Contributed Articles - ACS Publications - American Chemical Society

Computer Evaluation of Continuously Scanned Mass. Spectra of Gas Chromatographic Effluents. R. A. Hites and K. Biemann. 855. Spectrophotometric .... w...
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Contributed Articles

Physical Basis of Atomic Absorption Spectrometry. Influence of Temperature Gradients on Spatial Distribution of Neutral Atoms in the Long Pathlength Cell. Atsushi Ando, Keiichiro Fuwa, and B. L. Vallée

Electrochemical Behavior of Triphenyltin Compounds and Their Determination at Submicrogram Levels by Anodic Stripping Voltammetry. M. D. Booth and B. Fleet

Nondestructive Determination of Fluorine by Photon Activation Using a Betatron. L. Kosta and J. Slunecko

Nondestructive Determination of Platinum Metals in Ores, Matte, and Lead Assay Beads by Reactor Activation Analysis and High Resolution Gamma Spectrometry. Jacob Turkstra, P. J. Pretorius, and W. J. de Wet

Specific Spectrofluorometric Determination of Atmospheric Ozone using 2-Diphenylacetyl-l,3-lndandione-lHydrazone. Denys Amos

Liquid Anion Membrane Electrodes Sensitive to Metal Cation Concentration. G/ancar/o Scibona, Leda Mantella, and P. R. Danes/

Decision and Detection Limits for Linear Calibration Curves. Andre Hubaux and Gilbert Vos

Palladium-Hydrogen System. Efficient Interface for Gas Chromatography—Mass Spectrometry. P. G. Simmonds, G. R. Shoemake, and J. E. Lovelock

881

Practical Least Squares Approximation of Chromatog r a m s . S. M. Roberts, D. H. Wilkinson, and L. R. Walker

886

Analysis for Surface Peroxides. T. R. Heagney

894

818

825 Arthur Bradley

and

831 Identification of Impurities in α-Trinitrotoluene by Nu­ clear Magnetic Resonance Spectrometry. D. G. Gehring

898

835

Automated Kjeldahl Determination of Nitrogen in Pe­ troleum. R. N. Heistand

903

842

Numerical Deconvolution of Overlapping Stationary Electrode Polarographic Curves with an On-Line Digital Computer. W. F. Gutknecht and S. P. Perone

906

Electrochemical Oxidation of NADH Analogs. Blaedel and R. G. Haas

918

W. J.

844

Notes 849 Precision and Optimum Acidity in Complexometry. W. Budesinsky

Computer Evaluation of Continuously Scanned Mass Spectra of Gas Chromatographic Effluents. R. A. Hites and K. Biemann

Nondestructive Neutron Activation Analysis of Air Pollution Particulates. R. Dams, J. A. Robbins, K. A. Rahn, and J. W. Winchester

Ionic Hydration and Single Ion Activities in Unassociated Chloride at High Ionic Strengths. R. C. Bates, B. R. Staples, and R. A. Robinson

Preparation of Known Concentrations of Gases and Vapors with Permeation Devices Calibrated Gravimetrically. F. P. Scaringelli, A. E. O'Keefe, Ethan Rosenberg and J. P. Bell

Determination of Trace Impurities in Argon by Microwave Induced Excitation. H. E. Taylor, J. H. Gibson, and R. K. Skogerboe

B. 928

Spectrophotometric Determinations Based on the For­ mation of Tris-l,10-Phenanthroline Iron(ll). T. J. Bydalek, J. E. Podoski, and D. B. John

929

861

Volumetric Determination of Pyridine Bases Using Iron(lll) Hydroxide Sulfate as Indicator. Yoshio Koda

931

867

Use of Ammonium Fluoride in Determination of Zirco­ nium and Other Elements by Atomic Absorption Spec­ trometry in the Nitrous Oxide—Acetylene Flame. A. M. Bond

932

871

Preparation of Thermally Stable Gas-Chromatographic Packing Materials. A. H. Al-Taiar, J. R. Lindsay Smith, and D. J. Waddington

935

876

Application of Capillary Burners in Flame Spectrometry. K. M. Aldous, R. F. Browner, R. M. Dagnall, and T. S. West

939

855

ANALYTICAL CHEMISTRY, VOL. 42, NO. 8, JULY 1970

·

3A

Viscosity

directly

in

centipoises

Contributed Articles

HOEPPLER VISCOMETER PRECISION MODEL

Fluorometric Determination of Microgram Amounts of

Hoeppler Viscometer provides a fast, accurate method of determining viscosity of Bases, liq­ uids, oils, plastics, syrups, viscous tars and dark liquids. From 0°C. to 100°C. Direct readings in centipoises (or centistokes). From 0.01 to 1,000,000 centipoises. Accuracy 0 . 1 % to 0 . 5 % . Small sample (30cc) required. Results consistent and reproducible. Price $350. Interchangeable spare parts available. Write for Bulletin HV-303.

Meperidine.

L. A. Dal Cortivo,

M. M. De Mayo,

and

S. B. Weinberg

941

Indicator Titrations in Sulfolane. MADE I N U . S . A .

UBBELOHDE VISCOMETER

943

Potentiometric Analysis of Hypophosphite in Electroless Nickel Plating Baths.

on the principle of the suspended level A capillary-type viscometer for determining the kinematic vis cosity of any true viscous liquid, such as petroleum products or lubricants. See American Society for Testing Materials, A.S.T.M. designation D 2515. Measures viscosity with an e r r o r not greater than ± 0 . 1 % , when used at efflux times at 8 0 - 1 0 0 0 seconds. The smallest listed capil­ lary is used for light fuel oil or kerosene, the others for lubricating oils. T h e temperature of the bath should be controlled within ±0.02°F. In all capillary sizes as called for by the A.S.T.M.—calibrated or uncalibrated. Uncalibrated capillary, *S24. Calibrated, S42 Metal frame to fit capillary, $7.50. Write lor Bulletin UV-S14.

A. P. Zipp

N. Fe/dste/n, T. S. Lancsek, a n d

J. A. Amick

945

Gas-Liquid

Chromatographic

Separation

of

the

Ten

Geometric Isomers of Chromomethylaniline Using Ucon Oil a s Stationary Phase on a Textured Glass Bead Support.

Edward

Townley,

Isidoro

Perez,

and Peter

Kaba-

sakalian

947

Determination of Carbon in High Purity Metals by Photon Activation Analysis.

G. J. Lutz and L. W. Masters

Correction. Analysis of

Polyimide

948

,,,,„ ,„ c s A BARRIER AND EXCITING FILTERS FOR FLUORESCENT STUDY Standard Stock Types:

Correction.

Processed in our N e w Rochelle Optical Shop. Write for Bulletins CF-417,

UV-430

Dilution. and

Dielectric

Using Attenuated Total Reflectance.

$6.50 each, 2 χ 2" χ 1 to 3mm $7.50 each, 50mm diameter $4.50 each, 25mm diameter

ND-419.

FISH-SCHURMAN CORPORATION 7 2 Portman R o a d , N e w R o c h e l l e , Ν . Υ. 1 0 8 0 2

Coatings

R. J. McGowan

942

A c i d - B a s e Microtitrations Based on Serial

J. R. Robinson,

Honore

Stelmach,

and S. P.

Eriksen

944

Aids for Analytical Chemists

Fish-Schurman

New Sample trometer.

Introduction Technique

for

Mass

Spec-

F. G. Padrta and J. J. Donohue

950

Circle No. 51 on Readers' Service Card © Copyright 1970

PELLET PRESS

by the American Chemical Society

ABC MANUSCRIPT REQUIREMENTS published in December 1969 issue, paie 2137, outlines scope and copy requirements to be observed in preparing manuscripts for consideration. Manuscript (4 copies) should be submitted to ANALYTICAL CHEMISTRY, 1155 Sixteenth St., N.W., Washington, D. C. 20036. The American Chemical Society assumes no responsibility for the statements and opinions advanced by contributors to its publications. Views expressed in the editorials are those of the editors and do not necessarily represent the official position of the American Chemical Society.

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1970 Subscription Rates 1 yr, Members, domestic and foreign Nonmembers, domestic and Canada Nonmembers, foreign except Canada PELLETS, TABLETS o r W A F E R S for any investigative or t e s t purpose can b e m a d e q u i c k l y a n d e a s i l y in this p o r t a b l e press w i t h o u t a h e a v y i n v e s t m e n t in t a b l e t m a k ­ ing m a c h i n e r y .

2811 gives

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Fifty-Third

St.

details.

Moline,

Illinois

61265

Circle No. 93 on Readers' Service Card 4 A

·

3 yr. $10.00 12.00 40.00

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P e l l e t s a r e p r o d u c e d in p o l i s h e d s t a i n l e s s steel dies a n d e j e c t e d smoothly into a stain­ less r e c e i v e r . Six d i f f e r e n t sizes, v a r y i n g from -1 18 t o o n e - h a l f inch d i a m e t e r , c a n b e p r o d u c e d in t h e s a m e b a s i c p r e s s using interchangeable punch a n d d i e sets. Specification

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ANALYTICAL CHEMISTRY, VOL. 4 2 , NO. 8, JULY 1 9 7 0

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