Pittsburgh Conference & Exposition - ACS Publications

The 38th Pittsburgh Conference and. Exposition ... Illinois at Urbana-Champaign at a ..... Particles—R.E. LAMB, Ohio Northern University, J.E. Masla...
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The 38th Pittsburgh Conference and Exposition on Analytical Chemistry and Applied Spectroscopy will be held March 9-13, 1987, in the Atlantic City Convention Center, Atlantic City, N.J. This year more than 100 technical sessions are scheduled, including 24 planned symposia and more than 1000 papers. The Exposition of Modern Laboratory Equipment will feature more than 750 exhibitors in more than 2050 booths showing the latest analytical instruments, related chemicals, and publications. Several awards will be presented to scientists who have contributed extensively to analytical chemistry and applied spectroscopy. The 1987 P i t t s b u r g h Analytical Chemistry Award, sponsored by the Society for Analytical Chemists of P i t t s b u r g h , will be given to Fred McLafferty of Cornell University in recognition of his continuing contributions in mass spectrometry. The presentation will be made at an award symposium on Tuesday, March 10. The 1987 Pittsburgh Spectroscopy Award, sponsored by the Spectroscopy Society of Pittsburgh, will be presented to Paul Lauterbur of the University of Illinois at Urbana-Champaign at a symposium on Wednesday, March 11. Lauterbur is being recognized for his work in nuclear magnetic resonance spectrometry, including heteronuclear

NMR and NMR imaging. The 1987 Dal Nogare Award will be presented by the Chromatography Forum of the Delaware Valley to Fred Régnier of Purdue University at a symposium on Tuesday, March 10. Régnier is being honored for his contributions to the study of fundamental principles of macromolecular retention and separation. The 1987 Williams-Wright Award, sponsored by the Coblentz Society, will be presented to A. Lee Smith of Dow Corning for his work in group frequencies, molecular structure determination, and structure-property relationships for organo-silicon compounds. The award will be presented at a symposium on Thursday, March 12. The 1987 Charles N. Reilley Award, given by the Society of Electroanalytical Chemistry (SEAC) and sponsored by Bioanalytical Systems and the Reilley Endowment Fund of SEAC, will be presented to Robert Osteryoung of the State University of New York at Buffalo for his work in pulse polarography, the application of computers to electrochemistry, and electrochemistry of molten salts. The award symposium will be held on Wednesday, March 11. The 1987 Maurice R. Hasler Award, sponsored by Applied Research Laboratories and administered by the Spectroscopy Society of Pittsburgh, will be given to George Pimentel for his

136 A · ANALYTICAL CHEMISTRY, VOL. 59, NO. 3, FEBRUARY 1, 1987

work with matrix isolation spectrometry, chemically pumped lasers, and time-resolved spectrometry at a symposium on Wednesday, March 11. The 1986 Pittsburgh Conference Memorial National College Grants, sponsored by the Pittsburgh Conference on Analytical Chemistry and Applied Spectroscopy, the Spectroscopy Society of Pittsburgh, and the Society for Analytical Chemists of Pittsburgh, have been awarded to the following colleges: Blackhawk Technical Institute, Janesville, Wis.; Kalamazoo College, Kalamazoo, Mich.; Lebanon Valley College, Annville, Pa.; Médaille College, Buffalo, N.Y.; Middlesex Community College, Bedford, Mass.; Regis College, Weston, Mass.; Rockhurst College, Kansas City, Mo.; Southeast Community College, Cumberland, Ky.; St. Mary of the Plains College, Dodge City, Kan.; St. Mary's College of California, Moraga, Calif.; and St. Scholastica College, Duluth, Minn. In 1987, at least eight colleges will be selected to receive awards for the purchase of scientific equipment, audiovisual and other teaching materials, and library materials for use in teaching science at the undergraduate level. Eligibility for the awards ($2500 maximum) will be based on proposals submitted by the colleges. Further information about the 1987 awards appears in the January 1 issue (p. 26 A).

March 11

March 9 Monday Morning SYMPOSIUM—Computer-Aided Microscopy and Analysis SYMPOSIUM—-Occupational Health and Safety in the Laboratory SYMPOSIUM—Reflectance Infrared Spectroscopy Air Pollution I Chemometrics and Special Data Handling Methods Chromatographic Analysis of Herbicides, Pesticides, and Pollutants Computerized Spectroscopy Electrochemistry—Kinetics and Mechanisms Gas Chromatographic Applications Ion Chromatography—Hardware Multidimensional Chromatography New Instrumentation NMFt Water Pollution I POSTER SESSIONS Monday Afternoon SYMPOSIUM—Instrumentation and Automation of Environmental Sample Analysis SYMPOSIUM—Multidimensional Separations SYMPOSIUM—NMR in Solids Air Pollution II Automated Laboratory Analysis I Electrochemistry—Advances in Methodology HPLC—Detectors I HPLC—Pharmaceutical Analysis Industrial Hygiene and Food Analysis (HPLC) Near-Infrared I New Instrumentation Concepts Sample Introduction Techniques for GC UV-Vis Spectroscopy: Recent Advances and General Analysis

March 10 Tuesday M o r n i n g SYMPOSIUM—The Analytical Chemistry Opportunity in Process Instrumentation SYMPOSIUM—ASTM E-42: Hybrid Analytical Techniques Involving Surface Analysis SYMPOSIUM—Pittsburgh Analytical Chemistry Award—Future Directions in MS AAS—Methodology Automated Laboratory Analysis II Clinical Chemistry Electrochemistry—Advances in Methodology Emission Spectroscopy and Magnetic Resonance Food Analysis GC—Detectors HPLC—Proteins and Peptides Infrared I—Microspectroscopy, Infrared Instrumentation Ion Chromatography—Applications Water Pollution II POSTER SESSIONS Tuesday A f t e r n o o n SYMPOSIUM—Chemometrics in the Computer-Integrated Laboratory SYMPOSIUM—1987 Dal Nogare Award SYMPOSIUM—Williams-Wright Award Atomic Absorption Analysis and Application Biochemical Analysis I Electrochemistry—Chemically Modified Electrodes Flow Injection Analysis GC—Applications and Optimization Ion Chromatography—New Approaches to Separation and Detection MS—Instrumentation and Applications New Concepts in Instrumentation and Data Handling Plasma Emission Spectroscopy I Surface Analysis Thin-Layer Chromatography and Preparative LC

Wednesday Morning SYMPOSIUM—New Developments in FTMS SYMPOSIUM—Pittsburgh Spectroscopy Award and Maurice M. Hasler Award SYMPOSIUM—Stationary-Phase Structure and Retention in ReversedPhase LC Biochemical Analysis II Computer Augmentation of Chromatography and Spectroscopy Forensic and Drug Analysis Gas Chromatographic Analysis of Crude Oil, Petroleum Products, and Light Hydrocarbons HPLC—Applications and Methodology Infrared II—Quantitative Analysis Molecular Fluorescence and Luminescence I Particle Size Analysis and Flow Injection Analysis Plasma Emission Spectroscopy II Thermal Analysis I X-ray Fluorescence and AAS—New Instrumental Techniques POSTER SESSIONS Wednesday Afternoon SYMPOSIUM—LC/MS and SFC/MS: Will They Replace GC/MS? SYMPOSIUM—Charles N. Reilley Award SYMPOSIUM—Separation Science and Technology: Metals Countercurrent Chromatography Environmental Analysis and Thermal Analysis II HPLC—Physiological Analysis HPLC—Stationary Phase Evaluation Infrared III—Matrix Isolation and Other Topics Molecular Fluorescence and Luminescence II New Advances in Column Technology for GC MS Instrumentation Plasma Emission Spectroscopy III Recent Developments in Chromatography Instrumentation Size Exclusion Chromatography

March 12 Thursday Morning SYMPOSIUM—Advances in Raman Spectroscopy SYMPOSIUM—Detectors for LC and SFC SYMPOSIUM—Symposium Honoring the Late Tomas Hirschfeld Analytical Aspects of SFC Biomedical Pharmaceutical I Characterization of Polymers I Electrochemistry—Detectors FTMS and ICP-MS GC/MS and LC/MS HPLC—Biological Analysis HPLC—Stationary-Phase Chemistry Instrument Automation and Interfacing Infrared IV—-Applications Plasma Emission Spectroscopy IV

Thursday Afternoon SYMPOSIUM—ICP/MS SYMPOSIUM—Immobilized Reagents in Chemical Analysis SYMPOSIUM—Quality and Productivity in the Analytical Laboratory Biomedical Pharmaceutical II Characterization of Polymers II Computerized and Automated Instrumentation Electrochemistry HPLC—Detectors II HPLC—Optimization Molecular Fluorescence and Luminescence III Near-Infrared ll/lnfrared Analysis IV Plasma Emission Spectroscopy V/Capillary SFC Raman Spectroscopy I Robotics—Laboratory Applications

March 13 Friday M o r n i n g Advances in SFC Applications of Commercial Computer Systems Computers and Laboratory Management General Analysis HPLC—Detection and Optimization HPLC—Hardware MS/MS and SIMS New Advances in GC Instrumentation and Automation Raman Spectroscopy II Robotics—Applications and Systems Updates Trace Analysis—Biological and Environmental

Monday, March 9, 1987 SYMPOSIUM Computer-Aided Microscopy and Analysis - arranged by D.E. Newbury o( National Bureau of Standard·

9:35 (013) Use of Diffuse Reflectance Infrared Spectroscopy in the Investigation of Chemical Reactions with Surfaces—DE. LEYDEN, Colorado State University 10:15 RECESS 10:30 (014) Vibrational Structure of Adsorbates on Metal Surfaces -B S PONS, University of Utah 11:10 (015) Quantitative Analysis of Surface Films by Reflectance Spectroscopy—D. ALLARA, Bell Communications Res., Inc. 11:50 Round Table Discussion

Monday Morning, Ballroom B, Atlantis D.E. Newbury, Presiding National Bureau of Standards 8:50 (001) Mlcrobeam Analysis: The Historical Development of Composi­ tional Mapping Techniques—D.E. NEWBURY. National Bureau of Standards 9:20 (002) Quantitative Compositional Mapping by Electron Probe Micro­ analysis with Digital Imaging - RL MYKLEBUST. National Bureau of Standards 9:50 (003) Compositional Mapping in Secondary Ion Mass Spectrometry with Direct Digitization Using the Resistive Anode Encoder—D. A. REED. Charles Evans S Associates 10:20 RECESS 10:35 (004) The New Electron Microscopy: Imaging the Chemistry of Nature—CE. FI0RI, National Institutes of Health 11:05 (005) Nanometer Ion Imaging—M T. BERNIUS, Cornell University, Y.C. Ling, G.H. Morrison 11:35 (006) Advanced Image Processing Techniques for Computer-Aided Microscopy—D. BRIGHT, National Bureau of Standards

SYMPOSIUM Occupational Health and Safety in the Laboratory-arrangedby J.A. Wrontkl of NATLSCO Monday Morning, Ballroom A, Atlantis J.A. Wronski, Presiding NATLSCO 8:50 Introductory Remark» - J A WRONSKI 8:55 (007) Laboratory Ventilation Evaluation—J GORSKI, Kemper Corporation 9:25 (008) Elements of a Laboratory Safety Program—Ν V STEERE, N.V. Steere Associates 9:55 (009) Hazardous Waste Management In Laboratories—R.T.QUIER, JR., J.T. Baker Chemical Co. 10:25 RECESS 10:40 (010) Monitoring Chemical Exposures in a Laboratory—S.C WR0BLEWSKI, NATLSCO 11:10 (011) Overview of OSHA's Hazard Communication Standard—J.C. SILK, U.S. Dept. of Labor - 0SHA 11:40 Open Discussion Session

SYMPOSIUM Reflectance Infrared Spectroscopy - arranged by J.F. coetzee of University of Pittsburgh Monday Morning, Ballroom A/C, Trump Plaza J.F. Coetzee, Presiding University of Pittsburgh 8:50

Introductory Remarks—J.F COETZEE

8:55 (012) Infrared Reflectance Spectroscopies—PR. GRIFFITHS, University of California, Riverside, N.A. Wright, J. Olinger

Air Pollution I Monday Morning, Ventnor AB, Atlantis F, Lipari, Presiding General Motors Research Labs. 8:50 (016) The Thermal Decomposition Characterization of Organic Materials Using a System for Thermal Diagnostic Studies (STDS)—S.L. MAZER, University of Dayton, W.A. Rubey, J. Stalter, B. Dellinger 9:10 (017) The Determination of Soil Metals In Rain-Scrubbed Airborne Particles—RE. LAMB, Ohio Northern University, J.E. Maslar, A.D. Trusty 9:30 (018) Organic Vapors and Benz-a-Pyrene in the Indoor Air from NonVented Kerosene Heaters and Wood Burning Fireplaces—J.W. BOZZELLI, New Jersey Inst, of Technology, J.I. Dong, C. Bobenhausen, A. Mishra 9:50 (019) A Portable Concentration Device for Trace Analysis of Organics in Air and Water— E.B. OVERTON, Louisiana State University, R.W. Sherman, E.S. Collard 10:10 (020) Selective Inclusion of Solvent Vapor Molecules into a Hexalactam Macrocycle Host—E.B. OVERTON, Louisiana State University, S.S. Stewart, V.K. Gupta, G.R. Newkome 10:30 RECESS 10:45 (021) Environmental Optic Sensors—J.N. ROE, Lawrence Livermore Nat'l. Lab. 11:05 (022) Multibed Adsorbent Tube Monitors a Wide Range of Airborne Organic Contaminants—W.R. BETZ, Supelco, Inc., G.D. Wachob 11:25 (023) Improved Sampling Cassette and Analysis for Airborne Acids-E.H. BAUGHMAN, Amoco Corporation, E. Watson, Jr. 11:45 (024) Development of a New Trapping System for Purge and Trap Analysis of Volatile Organic Compounds Ν Η MOSESMAN, Supelco, Inc., W.R. Betz, D.T. Daugherty, S.D. Corman

Chemometrics and Special Data Handling Methods Monday Morning, Chelsea AB, Trump Plaza G.L. Carlson, Presiding GPU Nuclear Corporation 8:50 (025) Characterization of Mlcrosensor Arrays—W.P. CAREY, University of Washington, B.R. Kowalski 9:10 (026) Applications of Cellular Automata: Attractors and Fractals in Analytical Chemistry?—R A LODDER, Indiana University, M. Selby. G.M. Hieftje 9:30 (027) Instrumental Analysis of Aircraft Fuels and Chemometric Procedures for Predicting Their Physical and Chemical Properties—W.A. RUBEY, University of Dayton, P.W. Hovey, S.L. Mazer, R.C. Striebick 9:50 (028) Parameter Estimation of Chemical Kinetic Data Using the Extended Kalman Filter—TO. BARKER, University of Delaware, S.D. Brown 10:10 (029) The Use of An Expert System In Selecting Methods for Chemical Analysis—FA. SETTLE, JR., Virginia Military Institute, M.A. Pleva 10:30 RECESS