Analysts Aid Petroleum Product Development - Analytical Chemistry

May 25, 2012 - Analysts Aid Petroleum Product Development. Anal. Chem. , 1957, 29 (8), pp 49A–51A. DOI: 10.1021/ac60128a746. Publication Date: Augus...
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Light-faced brick and glass characterize Cities Service's new 30,000 square foot Research and Development Laboratory. The research and analytical laboratories and cafeteria are in the one-story wing with automotive and photo laboratories, machine shop, and administrative offices in the two-story part. There are also an extensive library and art department

LABORATORY

OF THE MONTH

Analysts A i d Petroleum Product D e v e l o p m e n t Petroleum refiners face constant pressure t o make better gasolines, fuels, and lubricants. Cities Service meets this competitive battle with a substantial research program which emphasizes product development. Responsibility for this program lies with Cities Service Research and Development Co. This consolidated research a r m was set u p in 1948. Activities were then located in five labs: Hillside, N . . J . , P e t t y Island, N . J., E a s t Chicago, 111., Tallant, Okla., and Lake Charles, La. Growth since its founding created need for more space and also the need for centralized effort. Last J u n e the company officially opened a new product development lab a t Cranbury, N . J . Located on a 100-acre t r a c t it consolidates research formerly handled a t the Hillside, P e t t y Island, and E . Chicago labs. Lake Charles continues as a process development and catalyst research unit while another lab, a t Tulsa, handles the drilling and exploration side. Research a t C r a n b u r y centers on improved aviation, motor, Diesel, and jet fuels. Other important areas include lubriConventional w e t chemical analysis still plays an portant role in the modern research laboratory

cants—oils, greases, or synthetics—fuel oils, and asphalts. Basic research is also included in Cranbury's program. T y p i cal basic problems now under study are friction coefficient effects, wear fundamentals, and theoretical flame. research. T h e Cranbury lab also has a nuclear energy section housed in a separate building. I t has three labs plus the radiation cave. T h e latest automatic and semiautomatic safety features are used t o prevent accidental exposure t o radiation. I t is

im-

The new R&D center has 1 0 main laboratories with service lines feeding from the floor into the center and wall working areas. Each laboratory has a safety shower, chemicalresistant work benches, and vinyl tile flooring. An accelerated stability apparatus gives information concerning oxidation rates of fuel oils VOL. 29, NO. 8, AUGUST 1957

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49 A

Cities Service is also exploring nuclear energy as a means to improved fuels and lubricants. The nuclear laboratory is housed in a separate building. Shown here is the radiation area. The operator works in a pit while operations are carried out at floor level. The cobalt-60 source is kept in 10 feet of water. A 42-inch-thick window, 42-inch high density concrete walls, a 15ton lead door, and remote controls assure safe operating conditions

When animal and vegetable oils were major lubrication materials, mechanical performance was often erratic. Today's petroleum-based lubes require close adherence to physical specifications. A physical testing laboratory helps maintain quality standards

Sulfur content of petroleum products, such as gasoline, is determined by the conventional lamp method

the only nuclear unit, owned by a petroleum company, t h a t uses cobalt-60, in flat plates 13.5 X 2 X 1 / 8 inches, as its radiation source. T h e cobalf>60 has a potency of 5000 curies. These research facilities need extensive analytical support. Hence over l / 3 of the work a t C r a n b u r y is analytical. This includes research services, product inspection, and analytical research. T h e latest wet chemical methods and physical tests are used. M u c h instrumentation is involved. More t h a n 100 people are employed a t the new lab. Half are technically trained, mostly chemists or chemical engineers. T h e company plans to increase t h e staff in the future. 50 A

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ANALYTICAL CHEMISTRY

NEW! WACO . . . f o r Karl

TITRATOR Fischer

Moistures

Physicochemical methods of analysis are utilized extensively in petroleum research

Viscosity determinations are one of a series of tests applied to petroleum products

Infrared equipment is among the extensive instrumentation used. Other instrumentation includes photometers, recording titrimeters, microdistillation equipment, gas chromatographic units, and x-ray fluorescence apparatus

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Circle No. 51 A on Readers' Service Card, page 73 A

VOL. 29, NO. 8, AUGUST 1957

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51 A