysis of Dilute Hydrocarbon Mixtures Using Temperature Programmed Capillary Columns. David J. McEwen, Research Laboratories, General Motors Corp., Warren, Mich.

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ANALYTICAL CHEMISTRY

R. Ring, Presiding 10:35 The Analysis of Glycols, Alco­ hols, and Related Compounds by Gas Chromatography. Samuel F . Spencer and Louis Mikkelsen, F & M Scientific Corp., New Castle, Del. 10:55 A Mixed-Substrate Column for Gas Chromatographic Analysis of Paint-Thinners and Related Solvent Mixtures. Roger L. Gatrell, Research Laboratories, General Motors Corp., Warren, Mich. 11:15 An Application of Gas Chro­ matography to the Separation and Analysis of Organic Carbonates, Chlorophenylphenol Germicide Mixtures, and Perfluoro-organic Compounds. B. J. Gudzinowicz, J. L. Driscoll, J. Aim, and W. R. Smith, Monsanto Research Corp., Everett, Mass. 11:40 Gas Chromatographic Investiga­ tion of Certain Chlorinated Hy­ drocarbon Mixtures. Vernon Davies and D . F . Boltz, Depart­ ment of Chemistry, Wayne State University, and Analytical D e ­ partment, Parke, Davis & Co., Detroit, Mich. 12:00 Design Considerations and Ap­ plications of a Fully Automatic Preparative Gas Chromatograph. J. M. Kauss, J. Peters, and A. J. Martin, F & M Scientific Corp., Avondale, Pa. 12:20 Electron Affinity Chromatog­ raphy. Gerald Neville, JarrelAsh Co., Newtonville 60, Mass.

NEW JERSEY

Wednesday Morning Analytical Absorption Spectroscopy

J. M . Vandenbelt, Presiding 8:45 Indirect Precision Spectro­ photometry, R. Bastian, A. E l dridge, and R. S. Kelly, Research and Development Center, R e ­ public Aviation Corp., Farmington, Ν . Υ.

NEWS 9:15

9:45

10:10

11:10

11:35

12:00

12:20

Comparison of Methods for the Spectrophotometric Determina­ tion of the Nitrite Ion. E . Sawicki, T . W. Stanley, and J. D . Pfaff, Laboratory of Engineering and Physical Sciences, Division of Air Pollution, Robert A. Taft Sanitary Engineering Center, Public Health Service, Cincinnati 26, Ohio. Spectrophotometric Determina­ tion of 1-Naphthol. George A. Pearse, Jr., Dept. of Chemistry, LcMovne College, Syracuse 3, Ν . Υ." A Standard Filter for Wave­ length and Absorbance Check of Near Infrared Spectrophotom­ eters. J. M . Vandenbelt, R e ­ search Laboratories, Parke, Davis & Co., Ann Arbor, Mich. Spectrophotometric and Fluorometric Determination of Mag­ nesium with O, O'-Dihydroxyazobenzene. Rodney Olsen, Rich­ ard Jensen, and Harvey Diehl, Department of Chemistry, Iowa State University, Ames, Iowa. The Effect of Fluorine on Infra­ red Spectra. A. H . Gropp, De­ partment of Chemistry, Univer­ sity of Florida, Gainesville, Fla. Recent Developments in the Ab­ sorption Spectroscopy Group. Martin H . Gurley I I I and E d ­ ward H . Merrill, Baird-Atomic, Inc., Cambridge 38, Mass. A New Extended Range Infrared Spectrophotometer. J. Ashley, N . Shifrin, and Robert J. Man­ ning, Beckman Instruments, Inc., Scientific and Process Instruments Division, Lincolnwood, 111.

Wednesday Afternoon Analytical Chemistry

Walter Wagner, Presiding 2:00 The Cerium(IV) Oxalate Reac­ tion in Sulfate Media. Garry A. Rechnitz and Yehic El-Tantawy, Department of Chemistry, Uni­ versity of Pennsylvania, Philadel­ phia 4, Pa. 2:20 Determination of the Tetrazote Ring by Acylation. Coe D . Suydam and K. G. Stone, Depart­ ment of Chemistry, Michigan State University, East Lansing, Mich. 2:40 Determination of ZirconiumHafnium Ratios by EDTA Titra­ tion. Richard B. Hahn and Ahmed H . Wardi, Department of Chemistry, Wayne State Univer­ sity, Detroit, Mich. 3:00 An Apparatus for Fluorescent Titrations. T . J. Paulos and T . H. Clarke, Fisher Scientific Co., Pittsburgh 19, Pa. 3:20 A Method for Determining Sul­ fite with an Automatic Colorim­ eter. Dan P . Walton and Pratt H. Johnson, Milton Roy Co., St. Petersburg, Fla.

Wednesday Afternoon Analytical Chemistry—General

Clyde Leaf, Presiding 2:00 A Rapid Combustion Method for the Determination of Organic Substances in Aqueous Solutions.

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.

51 A

NEWS C. E. Van Hall, J. Safranko,* and V. A. Stenger, The Dow Chemical Co., Midland, Mich. (*Hercules Powder Co., Alle­ gany Ballistics Laboratory, Cumberland, Md.) 2:30 A Study of Elution Behavior of Manganese and Cobalt Using Two Strong-Base Anion E x ­ change Resins with Varying Physical Properties. Wm. R. Lee and Robert E. Kohn, Re­ search Laboratories, General Mo­ tors Corp., Warren, Mich. 2:55 Refractive Index Monitor for Chromatographic Columns. R. D. Conlon, The Procter and Gamble Co., Cincinnati 17, Ohio. 3:15 Solvent Extraction and Colorimetric Determination of Cobalt. Otho McFarland and A. M. Wil­ son, Department of Chemistry, Wayne State Universitv, Detroit 2, Mich. Wednesday

Afternoon

Electroanalytical Chemistry

Al Gassman, Presiding 3:55

Determination of Water below 10 P.P.M. in Benzene and Related Solvents Using Coulometrically Generated Iodine. R. F . Swensen and D. A. Keyworth, Univer­ sal Oil Products Co.. Des Plaines, 111. 4:20 Coulometric Titration of Trace Amounts of Organic Chlorine in Alkylene Oxides. S. T. Hirozawa and Ν . Μ. Lisicki, Wyandotte Chemicals Corp., Wyandotte, Mich. 4:40 Nonaqueous Conductometric Ti­ tration of Diprotic Acids in Triethylphosphate with Lithium Methoxide. George H . Schenk and Leonard Keith, Department of Chemistry, Wayne State Uni­ versity, Detroit 2, Mich. 5:00 Conductometric Determination of Carbon Using a Carbonate Satu­ rated Barium Hydroxide Ad­ sorbent. E. J. Violante, Research Service Dept., Scientific Labora­ tory, Ford Motor Co., Dearborn, Mich.

Thermal Radiation Symposium A symposium on M e a s u r e m e n t of T h e r m a l R a d i a t i o n Properties of Solids will be held a t t h e Biltmore Hotel, D a y t o n , Ohio, September 5 to 7. This unclassified meeting is sponsored jointly by t h e Aeronautical Systems D i ­ vision of t h e U.S. Air Force, t h e N a ­ tional Bureau of Standards, and t h e National Aeronautics and Space Ad­ ministration. T h e symposium will deal with instru­ mentation and techniques for measur­ ing t h e r m a l radiation properties such as emittance (emissivity), absorptance, reflectance, and t r a n s m i t t a n c e . The t e m p e r a t u r e range of interest extends from 10° K. to above 3000° K., and t h e wavelength range of interest ex­ tends from the ultraviolet into the in-

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frared to 15 microns and beyond. Inquiries regarding submission of papers or attendance at the symposium, should be addressed t o C Robert Andrews, L T niversity of D a y t o n , D a y ­ ton 9, Ohio.

IUPAC Meetings T h e X X I I n d Conference of the I n ­ ternational Union of P u r e and Applied Chemistry ( I U P A C ) will be held in London, J u l y 5 to 9, 1963, and will be followed by the X l X t h International Congress of Pure and Applied Chem­ istry, J u l y 10 to 17. T h e scientific program of the Con­ gress will feature 20 invited lectures in addition to t h e contributed papers. The Analytical Chemistry Division of the Congress will consider the following topics: trace analysis, separation methods, electroanalysis, and teaching of analytical chemistry. All correspondence concerning the Congress should be addressed t o : L t . Col. Francis J. Griffin, H o n o r a r y Sec­ retary, X l X t h International Congress of P u r e and Applied Chemistry, 14 Belgrave Square, London, S.W. 1, England. All correspondence concerning the Conference should be addressed t o : D r . Rudolf Morf, Secretary General of I U P A C , c/o Hoffmann La Roche & Co. Ltd., Basle 2, Switzerland.

National Medal of Science Candidate Selection Nomination and selection procedures were adopted a t a recent meeting of t h e President's Committee on the N a ­ tional Medal of Science. Five condi­ tions will govern selection of candi­ d a t e s : total effect of the candidate's work on t h e present state of physical, biological, mathematical, and engineer­ ing science; recent achievements and their potential effect on the develop­ m e n t of scientific t h o u g h t ; distin­ guished service in s u p p o r t of science and engineering; achievements since previous recognition b y means of in­ ternational or national awards ; no limi­ tation as to the time when t h e out­ standing work was performed. Nominations are invited primarily from recognized professional societies and academies of national scope and from editors of professional journals. Deadline for submission is August 1 and should be sent to Professor F r e d ­ erick Seitz, Chairman, President's Com­ mittee on t h e National M e d a l of Sci­ ence, National Science Foundation, 1951

no blind alley with this colorimeter T h e Coleman Electric i m e t e r is different.

Color­

Other colorimeters, while some­ t i m e s a d e q u a t e for t h e i r o r i g ­ inal purpose, lead only to a dead end w h e n it c o m e s t i m e to upgrade laboratory capabil­ ity to the more advanced tech­ n i q u e s of s p e c t r o p h o t o m e t r y . N o t so w i t h t h e C o l e m a n C o l o r i m e t e r . It p r o v i d e s a n e a s y e c o n o m i c a l m e a n s for g r o w t h into spectrophotometry. It uses exactly the same cuvettes, adapters, accessories — even the same power supply — as the famous Coleman Junior Spectrophotometer. T e c h n i q u e s o f o p e r a t i o n are almost identical . . . your labo­ ratory technicians can make an i m m e d i a t e t r a n s i t i o n f r o m colorimetry to spectrophotometry w i t h the Junior. Finally, when the major an­ alytical workload is transferred to the Junior, the Coleman Col­ orimeter remains a valuable standby instrument. Avoid planned obsolescence in your instrumentation plan­ ning . . . equip your laboratory for f u t u r e g r o w t h . Write for Coleman Colorimeter Bulletin AB-254 and Junior Spec­ trophotometer Bulletin AB-240B. COLEMAN INSTRUMENTS, INC. MAYWOOD, ILLINOIS Circle No. 152 on Readers' Service Card VOL. 3 4 , N O . 8, JULY 1 9 6 2

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NEWS Constitution Ave., N . W . , Washington 25, D . C. F u r t h e r information can be obtained from D r . Robert W . Johnson, National Science Foundation.

Applied Spectroscopy and Analytical Chemistry Meeting T h e First Annual Pacific Meeting on Applied Spectroscopy a n d Analytical Chemistry will take place a t t h e H u n t ington Sheraton Hotel, Pasadena, Calif., October IS to 19. T h e program includes four technical sessions of one invited a n d six contributed papers, a dinner address b y D r . Harrison Brown, a n d a n instrument exhibit. Abstracts of papers should be submitted b y J u l y 1 to A r t h u r A. Chodas, P r o g r a m Chairman, Division of Geochemistry, California I n s t i t u t e of Technology, Pasadena, Calif. Additional information can be obtained from t h e Meeting Chairman, D r . W . F . Ulrich, Scientific a n d Process I n s t r u m e n t s D i vision, Beckman Instruments Inc., Fullerton, Calif.

Industrial Spectroscopy Course A concentrated course on t h e theoretical a n d experimental aspects of spectroscopy will be given a t Southern Missionary College, Collegedale, Term., from August 8 to 22. T h e tuition fee is $160 a n d includes all supplies, t r a n s p o r t a t i o n on local field trips, and reference book. I t does not include board and room. Applications should include a brief statement of qualifications, background, interest, a n d a snapshot, a n d should b e sent t o D r . R a y Hefferlin, Physics D e p a r t m e n t , Southern Missionary College, Collegedale, Tenn., b y J u l y 1. A certificate of a t t a i n m e n t will b e presented to each student.

Search Strategy Seminar Lectures a n d laboratory o n leading systems of information retrieval, m e t h ods of indexing a n d of thesaurus construction will b e offered as a 3-week session b y t h e Drexel I n s t i t u t e of Technology from October 8 t o 26. T h e registration is limited t o 35 students. Tuition is $350 for 3 weeks. Deadline for registration is September 15. F o r further information contact M r s . M . H . Davis, G r a d u a t e School of L i b r a r y Science, Drexel I n s t i t u t e of Technology, Philadelphia 4, P a . 54 A

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ANALYTICAL CHEMISTRY

CALENDAR OF EVENTS July * 2 tO4

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High Resolution N M R Spectroscopy Symposium, Boulder, Colo. Contact: Dr. Melvin Hanna, Univeritv of Colorado, Boulder, Colo. Page 47 A, July.

Aug. 6 to 7—Fifth Annual Rocky Mountain Spectroscopy Conference. Olin Hotel, Denver, Colo. Sponsor: Society CominQ Events l o r Applied Spectroscopy (Rocky Mountain Section). Contact: F. S. Bonomo, Denver Research Institute, University of Denver, Denver 10, Colo. Page 55 A, March. Aug. 6 to 10—Gordon Research Conferences, Instrumentation Session, Colby Junior College, New London, N. H . Contact: Dr. W. G. Parks, University of Rhode Island, Kingston, R. I. Page 39 A, May. Aug. 8 to 10—Eleventh Annual Conference on Applications of X-Ray Analysis. Albany Hotel, Denver, Colo. Sponsor: Denver Research Institute. Contact: W. M . Mueller, Denver Research Institute, University of Denver, Denver 10, Colo. Page 57 A, March. Aug. 8 to 10—1962 Standards Laboratory Conference, National Bureau of Standards Laboratories, Boulder, Colo. Contact: A. E . Hess, Circuit Standards Division, NBS, Boulder, Colo. Page 46 A, June. Aug. 13 to 17—Gordon Research Conferences, Analytical Chemistry Session, New Hamilton School, New Hampton, N . H . Contact: Dr. W. G. Parks, University of Rhode Island, Kingston. R. I. Page 39 A, May. Aug. 20 to 24—Gordon Research Conferences, Separation and Purification Session, Colby Junior College, New London, N . H . Contact: Dr. W. G. Parks, University of Rhode Island, Kingston, R. I. Page 39 A, May. August 21 to 24—International Symposium on F a r Infrared Spectroscopy. SheratonGibson Hotel, Cincinnati, Ohio. Sponsor: Analytical Branch, Physics Laboratory, Materials Center, W A D D . Contact: F . F . Bentley, Materials Control, ASD, Wright-Patterson AFB, Ohio. Aug. 26 to 31—13th Meeting ICUMSA, Hamburg, Germany. Contact: Dr. D. Gross, Tate & Lyle Research Laboratories, Keston, Kent, England. Page 45 A, June. Aug. 27 to 31—Gordon Research Conferences, Infrared Spectroscopy Session, Kimball Union Academy, Meriden, N . H . Contact: Dr. W. G. Parks, University of Rhode Island, Kingston, R. I. Page 39 A, May. Aug. 29 to Sept. 5—FLth international Congress for Electron Microscopy, Philadelphia, P a . Host: Electron Microscope Society of America. Contact: Fifth International Congress for Electron Microscopy, 7701 Burholme Ave., Philadelphia 11, Pa. Page 50 A, Nov. Sept. 5 to 7—Symposium on Measurement of Thermal Radiation of Solids. Biltmore Hotel, Dayton, Ohio. Sponsors: U. S. Air Force, National Bureau of Standards, National Aeronautics and Space Administration. Contact: C. R. Andrews, University of Dayton, Dayton 9, Ohio. Sept. 9 to 14—American Chemical Society, 142nd National Meeting, Atlantic City, N.J. Sept. 10 to 15—International Symposium on Molecular Structure and Spectroscopy, Tokyo, Japan. Sponsor: International Union of Pure and Applied Chemistry and Science Council of Japan. Contact: Secretary, International Symposium on M o lecular Structure and Spectroscopy, Science Council of Japan, Ueno Park, Tokyo, Japan. Page 105 A, Feb. Sept. 16 to 20—Second Annual Conference on Pharmaceutical Analysis, Kings Gateway, Land O'Lakes, Wis. Contact: R. S. Strommen, University of Wisconsin, Madison 6, Wis. Page 108 A, Feb. Sept. 16 to 22—Eighth Latin American Congress of Chemistry, Buenos Aires. Contact: Secretaria, Octavo Congreso Latinoamericana de Quimica, Casilla Correo 2153, Buenos Aires, Argentina. Page 105 A, Feb. Sept. 17 to 19—Ninth Ottawa Symposium on Applied Spectroscopy, Ottawa, Canada. Sponsor: Canadian Association for Applied Spectroscopy. Contact: Ben Farrar, J. T . Donald & Co., Ltd., 1181 Guy St., Montreal 25, Quebec. Page 63 A, March. Sept. 26 to 28—Practice of Gas Chromatography. Michigan State University. Sponsors: ASTM Committee E-19 and Michigan State University. Contact: Nathaniel Brenner, The Perkin-Elmer Corp., Norwalk, Conn. Page 46 A, April. Oct. 8 to 12—12th Annual Instrument Symposium and Research Equipment Exhibit, National Institutes of Health, Bethesda, Md. Contact: James B . Davis, National Institutes of Health, Bethesda 14, M d .

Technical and Industrial Communications Institute T h e Fifth Annual I n s t i t u t e in Technical a n d Industrial Communications will b e held a t Colorado State University, F o r t Collins, J u l y 9 to 13. T h e intensive, week-long workshop and course will feature 19 communica-

tions authorities, group discussions, special problem clinics, a n d laboratory writing exercises. Basic a n d advanced instruction in technical writing a n d industrial communications will b e presented. Information can b e obtained from D r . H e r m a n Weisman, Colorado State University, F o r t Collins, Colo.

NEWS

Industry Items Aqua-Chem International, Ltd., London, England, has been formed by Aqua-Chem. Inc., Waukesha, Wis., and several British interests. The new firm will specialize in water purification equipment and land-based long tube flash evaporators for conver­ sion of sea water into fresh water. Aqua-Chem, Inc., is an affiliate of Cleaver-Brooks Co., Milwaukee, Wis. Computer Products, Inc., 21 Broad St., Manasquan, N. J., is a newly formed company specializing in elec­ tronic mode controls and analog com­ puter modernization. Controls for Radiation Inc., 130 Alewife Brook Parkway, Cambridge 40, Mass., provides radiation protection and nuclear services. The services in­ clude: radiochemical and bioassay analyses, film badge service, and leasing and maintenance of radiation monitor­ ing equipment. F & M Scientific Corp., Avondale, Pa., has announced a $300,000 expan­ sion program which will add 38,000 sq. ft. to present plant facilities. The newbuilding, to be completed by mid­ summer, will house the Research and Engineering Department and the Ap­ plication Research group. The company manufactures gas chromatographic equipment and is ex­ panding its product line into new and related analytical instruments and elec­ tronic equipment. The company has also announced the formation of a European subsidiary, F&M Scientific Europa, N. V., Am­ sterdam, The Netherlands. At present, the European company will market the full line of instruments offered by the parent company; however within 1 or 2 years the analytical instruments will be manufactured in Europe. J & G Instrument Corp., Milltown, N. J., has moved its offices to 1996 Highway 27, Edison, N. J. The com­ pany is the U. S. agent for Oertling balances and specializes in analytical and microbalances. It also provides a balance and repair service. LaPine Scientific Co., 6001 S. Knox Ave., Chicago 29, 111., has been ap­ pointed a distributor for the new stabilized pH indicator, Model No. 7401-A1 produced by Leeds & Northrup Co., Philadelphia, Pa. Maser Optics-West, 430 Cambridge Ave., Palo Alto, Calif., has announced plans for a new building to be com­ pleted in September, in the Palo Alto Industrial Park.

The new facility will be used for re­ search, development, and the manu­ facture of laser and quantum electronic devices. The company is a research subsidiary of Maser Optics, Inc., 89 Brighton Ave., Boston, Mass. Molecular Science Corp., 3939 Bohannon Dr., Menlo Park, Calif., is the newest subsidiary of Universal Microtron Corp., Beverly Hills, Calif. The new company will develop and manufacture a wide range of microelec­ tronic subsystems. Oak Ridge National Laboratory, Oak Ridge, Tenn., has placed aboard the N. S. Savannah its Mobile Shield­ ing Laboratory-1, in order to measure the effectiveness of the biological shield on the nuclear ship. The MSL-1 has been used extensively in shield studies on land-based reactors and in the recent Bare Reactor Experiment (BREN) tests in Nevada. Radiation Materials, Inc., 36-32 37th St., Long Island City 1, Ν. Υ., has opened an electron beam irradiation service for research and commercial processing. Machine operating time and laboratory time used in sample preparations will be charged on an hourly basis. Scientific Glass Apparatus Co., Inc., Bloomfield, N. J., has announced completion of its $500,000 administra­ tion wing attached to the present build­ ing housing the company. The new building has a fully equipped laboratory for demonstrations. The company's products include electronic instruments, chemicals, glassware, and general laboratory supplies. Temtro, Inc., 3016-C S. Halladay, Santa Ana, Calif., has changed its name to Temtech, Inc. The name change marks an expanded line of products in the ultraprecision temperature sensor field and control subsystems. The new company remains a subsidiary of David Industries. United Electrodynamics, Inc., Pasadena, Calif., has acquired Research Instruments Corp. and its Analytic Systems Co. division, Pasadena; both will be operated as wholly-owned subsidiaries. Analytic Systems Co. designs, de­ velops, manufactures, and distributes process stream analyzers and analysis systems including infrared and ultra­ violet photometric analyzers, flame ionization detectors, and thermal con­ ductivity detectors.

THE MIXER YOU CAN USE ANYWHERE This mixer is safe. Its motor is totally enclosed, explosionproof — approved by U/L for Class I, Group D, and for Class II, Groups E, F and G, service. It's a heavy-duty mixer, designed for continuous operation. Using it, you can quickly bring 50 gallons of low-viscosity fluids to uniformity, or mix smaller quan­ tities of high-viscosity fluids. It's a good tool for suspending solids, dispersing gas or studying mass transfer and heat transfer. Put it into a pilot-plant setup and you can derive accurate mixing data for scale-up computations. It's a LIGHTNIN Mixer—Model XP. Like all LIGHTNIN Mixers, it's fully guaran­ teed. The 1/20-hp motor turns the 24inch stainless steel shaft and 2%-inch propeller at a constant 1750 rpm. Bear­ ings that never need lubrication support the motor shaft. An extra sealed bearing steadies the tube holding the shaft, for true running with minimum deflection. Bronze tank clamp and ball-joint mount­ ing permit locking the mixer at any angle. Order it from your supply house, or write us. Specify LIGHTNIN Model XP Mixer: With motor lead wires but without cord, for l l O v 60cy l p h $130.00 There's a full line of heavy-duty LIGHTNIN Mixers and accessories for the labora­ tory. Bulletin B112 describes them all. To receive it, check reader service card or write us.

Lightnin® Mixers MIXING EQUIPMENT Co., Inc. 160-g Mt. Read Blvd., Rochester 3, Ν . Υ. In Canada: Greey Mixing Equipment, Lfd., 700 Miranda Ave., Toronto 19, Ont. In Europe: Lightnin Mixers, Ltd., Poynton, Cheshire, England Circle No. 60 on Readers' Service Card

VOL.

34, NO. 8, JULY 1962

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